• Journal of Powder Materials
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• v.25 no.4
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• pp.327-330
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• 2018

This study is conducted as a preliminary research to verify the feasibility of Ti-based Oxide dispersion strengthened (ODS) alloy. Pure-Ti powder is mixed with $Y_2O_3$ powder and subsequently, mechanically alloyed at $-150^{\circ}C$. The Ti-based ODS powder is hot-isostatically pressed and subsequently hot-rolled for recrystallization. The microstructure consists of elongated grains and Y excess fine particles. The oxide particle size is larger than that of the typical Fe-based ODS steel. Tensile test shows that the tensile ductility is approximately 25%, while the strength is significantly higher than that of pure Ti. The high-temperature hardness of the Ti-ODS alloy is also significantly higher than that of pure Ti at all temperatures, while being lower than that of Ti-6Al-4V. The dimple structure is well developed, and no evidence of cleavage fracture surface is observed in the fracture surface of the tensile specimen.

• Journal of Ocean Engineering and Technology
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• v.8 no.2
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• pp.173-184
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• 1994

원자력 압력용기강의 탄소성 파괴인성값 $J_IC$를 CT형 시험편을 이용하여 검토하였으며, 평활 시험편 및 측면홈 시험편의 두께는 각각 $B_O$=25.4mm, $B_N$=20.4mm 이다. 측면홈의 깊이는 19.7% 이며, 홈의 각도는 90 .deg.로 가공하였다. 탄소성 파괴인성시험은 ASTM E813-81과 JSME S001-81의 추천방법에 따라 실시하였다. 두 추천방법으로 실험한 결과 ASTM 방법에 의한 $J_IC$값이 과대평가됨으로써 부대조건에 만족되지 못하였지만 JSME방법은 만족되었다. 측면홈 시험편은 R고선법에 의한 ductile tearing의 결정이 평활 시험편보다 용이하였으며, 이에 따른 $J_IC$값의 정확성을 배가 할 수 있었다. 또한 임계 스트레치존 폭($SZW_C$)은 측면홈에 의한 높은 3축응력이 발생되어 평활시험편보다 적게 나타났으며, 이러한 복합적인 원인에 기인하여 스트레치존법에 의한 $J_IC$평가는 R곡선법에 의한 평가보다 약간 과대평가됨을 알 수 있었다.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.25 no.3
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• pp.510-519
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• 2001

The tensile and fracture toughness tests have been conducted to investigate the degradations of mechanical properties induced mainly by neutron irradiations in Zr-2.5Nb CANDU pressure tube materials operated in Wolsung Unit-1. the tests were performed at room, 150, 200, 250, 300 $\^{C}$ for the irradiated and unirradiated specimens in hot cell. The specimens were directly machined from the tube retaining original curvature using specially designed electric discharge machine(EDM). From the tensile tests of the irradiated specimens, it was found that tensile strength was increased and total elongation was decreased compared to those of the unirradiated ones. The active voltages in the fracture toughness tests for the irradiated showed the discontinuous abrupt increases caused by crack jumping in lower temperature. In the crack resistance curves we found the stable crack growth in the unirradiated, whereas the unstable and three crack growth stages in the irradiated specimens due to the accumulated irradiation defects. The various fracture characteristic values in the irradiated are remarkably lower than those of the unirradiated. Through the fractography, we found in the irradiated that smaller dimple and shorter fissures than the unirradiated, and that the fractured surface had three regions that were flat, transition and slant/shear area. These can explain the difference in the crack growth characteristic values of the irradiated and the unirradiated ones.

• Journal of the Korean Society of Fisheries and Ocean Technology
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• v.20 no.1
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• pp.23-29
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• 1984

Nowdays, the high strength aluminum alloys are broadly used for structural purpose, but the practical strengthening method by aging treatment are not much available. So that, in this study, in order to investigate the effect of aging treatment for strengthening on the fracture characteristics of the domestic high strength Al alloy (A2024BE), the variations of the aging temperature and time were taken after solution treatment. By microstructural examination, and by SEM fractographs of the fractures, the effects of aging temperature and time were investigated, considering on the fracture behaviour. The results obtained are as follows: 1) It was confirmed by microstructural investigation that the aging temperature of $190^{\circ}C$ and the aging time of 12hours were optimal to get more sound microstructure with distribution of uniform precipitation. 2) By step aging treatment, the proper aging time for obtaining the similar microstructure without any microstructural defects could be shortened in half the normal aging time. 3)By examining the SEM fractographs of the fracture surface, it was found that, regardless of the aging treatment time and temperature, all were intergranular ductile fractures, but the aging treatment at $190^{\circ}C$ for 12 hours resulted in dimple-type-transgranular and intergranular-ductile-frature.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.20 no.4
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• pp.1123-1132
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• 1996

It has been reported that high temperature structural components represent the phenomenon of material degradation according to a long term service under high temperature and pressure. Especially, fossile power plant components using the fossil fuel and heavy oil are affected by dewpoint corrosion of $H_2SO_4$produced during a combustion. Therefore, the service materials subjected to high temperature and pressure may occur the stress corrosion cracking. The object of this paper is to investigate SCC susceptibility according to the material degradation of the high temperature structural materials in dewpoint corrosive environment-$H_2SO_4$.The obtained results are summarized as follows : 1) In case of secondary superheater tube, the fractograph of dimple is observed at the concentration of $H_2SO_4$-5%. When the concentration of $H_2SO_4$ is above 10%, the fracture mode is shifted from a transgranular fracture to an quasi-intergranular fracture according to the increment of concentration. 2) In the relationship between [$\Delta$DBTT]$_sp$ and SCC susceptibility, it is confirmed that the greater material degradation degree is, the higher SCC susceptibility is. In addition, it can be known that SP test is useful test method to evaluate SCC susceptibility for high temperature structural components. 3) When [$\Delta$DBTT]$_sp$ is above 17$17^{\circ}C$ the SCC fracture behavior is definitely observed with SCC susceptibility of above 0.4.

• Korean Journal of Materials Research
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• v.31 no.9
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• pp.519-524
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• 2021

The impact properties of two austenitic Fe-23Mn-0.4C steels with different Al contents for cryogenic applications are investigated in this study. The 4Al steel consists mostly of austenite single-phase microstructure, while the 5Al steel exhibits a two-phase microstructure of austenite and delta-ferrite with coarse and elongated grains. Charpy impact test results reveal that the 5Al steel with duplex phases of austenite and delta-ferrite exhibits a ductile-to-brittle transition behavior, while the 4Al steel with only single-phase austenite has higher absorbed energy over 100 J at -196 ℃. The SEM fractographs of Charpy impact specimens show that the 4Al steel has a ductile dimple fracture regardless of test temperature, whereas the 5Al steel fractured at -100 ℃ and -196 ℃ exhibits a mixed fracture mode of both ductile and brittle fractures. Additionally, quasi-cleavage fracture caused by crack propagation of delta-ferrite phase is found in some regions of the brittle fracture surface of the 5Al steel. Based on these results, the delta-ferrite phase hardly has a significant effect on absorbed energy at room-temperature, but it significantly deteriorates low-temperature toughness by acting as the main site of the propagation of brittle cracks at cryogenic-temperatures.

• Journal of Dental Rehabilitation and Applied Science
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• v.26 no.4
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• pp.373-388
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• 2010

Fracture causes serious problems in many instance of prosthetic failures. But it is hard to find the definite causes when fractures occur. Fractography encompasses the examination of fracture surfaces that contain features resulting from the interaction of the advancing crack with the microstructure of the material and the stress fields. All fractured specimens(implant retaining screw) retrieved from Gangneung-Wonju national university dental hospital for 3 years(from 2007 to 2009). After pretreatment of samples, the scanning electon microscope were used for surface examination and fracture analysis. In case of most of the fractured specimens, fracture took place by fatigue fracture and fractured surface represents fatigue striation. Fatigue striation indicate the progression of the crack front under cyclic loading, are characteristic of stage 2 crack growth. The site of crack initiation and stage 1 crack growth were not easily identified in any of the failure, presumably because of the complex microstructural features of the polycrystalline sample. In case of fractured by overload, dimpled or cleavage surface were observed. Using the interpretation of characteristic markings(ratchet mark, fatigue striation, dimple, cleavage et al) in fracture surfaces, failure events containing the crack origin, crack propagation, material deficiency could be understand. Using the interpretation of characteristic markings in fracture surfaces, cause and mechanism of fractures could be analyzed.

• Journal of the Korean Society of Safety
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• v.14 no.2
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• pp.3-10
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• 1999

Fatigue crack growth rates in commercial plate of high strength Al 7075-T651 were investigated for the T-L direction in air, water and sea water. In this paper the effect of cyclic load wave-form(trapezoid and triangle) on fatigue crack growth rates in air, water and sea water environments were investigated using standard LEFM testing procedures. It was founded that the fatigue crack growth behaviors were not affected by cyclic load wave-forms. In region II (stable crack growth region), the fatigue crack growth behaviors were insensitive to cyclic load wave-forms and were sensitive to environment i.e. fatigue crack growth behaviors were higher in sea water than in air for all cyclic load wave-form. The result of fractographical morphology in air, water and sea water by SEM showed obvious dimple rupture and typical striation in air, but transgranular fracture surface in water and sea water. The values m are not affected by corrosion environments but C are different values.

• Proceedings of the KSME Conference
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• 2000.04a
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• pp.67-72
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• 2000

Demand for now nondestructive evaluation are growing to detect fatigue crack growth behavior to predict long term performance of materials and structure in aggressive environments especially when they are In non-visible area. Acoustic emission technique is well suited to these problems and has drawn a keen interests because of its dynamic detection ability, extreme sensitivity and location of growing defects. In this study, we analysed acoustic emission signals obtained in fatigue and tensile test of high strength fire resistance steel for frame structure with time-frequency analysis methods. The main frequency range is different in the noise and the fatigue crack propagation. It could be classified that it were also generated by composite fracture mechanics of cleavage, dimple, inclusion separation etc.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.31 no.4
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• pp.532-539
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• 2007

The 7075-T651 Al alloy was welded by friction stir welding. Microstructure, macro behaviors and fracture type in the nugget, thermo-mechanically affected zone(TMAZ) and heat affected zone(HAZ) of the welded part were compared to base metal. The microsturctures of nugget zone were compared with tool rotation speeds and various tool transition speed. When the rotation speeds were decreased and transition speeds were increased, the hardness of nugget zone were decreased. Also, the optimal microstructure was observed at the low rotation speed of 800rpm and the high transition speed of 124mm/min. The transgranular dimple and quasi-cleavage at fractured part of nugget zone were investigated.