• Title/Summary/Keyword: Direct Comparison Method

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The Screening and Pattern Comparison of Organic Acids in 3 Kinds of Medicinal Herbal Extracts (3가지 약용 허브 추출물에 함유된 유기산 검색 및 조성 비교)

  • Chung, Ha-Yull;Jung, Do-Hyun;Park, Young-Joon
    • Korean Journal of Food Science and Technology
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    • v.32 no.5
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    • pp.997-1001
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    • 2000
  • The organic acids in 3 kinds of medicinal herbal extracts were screened and compared each other according to their organic acid contents by an efficient gas chromatographic method. It involves solid-phase extraction of organic acids using Chromosorb P with subsequent conversion to stable tert-butyldimethysilyl derivatives for the direct analysis by capillary column gas chromatography and gas chromatography-mass spectrometry. Total of 24 organic acids were reproducibly identified from 3 kinds of herbal extracts. When the GC profiles were simplified to their retention index spectra, characteristic patterns were obtained for each herb sample. As expected, three kinds of herbal extracts showed three distinct patterns.

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On the kinematic coupling of 1D and 3D finite elements: a structural model

  • Yue, Jianguang;Fafitis, Apostolos;Qian, Jiang
    • Interaction and multiscale mechanics
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    • v.3 no.2
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    • pp.192-211
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    • 2010
  • In most framed structures the nonlinearities and the damages are localized, extending over a limited length of the structural member. In order to capture the details of the local damage, the segments of a member that have entered the nonlinear range may need to be analyzed using the three-dimensional element (3D) model whereas the rest of the member can be analyzed using the simpler one-dimensional (1D) element model with fewer degrees of freedom. An Element-Coupling model was proposed to couple the small scale solid 3D elements with the large scale 1D beam elements. The mixed dimensional coupling is performed imposing the kinematic coupling hypothesis of the 1D model on the interfaces of the 3D model. The analysis results are compared with test results of a reinforced concrete pipe column and a structure consisting of reinforced concrete columns and a steel space truss subjected to static and dynamic loading. This structure is a reduced scale model of a direct air-cooled condenser support platform built in a thermal power plant. The reduction scale for the column as well as for the structure was 1:8. The same structures are also analyzed using 3D solid elements for the entire structure to demonstrate the validity of the Element-Coupling model. A comparison of the accuracy and the computational effort indicates that by the proposed Element-Coupling method the accuracy is almost the same but the computational effort is significantly reduced.

Effect of Sintering Condition on Tensile Strength of Fe-based Non-equiatomic High Entropy Alloy (철계 비동일분율 고엔트로피 합금의 인장 강도에 미치는 소결 조건 영향)

  • Seo, Namhyuk;Jeon, Junhyub;Kim, Gwanghun;Park, Jungbin;Son, Seung Bae;Lee, Seok-Jae
    • Journal of Powder Materials
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    • v.28 no.3
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    • pp.221-226
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    • 2021
  • We fabricate the non-equiatomic high-entropy alloy (NE-HEA) Fe49.5Mn30Co10Cr10C0.5 (at.%) using spark plasma sintering under various sintering conditions. Each elemental pure powder is milled by high-energy ball milling to prepare NE-HEA powder. The microstructure and mechanical properties of the sintered samples are investigated using various methods. We use the X-ray diffraction (XRD) method to investigate the microstructural characteristics. Quantitative phase analysis is performed by direct comparison of the XRD results. A tensile test is used to compare the mechanical properties of small samples. Next, electron backscatter diffraction analysis is performed to analyze the phase fraction, and the results are compared to those of XRD analysis. By combining different sintering durations and temperature conditions, we attempt to identify suitable spark plasma sintering conditions that yield mechanical properties comparable with previously reported values. The samples sintered at 900 and 1000℃ with no holding time have a tensile strength of over 1000 MPa.

Comparison of Supersonic Jet Characteristics between Hydrogen and Helium injected by Small-cone-angle Pintle-type Hydrogen Injector (수소 및 헬륨을 이용한 작은 원추각 핀틀형 수소인젝터의 초음속 제트 특성 비교)

  • Gyuhan Bae;Juwan Lim;Jaehyun Lee;Seoksu Moon
    • Journal of ILASS-Korea
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    • v.29 no.2
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    • pp.83-90
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    • 2024
  • Understanding the fundamental characteristics of supersonic hydrogen jets is important for the optimization of combustion in hydrogen engines. Previous studies have used helium as a surrogate gas to characterize the hydrogen jet characteristics due to potential explosion risks of hydrogen. It was based on the similarity of hydrogen and helium jet structures in supersonic conditions that has been confirmed using hole-type injectors and large-cone-angle pintle-type injectors. However, the validity of using helium as a surrogate gas has not been examined for recent small-cone-angle pintle-type injectors applied to direct-injection hydrogen engines, which form a supersonic hollow cone near the nozzle and experience the jet collapse downstream. Differences in the physical properties of hydrogen and helium could alter the jet development characteristics that need to be investigated and understood. This study compares supersonic jet structures of hydrogen and helium injected by a small-cone-angle (50°) pintle-type hydrogen injector and discusses their differences and related mechanisms. Jet penetration length and dispersion angle are measured using the Schlieren imaging method under engine-like injection conditions. As a result, the penetration length of hydrogen and helium jets showed a slight difference of less than 5%, and the dispersion angle showed a maximum of 10% difference according to the injection condition.

Modeling and Trends of Road Transport Development in Eastern European Countries

  • Viktoriia Harkava;Olena Pylypenko;Oleksandr Haisha;Armen Aramyan;Volodymyr Kairov
    • International Journal of Computer Science & Network Security
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    • v.24 no.3
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    • pp.189-195
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    • 2024
  • Road transport occupies the largest share in domestic and international transport. It is of key importance for the development of the economy, forasmuch as it provides the livelihood of the population, the development of the national economy, the possibility of establishing foreign economic relations. The purpose of the research is as follows: analysis of the current state of functioning of the road transport sector in Eastern Europe and identification of key problems and trends in its development. Research methods: Methods of grouping, comparison and generalization, correlation analisys have been used to identify the dynamics of the main indicators of road transport in Eastern Europe. The method of correlation-regression analysis has been applied to determine the impact of increasing the length of roads on the turnover of the road freight transport and the number of employed population in this area. Results. It has been found that the increase in the employed population by 96% and increase in revenues from transportation and storage of goods, postal and courier services (turnover of the road freight transport - in the original language) in the field of road transport by 82% is explained by the change in transport infrastructure capacity by increasing length of highways. According to the correlation analysis, it has been revealed that there is a high direct dependence between the length of roads and increased revenues from transportation and storage of goods in the field of road transport, as well as between the length of roads and increasing employment in this area.

Endoscopic ultrasound-guided coiling and glue is safe and superior to endoscopic glue injection in gastric varices with severe liver disease: a retrospective case control study

  • Kapil D. Jamwal;Rajesh K. Padhan;Atul Sharma;Manoj K. Sharma
    • Clinical Endoscopy
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    • v.56 no.1
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    • pp.65-74
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    • 2023
  • Background/Aims: Gastric varices (GV) are present in 25% of cirrhotic patients with high rates of rebleeding and mortality. Data on endoscopic ultrasound (EUS)-guided treatment in severe liver disease (model for end stage liver disease sodium [MELD-Na] >18 and Child-Turcotte-Pugh [CTP] C with GV) are scarce. Thus, we performed a retrospective comparison of endoscopic glue injection with EUS-guided therapy in cirrhotic patients with large GV. Methods: A retrospective study was performed in the tertiary hospitals of India. A total of 80 patients were recruited. The inclusion criteria were gastroesophageal varices type 2, isolated gastric varices type 1, bleeding within 6 weeks, size of GV >10 mm, and a MELD-Na >18. Treatment outcomes and complications of endoscopic glue injection and EUS-guided GV therapy were compared. Results: In this study, the patients' age, sex, liver disease severity (CTP, MELD-Na) and clinical parameters were comparable. The median number of procedures, injected glue volume, complications, and GV obturation were better in the EUS group, respectively. On subgroup analysis of the EUS method (e.g., direct gastric fundus vs. paragastric collateral [PGC] coil placement), PGC coil placement showed decreased coil requirement, less injected glue volume, decreased luminal coil extrusion, and increased successful GV obturation. Conclusions: EUS-guided treatment is more efficient and safer, and requires a smaller number of treatment sessions, as compared to endoscopic treatment in severe liver disease patients with large GV. Furthermore, PGC coil placement increases the complete obliteration of GV.

Development of a Rainfall Time Distribution Model for Urban Watersheds (도시유역의 유출특성을 고려한 강우분포 모형의 개발)

  • Joo, Jin-Gul;Lee, Jung-Ho;Jo, Deok-Jun;Jun, Hwan-Don;Kim, Joong-Hoon
    • Journal of Korea Water Resources Association
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    • v.40 no.8
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    • pp.655-663
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    • 2007
  • This study suggests a new time distribution method of rainfall for small urban watersheds. IETD (Interevent Time definition) determination method considering basin characteristics and dimensionless accumulation rainfall curves involving rainfall events with shorter duration than 3-hours are suggested. A new definition of IETD is the time period from the end of a rainfall event to the end of a direct runoff. Using the method, we drive an area-IETD regression curve for the Joong-Rang basin. The rainfall event with 10 year-return periods, 2-hour duration is distributed and applied four urban watersheds. In the four watersheds, we calculate hydrographs for four watersheds using SWMM and compare them with ones of the Huff's distribution model. From the comparison, we find that peak flows resulted from the developed methodology are $11\sim15%$ larger than ones from the Huff's model. As conclusion, the Huff method should be adopted for the urban watersheds with careful verification.

Evaluation of MODIS NDVI for Drought Monitoring : Focused on Comparison of Drought Index (가뭄모니터링을 위한 MODIS NDVI의 활용성 평가: 가뭄지수와의 비교를 중심으로)

  • Park, Jung-Sool;Kim, Kyung-Tak
    • Spatial Information Research
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    • v.17 no.1
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    • pp.117-129
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    • 2009
  • South Korea has been undergoing spring drought periodically and diverse researches using vegetation index have been carried out to monitor spring droughts. The strength of the vegetation index-based drought monitoring is that the monitoring method enables efficient spatio-temporal grasp of changes in drought events. According to the development of low resolution satellite images such as MODIS, which are characterized by outstanding temporal resolution, the use of the method is expected to increase. Drought analysis using vegetation index considered only meteorological factor as a cause that affects vitality of vegetation. But many indirect and direct factors affect vegetation stress, So many uncertainties are involved in such method of analysis. To secure objectivity of drought analysis that uses vegetation index it is therefore necessary to compare the method with most representative drought analysis tools that are used for drought management. In this study, PDSI and SPI which a meteorological drought index that quantifies drought and that is used as a basic index for drought monitoring and MODIS NDVI are compared to propose correlation among them and to show usefulness of drought assessment that uses vegetation index. This study shows changing patterns of NDVI and SPI 6-month are similar and correlation between NDVI and SPI was highest in inland vegetation cover.

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HIPIMS Arc-Free Reactive Deposition of Non-conductive Films Using the Applied Material ENDURA 200 mm Cluster Tool

  • Chistyakov, Roman
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.96-97
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    • 2012
  • In nitride and oxide film deposition, sputtered metals react with nitrogen or oxygen gas in a vacuum chamber to form metal nitride or oxide films on a substrate. The physical properties of sputtered films (metals, oxides, and nitrides) are strongly influenced by magnetron plasma density during the deposition process. Typical target power densities on the magnetron during the deposition process are ~ (5-30) W/cm2, which gives a relatively low plasma density. The main challenge in reactive sputtering is the ability to generate a stable, arc free discharge at high plasma densities. Arcs occur due to formation of an insulating layer on the target surface caused by the re-deposition effect. One current method of generating an arc free discharge is to use the commercially available Pinnacle Plus+ Pulsed DC plasma generator manufactured by Advanced Energy Inc. This plasma generator uses a positive voltage pulse between negative pulses to attract electrons and discharge the target surface, thus preventing arc formation. However, this method can only generate low density plasma and therefore cannot allow full control of film properties. Also, after long runs ~ (1-3) hours, depends on duty cycle the stability of the reactive process is reduced due to increased probability of arc formation. Between 1995 and 1999, a new way of magnetron sputtering called HIPIMS (highly ionized pulse impulse magnetron sputtering) was developed. The main idea of this approach is to apply short ${\sim}(50-100){\mu}s$ high power pulses with a target power densities during the pulse between ~ (1-3) kW/cm2. These high power pulses generate high-density magnetron plasma that can significantly improve and control film properties. From the beginning, HIPIMS method has been applied to reactive sputtering processes for deposition of conductive and nonconductive films. However, commercially available HIPIMS plasma generators have not been able to create a stable, arc-free discharge in most reactive magnetron sputtering processes. HIPIMS plasma generators have been successfully used in reactive sputtering of nitrides for hard coating applications and for Al2O3 films. But until now there has been no HIPIMS data presented on reactive sputtering in cluster tools for semiconductors and MEMs applications. In this presentation, a new method of generating an arc free discharge for reactive HIPIMS using the new Cyprium plasma generator from Zpulser LLC will be introduced. Data (or evidence) will be presented showing that arc formation in reactive HIPIMS can be controlled without applying a positive voltage pulse between high power pulses. Arc-free reactive HIPIMS processes for sputtering AlN, TiO2, TiN and Si3N4 on the Applied Materials ENDURA 200 mm cluster tool will be presented. A direct comparison of the properties of films sputtered with the Advanced Energy Pinnacle Plus + plasma generator and the Zpulser Cyprium plasma generator will be presented.

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Comparison of Mycobacterium tuberculosis Specific Antigen Stimulation Time for Performing Interferon Gamma mRNA Assay for Detecting Latent Tuberculosis Infection

  • Kim, Sunghyun;Cho, Jang-Eun;Kim, Hyunjung;Lee, Dongsup;Jeon, Bo-Young;Lee, Hyejon;Cho, Sang-Nae;Kim, Young Keun;Lee, Hyeyoung
    • Biomedical Science Letters
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    • v.19 no.2
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    • pp.90-97
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    • 2013
  • The tuberculin skin test (TST) and interferon gamma (IFN-${\gamma}$) release assay (IGRA) have been widely used for diagnosis of latent tuberculosis infection (LTBI). In order to overcome limitations of current LTBI diagnostic methods, the development of a novel molecular assay which is able to measure the IFN-${\gamma}$ messenger RNA (mRNA) expression level after stimulation with Mycobacterium tuberculosis (MTB) specific antigen was recently developed. The ability of a molecular assay to detect MTB infection was similar to commercial IGRA however, the optimal incubation time for stimulating IFN-${\gamma}$ was not yet established. Therefore, in this study the direct comparisons of MTB Ag stimulation times (4 and 24 hrs) were performed for diagnosis of MTB infection. Data showed that the coincident rate between QFT-GIT IFN-${\gamma}$ ELISA and IFN-${\gamma}$ RT-PCR (4 hrs) was 88.35% and that of QFT-GIT and IFN-${\gamma}$ RT-PCR (24 hrs) was 70.85%. Based on a receiver operating characteristic (ROC) curve, the 4 hrs-MTB specific Ag stimulation time for IFN-${\gamma}$ RT-PCR had the significant P value, 95% CI value, and AUC (P < 0.0001, 95% CI=0.82 to 1.02, and AUC=0.9214) in comparison with 24 hrs-MTB specific Ag stimulation time (P = 0.009, 95% CI=0.06 to 0.94, and AUC=0.7711). These results show that 4-hr was the most optimal MTB Ag stimulation time for performing IFN-${\gamma}$ RT-PCR. Although semi-quantitative RT-PCR had a few analytical limitations, it might be useful as an alternative molecular diagnostic method for detecting MTB infection.