• Title/Summary/Keyword: Dilatometer

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Thermal Expansion Behavior of Cordierite-SiC Whisker Ceramic Composites (코디어라이트-SiC위스커 복합재료의 열팽창 특성)

  • ;Weisskopf
    • Journal of the Korean Ceramic Society
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    • v.24 no.5
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    • pp.411-416
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    • 1987
  • Thermal expansions and thermal expansion coefficients of cordierite ceramics reinforced by SiC whiskers up to 40 vol. % were investigated. The composite specimens were hot pressed at 1523K for 30 min under 28.5 MPa pressing pressure in Ar atmosphere. Thermal expansions of the hot pressed composites were measured using a differential dilatometer up to 1262 K in air. Thermal expansions and thermal expansion coefficient of the composites increased with SiC whisker content. Thermal expansion behaviors of the composites were well explained by modelling parallel slabs randomly distributed on the whisker plane as the microstructural element of the composites.

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Formulation and Identification of an Anisotropic Constitutive Model for Describing the Sintering of Stainless Steel Powder Compacts

  • Vagnon, Alexandre;Bouvardb, Didier.;Kapelskic, Georges
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.64-65
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    • 2006
  • Anisotropic constitutive equations for sintering of metal powder compacts have been formulated from a linear viscous transversely-isotropic model in which an anisotropic sintering stress has been introduced to describe free sintering densification kinetics. The identification of material parameters defined in the model, has been achieved from thermomechanical experiments performed on 316L stainless steel warm-compacted powder in a dilatometer allowing controlled compressive loading.

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A Study on Hetero Junction using NiCuZn Ferrite System for SoP (NiCuZn 페라이트계를 이용한 SoP의 이종접합에 관한연구)

  • Kim, Nam-Hyeon;Kim, Gyeong-Nam
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2012.05a
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    • pp.256-256
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    • 2012
  • SoP용 재료에 응용하기 위하여 NiCuZn 페라이트계 이용한 이종접합의 관한연구를 하였다. NiCuZn 페라이트계와 유전체의 이종접합특성은 XRD, Dilatometer, LCR meter, FE-SEM, EDS 이용하여 물리 화학적 특성을 조사하였다. NiCuZn 페라이트계는 일반적인 세라믹 제조공정을 이용하여 분말을 제조하였으며, 이종접합은 모든 시편에서 잘 진행되었으며 일부 유전체의 이온들이 페라이트 쪽으로 확산이 진행되었으며 NCZF700계는 $900^{\circ}C$ 소결 시편에서 확산이 진행되지 않은 현상이 나타났다.

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The Effects of Sample Disturbance on Undrained Properties of Yangsan Clay (양산점토의 비배수 특성에 대한 시료교란의 효과)

  • 김길수;임형덕;이우진
    • Proceedings of the Korean Geotechical Society Conference
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    • 2000.03b
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    • pp.639-646
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    • 2000
  • It is important to estimate the mechanical properties of clay since it is directly related to the design and the construction of geotechnical structures. Site exploration, which is composed of boring, sampling, in-situ, or laboratory tests, is preformed to estimate the mechanical properties. However, mechanical properties of clay measured from laboratory test may be different from in-situ properties due to disturbances occurred during sampling, transportation, storage, and trimming. In this study, the degree of disturbance according to sampling method was estimated with the test results of CK/sub o/U triaxial compression test on Yangsan clay. The soil samples were obtained by three types of sampling method, j.e., 76mm-tube sampler, 76mm-piston sampler, and block sampler. In order to evaluate the quality of samples, volumetric strain, undrained shear strength, secant Young's modulus, and pore pressure coefficient at peak measured from each sample were compared with one another. From the test results, it was observed that mechanical properties of the block and piston samples were more reliable than those of tube samples. But it was observed that the water content of piston was similar to that of tube samples at given depths while the water content of block samples was 14.3∼15.8% smaller than that of piston and tube samples. In addition to the evaluation of the quality of samples, relationship between c/sub u// σ/sub vc/'and OCR was established from the results of the CK/sub o/U triaxial compression tests, which were carried out using SHANSEP method. And also undrained shear strength was analyzed using the in-situ test data such as Cone Penetration Test(CPT), Dilatometer Test(DMT), and Field Vane Test(FVT) and was compared with that evaluated from CK/sub o/U triaxial compression test.

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A Study on Partial Molar Volume of Fluoxetine in Membrane of Holobacterium Holobium (Halobacterium Halobium의 Membrane에서 Fluoxetine의 Partial Molar Volume에 관한 연구)

  • Kim, Ki-Jun;Jeong, Hyeon-Ghak;Kim, Ju-Han;Song, Hui-jun
    • Journal of the Korean Applied Science and Technology
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    • v.35 no.1
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    • pp.157-162
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    • 2018
  • The partial molar volumes of an antidepressant in Halobacteriun Halobium and in suspensions of several lipids have been determined at $25^{\circ}C$ it using a excess volume dilatometer. The potency of general antidepressant, Fluoxetine has long been known to correlate with lipid solubility. Denaturations of the vesicle, which is a sole membrane protein in the purple membrane of Halobacteriun Halobium, were studied by absorption changes at 280 nm and fluorescence changes at 330 nm with excess volume dilatometer. The 1H NMR analysis of viscous polymer solutions by diffusion interchange is the important step by measurement. The partial molar volume and particle size of Fluoxetine in Halobacteriun Halobium were measured to be positive. An antidepressant can prevent diseases that produce a variety of cognitive and mental symptoms based on low morale and depression, resulting in poor daily performance.

Correlation of Constrained Modulus for Busan Clay using DMT (DMT를 이용한 부산점토의 변형계수 추정)

  • Hong, Sung-Jin;Cho, Yong-Soon;Jung, Sang-Jin;Lee, Woo-Jin
    • Proceedings of the Korean Geotechical Society Conference
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    • 2008.03a
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    • pp.613-618
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    • 2008
  • Because the flat dilatometer (DMT) is operated in appropriate strain level, it has been known as an adoptable in-situ tool to evaluate the compressibility of soils compare with other in-situ test tools, such as SPT and CPT. This study is concerned about prediction method of constrained modulus by DMT, and a series of DMT and consolidation tests are performed at Busan new-port, Yangsan and Noksan test sites. By comparing DMT results with lab tests, the suitability of constrained modulus correlation, which is suggested by Marchetti, is investigated in Busan clay and new correlation is suggested. In lab test result, the compression indices ($C_c$) of Busan clay are turned out to be 0.4~0.12, and the constrained moduli are found out 0.5MPa~3MPa and these are increase with depth. The predicted constrained moduli using Marchetti's correlation are turned out 0.5MPa~4MPa, and these are bigger than measured constrained moduli by lab tests. By analyzing lab test and DMT results, it is shown that the correlation coefficient ($R_M=M/E_D$) has a linear relationship with (1/$I_D$) in Busan.

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A study on dielectric characteristic of phosphate glass-ceramic for AC-PDP (AC-PDP용 인산염 결정화 유리의 유전적 특성에 관한 연구)

  • Kim, Joon-Hyung;Yon, Seog-Joo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.17 no.3
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    • pp.102-107
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    • 2007
  • Dielectric layer of phosphate glass for plasma display panel (PDP) device made by silk screen printing on soda-lime glass. For regulate thermal expansion coefficient (CTE) of between substrate glass and dielectric layer use addition of $Al_2O_3$ and $TiO_2$. The crystallization process of glass-ceramics for dielectric layer have been examined by DTA, XRD some of optical, electrical properties of the dielectric layer were evaluated by UV-spectrometer, dilatometer, impedance analyser. The principal crystalline phase was identified as zinc metaphosphate [$Zn(PO_3)_2$] and zinc pyrophosphate [$Zn_2P_2O_7$]. Reflectance and dielectric constance increased with the addition of $TiO_2$ filler, dielectric constant lower the out side reflectance unchanging of the adding of $Al_2O_3$ filler. Besides CTE was at about $62{\times}10^{-7}/^{\circ}C$.

A New Method for Dilatometer Dissipation Analysis Using an Equivalent Radius and Optimization Technique (등가반경과 최적화기법을 이용한 딜라토메터 소산시험 해석법)

  • 김영상
    • Journal of the Korean Geotechnical Society
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    • v.17 no.5
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    • pp.43-50
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    • 2001
  • 딜라토메터는 실험의 간편성, 경제성, 신속성 및 반복성 등을 바탕으로 현장에서의 지반공학적 물성추정에 보편화되고 있다. 또한 간단한 장비구성과 손쉬운 사용법에도 불구하고 다양한 지반공학적 물성들 -예로서, $K_{o}$ , OCR, $c_{u}$ , $\psi$, $c_{h}$, $k_{h}$, ${\gamma}$, M, $u_{o}$ -을 추정할 수 있으며 다양한 지반공학적 설계문제에 성공적으로 적용되어 왔다. 그러나 제안된 관계식들이 대부분 기존실험 결과들과의 비교를 통하여 얻어진 경험적 상관관계이며, 특히 압밀계수 추정에 관한 부분은 관입시 평면변형 상태의 지반변형으로 인한 관입모사의 복잡성으로 인하여 피에조콘 소산시험 해석을 위해 제안된 이론 해들에 경험적인 가정사항들을 추가하여 사용하는 반경험적 방법들과 순수한 경험적인 방법이 사용되어 왔다. 본 연구에서는 elf라토메터 관입기의 실제 평면적을 등가의 원형반경으로 고려한 등가반경을 사용하고 최적화기법을 적용함으로써, 소산시험에서 실제 관측된 간극수압($p_2$)과 딜라토메터 소산시험을 모사하여 얻어진 예측 간극수압의 차이를 최소화하는 수평압밀계수 추정법을 제안하였다. 제안된 방법을 국내 양산지역에서 수행된 딜라토메터 소산실험에 적용하였으며 추정된 수평압밀계수 값을 기존의 딜라토메터 수평압밀계수 추정법들과 불교란 시료를 이용한 일차원 실내 압밀실험으로 얻어진 수평압밀계수 값들과 비교검증 하였다. 그 결과 제안된 방법으로 기존의 방법에 비해 실내 압밀실험 결과와 일치하는 수평압밀계수 추정결과를 얻었다. 또한, 제안된 방법으로 얻어진 수평압밀계수는 전 소산도 범위에서 고르게 관측값과 일치하는 소산곡선을 예측하여, 최적화기법을 이용한 딜라토메터 소산시험 해석으로 전 소산과정을 대표하는 압밀계수의 추정이 가능할 것으로 사료된다.

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Study on the Anisotropic Size Change by Austenitizing and Tempering Heat Treatment of STD11 Tool Steel Using Dilatometry (딜라토미터를 이용한 STD11 공구강의 오스테나이징 및 템퍼링 열처리에 따른 치수 변화 이방성 연구)

  • Hong, Ki-Jung;Kang, Won-Guk;Song, Jin-Hwa;Chung, In-Sang;Lee, Kee-Ahn
    • Korean Journal of Metals and Materials
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    • v.46 no.12
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    • pp.800-808
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    • 2008
  • Heat treatment is an important step for tool manufacture, but unavoidably generates dimensional distortion. This study investigated the continuous dimensional change and the anisotropic behavior of STD11 tool steel during austenitizing and tempering heat treatment especially using quenching dilatometer. Dilatometric results represented that the dimensional change along longitudinal direction was larger than that along transverse direction. Anisotropic phase transformation strain was produced in forged STD11 tool steel during heat treatment. Anisotropic dimensional change increased with increasing austenitizing temperature. After tempering, anisotropic distortion was partially reduced. FactSage thermodynamic equilibrium phase simulation and microstructural observation (FE-SEM, TEM) showed that large ($7{\sim}80{\mu}m$) elongated $M_7C_3$ carbides could be formed along rolling direction. The resolution of elongated carbides during austenitizing was found to be related with the change of martensite transformation temperature after heat treatment. Anisotropic size change of STD11 tool steel was mainly attributed to large elongated carbides produced during rolling process. Using dilatometric and metallographic examination, the possible mechanism of the anisotropic size change was also discussed.

A Method Evaluating K0 of Granular Soil using DMT (DMT를 이용한 사질토 정지토압계수 평가방법)

  • Choi, Sung-Kun;Lee, Moon-Joo;Bae, Kyung-Doo;Lee, Woojin
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.30 no.4C
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    • pp.193-200
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    • 2010
  • This study suggests a method predicting at-rest coefficient of earth pressure ($K_0$) in order to evaluate the effect of stress history of granular soil. The method is based on the relation $K_D/K_0={\chi}(E_D/{\sigma}_m{^{\prime}})^{\delta}$, which is developed by combining two previously published relations such as $E_D/{\sigma}_m{^{\prime}}-{\psi}$ and $K_D/K_0-{\psi}$. As $K_D$ and $E_D$ are observed to be sensitive to the pre-stress, both indices are adopted for the estimation of $K_0$ value of granular soil. It is shown that the proposed $K_D/K_0-E_D/{\sigma}_m{^{\prime}}$ relation is insignificantly affected by the stress history. It is concluded from the comparative study that the proposed method, which uses only dilatometer test results to predict the $K_0$ of granular soil, provides more convenient and reliable prediction than other methods which use both CPT and DMT results.