• Title/Summary/Keyword: Dip Measurement

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PVP Hydrogel Coatings on Polypropylene Fibers using E-beam Irradiation (전자 빔을 이용한 폴리프로필렌 섬유의 PVP 하이드로젤 코팅)

  • Lee, Ji Eun;kwak, Hyo-Bin;Lee, Yong-Hyo;Kim, Kyung-Min;Lim, Jung-Hyurk
    • Journal of Adhesion and Interface
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    • v.20 no.2
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    • pp.66-70
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    • 2019
  • The surface of hydrophobic polypropylene (PP) fibers (spun-bonded fabric) was treated by an atmospheric plasma treatment method. These pre-treated hydrophilic PP fabrics were dip-coated in the aqueous poly(N-vinyl pyrrolidone) (PVP) solution. PVP layers on the surface of PP fiber were crosslinked by an irradiation of electron beam. The thickness of PVP hydrogels coated on the surface was easily controlled by changing the concentration of PVP in coating solution. The stepwise surface treatment, PVP coating, and hydrogel formation via electron beam irradiation were analyzed by the measurement of contact angle, scanning electron microscopy, and optical microscopy.

Removal of Reactive Orange 16 by the Ag/TiO2 Composite Produced from Micro-emulsion Method (마이크로에멀젼 방법에 의해 제조된 Ag/TiO2의 Reactive Orange 16 제거에 관한 연구)

  • Lee, SiJin
    • Journal of the Korean GEO-environmental Society
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    • v.20 no.11
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    • pp.5-10
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    • 2019
  • For the development of long-wavelength responding photocatalyst, Ag was applied to commercial $TiO_2$ to produce $Ag/TiO_2$ photocatalyst. Moreover, micro-emulsion method was used in order to increase the efficiency of the photocatalyst by enhancing the dispersion of Ag. Physical properties of the manufactured catalyst were analyzed by scanning electron microscopy (SEM), field emission transmission electron microscopy (FE-TEM) and diffuse reflectance spectroscopy (DRS). For the catalytic performance measurement, RO 16 (Reactive Orange 16) removal was performed with 25 ppm RO 16 under UV-A (365 nm) irradiation. In addition, ball milling and dip-coating method were used to synthesize the photocatalyst for the comparison of the outcomes of using different synthesis methods. In addition, catalytic performance was improved by varying the Ag content and surfactant content. The highest catalytic performance was shown at $Ag/TiO_2$ synthesized by micro-emulsion method with 2 wt% of Ag content, and 0.5 g of the surfactant.

Evaluation of Spatial and Temporal Variations of Water Quality in Lake Shihwa and Outer Sea by Using Water Quality Index in Korea: A Case Study of Influence of Tidal Power Plant Operation (수질평가지수를 이용한 시화호 내측 및 외측 해역의 시·공간적 수질 변화 평가: 조력발전소 가동에 따른 영향 연구)

  • Ra, Kongtae;Kim, Joung-Keun;Kim, Eun-Soo;Kim, Kyung-Tae;Lee, Jung-Moo;Kim, Sung-Keun;Kim, Eu-Yeol;Lee, Seung-Yong;Park, Eun-Ju
    • Journal of the Korean Society for Marine Environment & Energy
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    • v.16 no.2
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    • pp.102-114
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    • 2013
  • The basin of Lake Shihwa is one of highly industrialized region of Korea and a current environmental issue of study area is the operation of tidal power plant (TPP) to improve water quality. The application of water quality index (WQI) which integrates five physiochemical parameters (transparency, DO, DIN, DIP and chlorophyll-a) of water quality in Lake Shihwa and outer sea during 2011~2012 were performed not only to evaluate the spatial and temporal distribution of the water quality but also to assess the effect of water quality improvement by the operation of tidal power plant. The higher WQI values were observed in monitored sites near the industrial complexes in Lake Shihwa and the outfall of wastewater treatment plants (WWTPs) in outer sea. This indicates that the quality of seawater is influenced by diffuse non-point sources from industrial, municipal and agricultural areas in Lake Shihwa and by point sources from the effluence of municipal and industrial wastewater throughout WWTPs in outer sea. Mean WQI value decreased from 53.0 in 2011 to 42.8 in 2012 of Lake Shihwa. Water quality has improved significantly after TPP operation because enhancement of seawater exchange between Lake Shihwa and outer sea leads to improve a hypoxic condition which is primarily a problem in Lake Shihwa. Mean WQI of outer sea showed similar values between 2011 and 2012. However, the results of hierarchical cluster analysis and the deterioration of water quality in summer season indicate that the operation of tidal power plant was not improved the water quality in the upper most area of Lake Shihwa. To successfully improve overall water quality of Lake Shihwa, it is urgently necessary to manage and reduce of non-point pollution sources of the basin of Lake Shihwa.

SiOC Coating on Stainless Steel Using Polyphenylcarbosilane, and Its Anti-corrosion Properties (폴리페닐카보실란을 이용한 SiOC가 코팅된 스테인리스스틸 제조 및 이의 내부식성 특징)

  • Kim, Jong-Il;Lee, Yoon-Joo;Kim, Soo-Ryong;Kim, Young-Hee;Kim, Jung-Il;Woo, Chang-Hyn;Choi, Doo-Jin
    • Korean Journal of Materials Research
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    • v.21 no.1
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    • pp.8-14
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    • 2011
  • To improve the chemical stability of metal, the ceramic coatings on metallic materials have attracted interest from many researchers due to the chemical inertness of ceramic materials. To endure strong acids, SiOC coating on metal substrate was carried out by dip coating method using 20wt% polyphenylcarbosilane solution; SiC powder was added to the solution at 10wt% and 15wt% to improve the mechanical properties and to prevent cracks of the film. Thermal oxidation as a curing step was carried out at $200^{\circ}C$ for crosslinking of the polyphenylcarbosilane, and the coating samples were pyrolysized at $800^{\circ}C$ under argon to convert the polyphenylcarbosilane to SiOC film. The thicknesses of the SiOC coating films were $2.36{\mu}m$ and $3.16{\mu}m$. The quantities of each element were measured as $SiO_{1.07}C_{6.33}$ by EPMA, and it can be confirmed that the SiOC film from polyphenylcarbosilane was formed in a manner that was carbon rich. The hardness of the SiOC film was found to be 3.2Gpa through nanoindentor measurement. No defect including cracks appeared in the SiOC film. The weight loss of the SiOC coated stainless steel was within 2% after soaking in 10% HCl solution at $80^{\circ}C$ for one week. From these results, SiOC coating shows good potential for application to protect against severe chemical corrosion of stainless steel.

Polarization-Maintaining Photonic-Crystal-Fiber-based Polarimetric Strain Sensor with a Short Sensing Head (짧은 센서부를 가진 편광유지 광자결정 광섬유 기반 편광 간섭형 스트레인 센서)

  • Noh, Tae Kyu;Lee, Yong Wook
    • Korean Journal of Optics and Photonics
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    • v.25 no.3
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    • pp.131-136
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    • 2014
  • In this paper we have implemented a temperature-insensitive polarimetric fiber strain sensor based on a Sagnac birefringence interferometer composed of a short polarization-maintaining photonic crystal fiber (PM-PCF), a 3-dB fiber coupler, and polarization controllers. The PM-PCF used as a sensor head was 2 cm long, which is the shortest length for a sensing element compared to other polarimetric fiber strain sensors using a PM-PCF. The proposed sensor showed a strain sensitivity of ${\sim}0.87pm/{\mu}{\varepsilon}$ with a strain measurement range from 0 to $8m{\varepsilon}$. The temperature sensitivity was also investigated and measured as approximately $-12pm/^{\circ}C$, when ambient temperature changed from 30 to $100^{\circ}C$. This temperature sensitivity is about 82 times smaller than that of conventional polarization-maintaining fiber (approximately $-990pm/^{\circ}C$). In particular, from a practical perspective we have experimentally and theoretically confirmed that the wavelength selected for the indicator dip location does not make a significant difference in the strain sensitivity.

Electrical and Magnetic Properties of Magnetite Powder during a Verwey Transition (Verwey 전이와 마그네타이트의 전기적 및 자기적 특성)

  • Yoon, Sunghyun
    • New Physics: Sae Mulli
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    • v.68 no.12
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    • pp.1302-1307
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    • 2018
  • The crystallographic, electrical and magnetic behaviors of magnetite powder in the vicinity of its Verwey transition were investigated in this study. Magnetite was prepared by synthesizing a nanoparticle precursor and then annealing it at $800^{\circ}C$ for 1 h under a dynamic vacuum. Crystallographic and morphology analyses were done by using scanning electron microscope (SEM) and X-ray diffraction (XRD). The electrical and the magnetic properties were examined by using $M{\ddot{o}}ssbauer$ spectroscopy, vibrating sample magnetometer (VSM) and resistivity measurement. Both the magnetic moment and the resistivity showed discontinuous changes at the Verwey transition temperature ($T_V$). The temperature dependence of magnetic anisotropy constant showed a monotonic decrease with increasing temperature, with slight dip near $T_V$. $M{\ddot{o}}ssbauer$ spectra showed the superposition of two sextets, one from the tetrahedral (A) and the other from the octahedral (B) sites. The results revealed that identical charge states existed in the B site at temperatures both above and below $T_V$. A coordination crossover resulted in a transition from an inverse to a normal spinel at or close to $T_V$.