• 제목/요약/키워드: Dip-coated

검색결과 188건 처리시간 0.019초

유기 은 착체 화합물을 코팅용액으로 사용하여 연속적인 담금코팅방법에 의한 은 안정화층 제조 (Preparation of silver stabilizer layer on coated conductor by continuous dip coating method using organic silver complexes)

  • 이종범;김지철;박신근;김병주;김재근;이희균;홍계원
    • 한국초전도ㆍ저온공학회논문지
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    • 제12권1호
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    • pp.1-5
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    • 2010
  • Silver stabilizing layer of coated conductor has been prepared by dip coating method using organic silver complexes containing 10 wt% silver as a starting material. Coated silver complex layer was dried in situ with hot air and converted to crystalline silver by post heat treatment in flowing oxygen atmosphere. A dense continuous silver layer with good surface coverage and proper thickness of 230 nm is obtained by multiple dip coatings and heat treatments. The film heat treated at $500^{\circ}C$ showed good mechanical adhesion and crystallographic property. The interface resistivity between superconducting YBCO layer and silver layer prepared by dip coating was measured as $0.67\;{\times}\;10^{-13}\;{\Omega}m^2$. Additional protecting copper layer with the thickness of $20\;{\mu}m$ was successfully deposited by electroplating. The critical current measured with the specimen prepared by dip coating and sputtering on same quality YBCO layer showed similar value of ~140 A and proved its ability to replace sputtering method for industrial production of coated conductor.

Structure of Surface Oxide Formed on Zinc-Coated Steel Sheet During Hot Stamping

  • Shota Hayashida;Takuya Mitsunobu;Hiroshi Takebayashi
    • Corrosion Science and Technology
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    • 제23권3호
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    • pp.221-227
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    • 2024
  • During hot stamping of hot-dip zinc-coated steel sheets such as hot-dip galvanized steel sheets and hot-dip galvannealed steel sheets, an oxide mainly composed of ZnO is formed on the sheet surface. However, excessive formation of ZnO can lead to a decrease in the amount of metal Zn in the coating layer, decreasing the corrosion resistance of hot-stamped members. Therefore, it is important to suppress excessive formation of ZnO. While the formation of Al oxides and Mn oxides along with ZnO layer during the hot stamping of hot-dip zinc-coated steel sheets can affect ZnO formation, crystal structures of such oxides have not been elucidated clearly. Thus, this study aimed to analyze structures of oxides formed during hot stamping of hot-dip galvannealed steel sheets using transmission electron microscopy. Results indicated the formation of an oxide layer comprising ZnAl2O4 at the interface between ZnO and the coating layer with Mn3O4 at the outermost of an oxide layer.

용융합금도금 강판 적용 노측용 방호울타리 충돌 안전성 평가 해석 사례 연구 (A Simulation Case Study on Impact Safety Assessment of Roadside Barriers Built with High Anti-corrosion Hot-dip Alloy-coated Steel)

  • 노명현
    • 한국안전학회지
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    • 제31권2호
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    • pp.83-89
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    • 2016
  • As the world's industrial development quickens, the highways and regional expressways have been expanding to serve the logistics and transportation needs of people. The burgeoning road construction has led to a growing interest in roadside installations. These must have reliable performance over long periods, reduced maintenance and high durability. Steel roadside barriers are prone to corrosion and other compromises to their functionality. Therefore, using high anti-corrosion steel material is now seen as a viable solution to this problem. Thus, the objective of this paper is to expand the scope of applications for high anti-corrosion steel material for roadside barriers. This paper assesses the impact safety such as structural performance, occupant protection performance and post-impact vehicular response performance by a simulation review on roadside barriers built with high strength anti-corrosion steel materials named as hot-dip zinc-aluminium-magnesium alloy-coated steel. The simulation test results for the roadside barriers built with high strength anti-corrosion steels with reduced sectional thickness meet the safety evaluation criteria, hence the proposed roadside barrier made by high strength and high anti-corrosion hot-dip zinc-aluminium-magnesium alloy-coated steel will be a good solution to serve safe impact performance as well as save maintenance cost.

코팅 방법에 따른 SnO2/Ti 전극의 제조 및 전기화학적 특성 (Preparation and Electrochemical Characterization of SnO2/Ti Electrode by Coating Method)

  • 김한주;손원근;홍지숙;김태일;박수길
    • 전기화학회지
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    • 제9권2호
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    • pp.59-63
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    • 2006
  • 전해코팅 법과 dip-coating 법을 이용해 산화주석(IV)을 티타늄 지지체에 코팅하여, 코팅 방법에 따른 코팅 전극의 물성과 전기화학적 특성에 대해여 연구하였다. HCl 로 전극 에칭 후, nitrate 용액에 $SnCl_2{\cdot}2H_2O$을 용해시켜 pulse technique를 이용하여 전해코팅 하였으며, dip-coating 법 또한 $SnCl_2{\cdot}2H_2O$를 사용하여 1:1V% HCl 용액에 용해시켜 코팅 소결 후 산화주석(IV)코팅 전극을 제작하였다. 두 가지 코팅 방법을 통해 제작된 산화주석(IV)코팅 전극은 전극의 물성을 비교하기 위해 x-ray diffraction (XRD), scanning election microscopy (SEM)를 관찰해보았고, 전기화학적 특성을 평가하기 위해 cyclic voltammetry (CV)를 측정하여 전위창을 비교해 보았다.

디젤엔진 배가스 처리를 위한 세라믹 필터 촉매코팅에 관한 연구 (A Study on catalyst-coated ceramic filter for diesel engine exhaust-gas treatment)

  • 최선희;구국희;정덕영;오광중
    • 청정기술
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    • 제7권1호
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    • pp.65-74
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    • 2001
  • 본 연구는 디젤엔진에서 배출되는 NOx환원용 촉매로서 산화반응에서 우수한 활성을 나타내고 있는 페롭스카이트상의 $LaCoO_3$을 sol-gel 공정을 이용하여 촉매코팅용액을 제조한 후, 이를 기존의 dip-coating방법보다 코팅시간, 코팅량, NO-CO 산화 환원 반응에 있어서 경제적이고 효율적인 modified dip-coating방법을 이용하여 촉매코팅필터를 제조하고 이를 후처리장치에 부착함으로써 디젤엔진에서 배출되는 배가스를 효과적으로 제거시키고자 한다. 실험결과, modified dip-coating방법이 기존의 dip-coating방법에 비해서 코팅에 소요되는 용액량이 8.3배 코팅시간 83.3배 단축되었으며, 코팅량은 2~3배정도 커지고, NO-CO 산화 환원 반응성도 1.1~1.8배 가량 증가하였다. 그리고 코팅점도는 $0.006202kg{\cdot}m/sec$을 이용하여 코팅횟수 2회, 코팅량은 88.56mg/g에서 우수한 반응을 보였다. 또한 세라믹 필터의 셀수에 있어서는 200 CPSI가 적절함을 확인할 수 있다.

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Gas Permeation of Y2O3-SiC Composite Membrane

  • Song, Daheoi;Jung, Miewon
    • 한국세라믹학회지
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    • 제52권4호
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    • pp.234-236
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    • 2015
  • $Y_2O_3$-SiC composite membrane was dip-coated using $Y_2O_3$ sol solution; this membrane was compared with a non- coated one. Each membrane was characterized by XRD, FE-SEM and BET techniques. Hydrogen and CO permeation were tested with self-manufactured Sievert's type equipment. $Y_2O_3$ coating was enhanced for the selectivity of the membrane ($H_2$ versus CO). The hydrogen permeation was measured at 1 bar with increasing temperatures. In case of the coated membrane, hydrogen permeation was found to be $1.24{\times}10^{-7}mol/m^2sPa$ with perm-selectivity of 4.26 at 323 K.

New Corrosion-Resistant Zn-Al-Mg Alloy Hot-Dip Galvanized Steel Sheet

  • Kohei Tokuda;Yasuto Goto;Mamoru Saito;Hiroshi Takebayashi;Takeshi Konishi;Yuto Fukuda;Fumiaki Nakamura;Koji Kawanishi;Kohei Ueda;Hidetoshi Shindo
    • Corrosion Science and Technology
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    • 제23권2호
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    • pp.121-130
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    • 2024
  • In recent years, Zn-Al-Mg alloy galvanized steel sheets have been widely used as coated steel sheets to support social capital in the infrastructure field. A feature of Zn-Al-Mg alloy-coated steel sheets is that they provide a better corrosion protection period than Zn-coated steel sheets. In this study, the corrosion resistance of a new Zn-Al-Mg alloy-coated steel sheet was investigated and compared to that of conventional commercially available coated steel sheets. The investigation confirmed that increasing the Mg concentration in the Zn-Al-Mg-coated steel sheet improved corrosion resistance, which was more than 10 times that of the galvanized steel sheet specified in JIS G 3302. The study findings also confirmed that the corrosion resistance reached more than twice that of the coated steel sheet specified in JIS G 3323. If such galvanized steel sheets are applied to social infrastructures that are exposed to severely corrosive environments, the service life of the infrastructure might be extended.

고내식성 용융합금도금강판 적용 교량난간의 충돌성능 평가 (Crashworthiness Evaluation of Bridge Barriers Built with Hot-dip Zinc-aluminium-magnesium Alloy-coated Steel)

  • 노명현
    • 한국산학기술학회논문지
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    • 제17권3호
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    • pp.171-176
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    • 2016
  • 본 논문은 도로안전시설물의 공용중 부식 발생으로 인한 기능 손실을 줄일 수 있는 방안으로 고내식성 용융합금도금 강판을 적용한 도로안전시설물을 제안한다. 고내식성 용융합금도금강판을 적용한 도로안전시설물 제품에 대한 신뢰성 있는 충돌성능 평가 기초자료를 제공할 목적으로 고내식강이 적용된 교량난간 제품에 대한 충돌 시뮬레이션 및 실물 차량 충돌시험 연구를 수행한다. 시뮬레이션 및 실차충돌 시험 결과, 변형률 속도 의존성을 고려할 수 있는 정교한 동특성 재료모델을 도입한 충돌 시뮬레이션을 통해 얻어지는 충돌 거동과 실물 차량 충돌 시험 결과가 매우 유사한 것으로 도출되었다. 본 논문에서 제안된 고내식성 용융합금도금 강판을 적용한 교량난간은 실물 차량 충돌 시험의 충돌성능 평가 기준을 모두 충족시켜 현장 적용을 앞두고 있다.

수소제조를 위한 다공성 FeCrAl 금속 합금 Foam의 NiO 촉매 담지 및 미세구조 분석 (Synthesis and Microstructure Analysis of NiO Catalysts Coated on the FeCrAl Metal Alloy Foam for Hydrogen Production)

  • 이유진;안건형;박만호;이창우;최상현;정주용;조성종;이근재;안효진
    • 한국재료학회지
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    • 제24권8호
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    • pp.393-400
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    • 2014
  • NiO catalysts were successfully coated onto FeCrAl metal alloy foam as a catalyst support via a dip-coating method. To demonstrate the optimum amount of NiO catalyst on the FeCrAl metal alloy foam, the molar concentration of the Ni precursor in a coating solution was controlled, with five different amounts of 0.4 M, 0.6 M, 0.8 M, 1.0 M, and 1.2 M for a dip-coating process. The structural, morphological, and chemical bonding properties of the NiO-catalyst-coated FeCrAl metal alloy foam samples were assessed by means of field-emission scanning electron microscopy(FESEM), scanning electron microscopy-energy dispersive spectroscopy(SEM-EDS), X-ray diffraction(XRD), and X-ray photoelectron spectroscopy(XPS). In particular, when the FeCrAl metal alloy foam samples were coated using a coating solution with a 0.8 M Ni precursor, well-dispersed NiO catalysts on the FeCrAl metal alloy foam compared to the other samples were confirmed. Also, the XPS results exhibited the chemical bonding states of the NiO phases and the FeCrAl metal alloy foam. The results showed that a dip-coating method is one of best ways to coat well-dispersed NiO catalysts onto FeCrAl metal alloy foam.

진공 슬러리 담금 코팅 공정에 의한 고체 산화물 연료전지용 박막 전해질막 제조에 관한 연구 (Fabrication Of Thin Electrolyte Layer For Solid Oxide Fuel Cell by Vacuum Slurry Dip-coating Process)

  • 손희정;임탁형;이승복;신동열;송락현;김성현
    • 한국수소및신에너지학회논문집
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    • 제17권2호
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    • pp.204-211
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    • 2006
  • The electrolyte in the solid oxide fuel cell must be dense enough to avoid gas leakage and thin enough to reduce the ohmic resistance. In order to manufacture the thin and dense electrolyte layer, 8 mol% $Y_2O_3$ stabilized-$ZrO_2$ (8YSZ) electrolyte layers were coated on the porous tubular substrate by the novel vacuum slurry dip-coating process. The effects of the slurry concentration, presintering temperature, and vacuum pressure on the thickness and the gas permeability of the coated electrolyte layers have been examined in the vacuum slurry coating process. The vacuum-coated electrolyte layers showed very low gas permeabilities and had thin thicknesses. The single cell with the vacuum-coated electrolyte layer indicated a good performance of $495\;mW/cm^2$, 0.7 V at $700^{\circ}C$. The experimental results show that the vacuum dip-coating process is an effective method to fabricate dense thin film on the porous tubular substrate.