• Carbon letters
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• v.2 no.1
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• pp.55-60
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• 2001

Graphite intercalation compounds (GIC) were prepared by direct reaction of $SO_3$ gas with flake graphite. The intercalated $SO_3$ molecules were ejected by rapid heating to $950^{\circ}C$ under an oxidizing atmosphere for about 1 minute, resulting in surprisingly high expansion in the direction of c-axis. The characteristics of the micro-structure and pore size distribution were examined with a SEM and mercury intrusion porosimetry. The XRD analysis and spectroscopic analysis were used for the identification of the graphite and surface chemistry state. The pore size distribution of the exfoliated graphite (EG) was a range of $1{\sim}170{\mu}m$. The higher expanding temperature the higher expanded volume, so oil sorption capacities were 58.8 g of bunker-C oil and 34.7 g of diesel oil per 1 g of the the EG. The sorption equilibrium was achieved very rapidly within several minutes. As the treatment temperature increases, bulk density decreases.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.28 no.12
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• pp.1494-1500
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• 2004

A zero-dimensional direct simulation Monte Carlo(DSMC) model is developed for simulating diatomic gas including vibrational kinetics. The method is applied to the simulation of two systems: vibrational relaxation of a simple harmonic oscillator and translational-rotational-vibrational energy exchange process under heating and cooling. In the present DSMC method, the variable hard sphere molecular model and no time counter technique are used to simulate the molecular collision kinetics. For simulation of diatomic gas flows, the Borgnakke-Larsen phenomenological model is adopted to redistribute the translational and internal energies.

• Transactions of the Korean Society of Automotive Engineers
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• v.4 no.1
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• pp.147-154
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• 1996

An one-zone heat release analysis was studied for a 6 cylinder direct injetction compressionignition engine. The heat transfer constants in this anlysis were calibrated to match the measured fuel energy at 1,000 rpm full load, which was the fuel mass multiplied by the fuel's heating value. The integrated gross heat release values were close to the measured fuel energy at various full load operating conditions. The combustion inefficiency from this calculation was proportional to the smoke of exhaust gas.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
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• v.9 no.4
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• pp.517-526
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• 1997

This study is focused on the development and selection of the optimal cool tube system to maximize its thermal performance. Cool tube is devised to reduce the heating and cooling load of building by preheating or refreshing of intake air with buried pipes. Finite volume method is adopted to solve the conduction problem between the cool tube and earth. We examine the cool tube system for two operating periods, a short term(12 hours) and a long term(3 months). The results of short term operations reveal that condensation significantly influences and raises the exit air temperature. For long term operations, optimum conditions of cool tube system are obtained with variations of flow-rate, depth, length and diameter of cool tube.

• Bulletin of the Korean Chemical Society
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• v.23 no.12
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• pp.1801-1805
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• 2002

The graphite intercalation compounds(GIC) were prepared by a dry process that led to the intercalation from the direct reaction of gaseous $SO_3$ with flake type graphite. The basal spacing of the GIC was increased from 8.3 ${\AA}$ to 12 in the gallery height. The ejection of interlayer $SO_3$ molecules by the heating for 1 minute at $950^{\circ}C$ resulted in an exfoliated graphite (EG) with surprisingly high expansion in the direction of c-axis. The expansion ratios of the exfoliated graphites were increased greatly between 220 times and 400 times compared to the original graphite particles, and the bulk density was range of 0.0053 to 0.01 $g/cm^3$, depending on reaction time. The pore size distribution of exfoliated graphite was in the range of $10-170{\mu}m$, which exhibites both mesoporosity and macroporosities. This result indicates that the direct reaction of graphite paricles with gaseous $SO_3$ can be proposed as an another route for the exfoliated graphite having excellent physical properties.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.342-343
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• 2006

In order to develop the nano-sized WC powder that improved the hardness of hardmetals, carbothermal reduction of WO3 by C was examined by using the thermogravimetric analysis. At the direct carburization reaction path of $WO_3{\rightarrow}WO_{2.72}{\rightarrow}WO_2{\rightarrow}W{\rightarrow}W_2C{\rightarrow}WC$, the nano-sized grain was generated at the reaction stage $WO_{2.72}$ to $WO_2$ and W. For trial production, the intermediate products which consists of metal and carbide phases obtained by the first heating has been carburized to the final WC powder. We succeeded in the development of the WC powder of about 70nm. In addition, the nano-sized WC powder in which the vanadium of the most effective grain growth inhibitor was uniformly dispersed was developed.

• Journal of the Korea institute for structural maintenance and inspection
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• v.6 no.4
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• pp.201-207
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• 2002

An advanced fiber sheet has been widely used for strengthening of the concrete structures due to its excellent properties such as high strength and light weight. Bond strength is very important in strengthening the concrete structures using an advanced fiber sheet. This research examines the bond behavior between fiber sheet and concrete, investigates the bond strength by the direct pull-out test and the tensile-shear test. To obtain the tensile-shear strength a double-face shear type bond test is conducted. The primary test variables are the types of concrete surface roughness (disk-grinding/chipping) and retrofitting methods (bonding/injection). Thirty specimens were tested to evaluate the bond strength. It is shown that the average bond strength between fiber sheet and concrete by the direct pull-out test and the tensile-shear test is $22.3{\sim}23.1kgf/cm^2$ $17.92{\sim}19.75kgf/cm^2$, respectively.

• Macromolecular Research
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• v.17 no.11
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• pp.901-906
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• 2009

Several aromatic optically active polyamides (PA)s were synthesized from 5-(2-phthalimidiylpropanoylamino)isophthalic acid with various aromatic diamines via direct polycondensation with triphenyl phosphite and pyridine in the presence of calcium chloride and N-methyl-2-pyrrolidone under microwave irradiation and conventional heating conditions. Under the optimized conditions, the reaction mixture was irradiated for 2 min. with a 100% irradiation power (900 W). The resulting polymers were obtained in high yield and moderate inherent viscosity ranging from 0.35 to 0.60 dL/g. All synthesized polymers showed excellent solubility in amide-type solvents. Thermogravimetric analysis revealed a 10% weight loss temperature and char yield at $600^{\circ}C$ in a nitrogen atmosphere of > $350^{\circ}C$ and > 58%, respectively, which suggests that the resulting PAs have good thermal stability.

• Journal of the Korean Magnetic Resonance Society
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• v.23 no.2
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• pp.46-50
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• 2019

Spin orbit torque would be applied as the next generation of MRAM, so many researchers are interested in related field. To make a more efficient device, electric current should convert into spin current with high efficiency. Moreover, it becomes important to measure efficiency of spin orbit torque accurately. We measured spin torque FMR of W/CoFeB hetero structure system with direct current. The efficiencies of the damping like torque and field like torque were measured by using the linewidth and on-resonance field proportional to direct current. In addition, we analyzed that a quadratic shift of the on-response field was caused by the Joule heating.

• Journal of the Korean Ceramic Society
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• v.27 no.1
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• pp.136-146
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• 1990

Whiskers of SiC were grown from the mixture of silica and graphite powders by Acheson method(direct heating method). The structrua, morphological and chemical characterizations have been performed by X-ray diffractometer(XRD), transmission electron microscopy(TEM), optical microscopy(OM), scanning electron microscopy(SEM), X-ray photoelectron spectroscopy(XPS) and energy dispersive spectrometer(EDS). The growth mechanism of SiC whiskers is also discussed.