• 제목/요약/키워드: Diffraction Phenomena

검색결과 111건 처리시간 0.023초

계면활성제를 사용하지 않는 Poly(DL-lactide-co-glycolide) 나노입자로부터의 Norfloxacin 방출과 생분해 특성 (Norfloxacin Release from Surfactant-Free Nanoparticles of Poly(DL-lactide-co-glycolide) and Biodegradation)

  • 권중근;정영일;장미경;이창형;나재운
    • 폴리머
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    • 제26권4호
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    • pp.535-542
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    • 2002
  • 투석법을 이ctide-co-glycolide) (PLGA) 나노입자를 제조하고 다양한 용매에 따른 입자 크기, 약물 함유량, 생분해도 등과 같은 물리ㆍ화학적 특성을 조사하였다. Dimethylacetamide (DMAc), dimethylformamide (DMF), dimethylsulfoxide (DMSO)로 제조된 PLGA 나노입자의 크기는 acetone으로 제조한 입자보다 적었다. 또한, 약물 함유량은 DMAc>DMF>DMSO=acetone 순서였다. PLGA 나노입자는 scanning electron microscopy (SEM)과 transmission electron microscopy (TEM)의 측정으로 구형임을 알 수 있었다. 계면활성제를 사용하지 않는 나노입자에 봉입된 norfloxacin (NFx)은 X-ray diffraction 분석을 통하여 입자 표면에 약물을 가지지 않는 좋은 약물 봉입 효율을 가짐을 알 수 있었다. 모델약물로 사용된 NFx의 방출속도는 약물 함유량뿐만 아니라 입사크기에 의해 좌우된다. 또한 PLGA 나노입자의 분해속도는 아세톤보다는 DMF를 사용하였을 때 더 빠르며 이는 PLGA 나노입자의 생분해성도 입자크기에 좌우된다는 것을 알 수 있었다.

영일만의 불규칙파 모형 (Irregular Wave Model for Youngil Bay)

  • 정신택;채장원;이동영
    • 한국해안해양공학회지
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    • 제8권2호
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    • pp.146-150
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    • 1996
  • 파랑은 해안 구조물의 안정성 및 지형 변화 분석을 위해서 가장 중요한 동역학적 요소의 하나로서, 해안공학분야에서 매우 중요하게 취급된다. 그러나 바람에 의해 발생한 파랑은 매우 불규칙한 형태를 갖고 있으며, 해저 지형과 수심이 변하게 심하게 변하는 천해역으로 전파할 때 굴절, 회절 그리고 천수 효과에 의하여 변형된다. 최근 Vincent등(1989)은 수중 타원형 천퇴에서 단순파 및 불규칙파의 변형에 대한 수리모형 실험을 보고하였다. 이들은 단순파와 불규칙파의 경우 천퇴에서의 굴ㆍ회절 복합 현상에 의한 파랑변형 형태가 판이하게 다르다는 것을 발견하였다. 수년동안 불규칙파 변형에 대한 이론 및 수치해석 연구가 계속되어, 파랑변형에 대한 이론 연구 및 수리 모형 연구는 상당히 발전되었으나, 실제 현상을 예측하기 위해서는 현장관측결과와 수치해석에 의한 해와의 비교 등이 필요하다. 본 연구에서는 여러 종류의 기기를 이용하여 영일만에서의 입사파와 변형된 파를 현장 관측하고, Chae와 Jeong(1992)의 타원형 모형을 이용하여 수중 천퇴 배후에서 불규칙파 변형에 대한 수치모형 실험을 실시하였다. 이들 2종류의 비교 결과가 잘 일치함으로써, 불규칙파 수치모형의 현장 적용성을 입증하였다.

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다양한 진주조개 패각의 색상 및 광학적 특성 분석 (Optical properties and color analysis of various pearl shells)

  • 이명진;채원식;서진교;박종완
    • 한국패류학회지
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    • 제25권3호
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    • pp.203-210
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    • 2009
  • 본 연구에서 우리는 다양한 종류의 패각을 사용하여 진주패각에서 나타나는 컬러 및 광학적 현상에 대해 비교 분석하였다. 다양한 종류의 패각의 진주층 단면 및 표면 SEM 이미지와 FFT 시뮬레이션을 수행했다. 그리고 반사율 측정을 통하여 패각에서 나타나는 광학적 현상에 대해 규명하고 패각의 광학적 현상에 의해 모패를 감별하기 위한 데이터를 구축하였다. 또한 패각의 진주층 구조에 기인한 회철현상을 바탕으로 하여 여러 각도의 분광반사율을 측정해서 보는 각도에 따라 패각의 색이 달라지는 현상에 대해 분석하였다.

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Degradation Phenomena of Wooden Pillars in the Main Hall of the Fengguo Monastery, Yixian, Liaoning, China - Scientific Investigation with XRD, IC, and FTIR Analysis -

  • Zhou, Yishan;Matsui, Toshiya;Liu, Cheng;Wang, Fei
    • 보존과학회지
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    • 제36권1호
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    • pp.15-27
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    • 2020
  • The Main Hall of the Fengguo monastery in Yixian county, Liaoning province, China, is the best preserved and largest wooden Buddhist structure, typical of the Liao dynasty style, in China. However, some degradation to the timber frame of the Main Hall has been noted, and this is causing concern in terms of the long-term preservation of the structure. In this study, wooden pillars showing the degradation phenomena of whitening, for areas in contact with the stone floor, and extensive surface damage at higher locations(mostly above 1 m) have been examined. Samples taken from wooden pillar surfaces were analyzed using X-ray powder diffraction, Fourier-transform infrared spectroscopy(FTIR), ion chromatography, and pH measurements. With respect to the whitening phenomenon, we found inorganic calcium precipitates and oxalate ions, along with higher pH values. These symptoms indicated that chemical changes were taking place in response to alkaline conditions, suggesting that alkaline mixtures with calcium content in the foundations may be responsible. Regarding the upper surface-damaged areas, no valid evidence for chemical degradation was found using FTIR analysis, while damaged areas exhibited the presence of more bat guano-related materials than which were apparent in undamaged areas. The occurrence of this surface-damaged phenomenon has therefore been attributed to physical damage caused by bat activity over long periods of time.

Electrical/Optical Characterization of PZT Thin Films Deposited through Sol-Gel Processing

  • Hwang, Hee-Soo;Kwon, Kyoeng-Woo;Choi, Jeong-Wan;Do, Woo-Ri;Hwang, Jin-Ha
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2012년도 제43회 하계 정기 학술대회 초록집
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    • pp.361-361
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    • 2012
  • PZT (Pb(Zr,Ti)O3) thin films have been used widely in the MEMS application, due to their inherent ferroelectric and piezoelectric properties. Such ferroelectricity induces much higher dielectric constants compared to those of the nonperovskite materials. In this work, the PZT thin films were deposited onto Indium-Tin-oxide (ITO) substrates through the spin-coating of PZT sols. The deposited PZT thin films were characterized in terms of the electrical and optical properties with special emphases on conductivity and optical constants. The detailed analysis techniques incorporate the dc-based current-voltage characteristics for the electrical properties, spectroscopic ellipsometry for optical characterization, atomic force microscopy for surface morphology, X-ray Photoelectron Spectroscopy for chemical bonding, Energy-dispersive X-ray Spectrometry for chemical analyses and X-ray diffraction for crystallinity. The ferroelectric phenomena were confirmed using capacitance-voltage measurements. The integrated physical/chemical features are attempted towards energy-oriented applications applicable to next-generation high-efficiency power generation systems.

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석탄회가 첨가된 점토의 마이크로파를 이용한 소결 (Microwave sintering of Fly Ash substituted body)

  • 김석범;한정환;김유택
    • 한국결정성장학회지
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    • 제8권3호
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    • pp.513-517
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    • 1998
  • 석탄회의 점노를 70:30의 비율로 혼합하여 마이크로파를 이용하여 소결하였으며, 소결에는 2.45Ghz의 일반가정용 마이크로파 오븐을 사용하였다. 시편은 $1,150^{\circ}C$에서 50분까지 10분 간격으로 소결하였다. 석탄회의 미세구조는 주사전자현미경(SEM)과 Energy dispersive spectrometry(EDS)를 이용하여 분석을 하였으며 X선회절 분석과 압축강도와 겉보기 비중을 추정하여 비교하였으며 시간이 지날수록 시편의 기공크기는 작아졌으나 압축강도와 겉보기 비중은 변화의 크기가 작았다. 로안에서의 마이크로파에 의한 시편으로의 열전달현상을 알아보기 위하여 컴퓨터를 이용한 수치해석을 행하였다.

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도심지 개발사업에 따른 환경영향평가시 소음지도 적용방안에 관한 연구 (Utilizing noise mapping in environmental impact assessment in a downtown development area)

  • 이시원;장서일;박영민;최진권
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 2005년도 춘계학술대회논문집
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    • pp.535-540
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    • 2005
  • In environmental impact assessment, noise impact assessment usually consists of three stages surveying the existing noise levels by measurements, predicting noise levels induced by construction works and predicting noise levels after the completion of project. When predicting noise level in urban area, this method does not consider acoustic phenomena like multi reflection, diffraction and absorption due to complex topographic configuration of building and terrains. For the purpose, a noise mapping tool is utilized to produce a series of noise maps, which are those for the present, for the works of construction and for the future. For accurate noise mapping, acoustical and topographic information is essential. Standard sound power levels and directivities of various construction equipments are required and scheduling of construction processes and locations of the equipments should be provided. In the case of exceeding legal limit, mitigation measures are applied to satisfy the legal limits and subsequent noise map is obtained and checked.

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교통소음의 모노럴과 바이노럴 청감 비교 연구 I: 측정 및 분석 (Comparison of Human Responses to Transportation Noise in Monaural and Binaural Hearing, Part I: Measurement and Analysis)

  • 김재환;임창우;정원태;홍지영;정완섭;이수갑
    • 한국소음진동공학회논문집
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    • 제14권12호
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    • pp.1268-1278
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    • 2004
  • Measurement of noise is not only to know the information of acoustic pressure but to assess human response to noise. To find human response to transportation noise through the laboratory study we have to measure and reproduce noise. The method of noise reproduction is largely divided into monaural and binaural techniques. But human fundamentally hears sound through both ears, referred as binaural hearing. Binaural signal is different from monaural signal because it includes more information of physical phenomena like acoustical reflection, diffraction and refraction. Especially head and pinna play an important role in perceiving change of signal origin. So, the amplitude of binaural signal is higher than that of monaural signal and spectrum of both signals is discriminated. Most of assessment and regulation of transportation noise are, however, based on monaural measurement techniques. The quantitative difference between monaural and binaural measurement is investigated in this study. Comparison on several transportation noisesshows defect of information in monaural measurements.

2차원 포토닉 크리스탈을 이용한 도파관 제작 (The manufacturing of waveguide using the photonic crystals)

  • 한송이;박형관;이송희;홍성준;;정홍배
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2008년도 Techno-Fair 및 추계학술대회 논문집 전기물성,응용부문
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    • pp.163-164
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    • 2008
  • Chalcogenide glass has been known for many photo induced phenomena and superial electron / optical specific by structure flexibility, unique electronic configuration. It is become known to the greatest specific as photonic material medium that possible to perfect controlling by continuity and photo inducing direction of amorphous chalcogenide. In our experiment, we choose the amorphous As-Ge-Se-S and corning glass as a substrate. And then we have evaporated in the ${\sim}2{\times}10^{-6}$ Torr using a E-beam evaporator, completed thin film sample that have 1um thickness of As-Ge-Se-S in $600{\AA}$, $10{\sim}5{\AA}/s$. At first, we let the change the angle between laser and sample by holography litho method and then, expect that satisfied conclusion which 2-dimension diffraction lattice manufacture and specifics by investing a He-Ne laser for 2000 seconds.

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Cr 첨가에 따른 PSS-PZT 세라믹스의 탄성 표면파 특성 (Surface Acoustic Wave Characteristics of PSS-PZT Cermaics with Cr addition)

  • 홍재일;유주현;김준한;강진규;박창엽
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1991년도 추계학술대회 논문집
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    • pp.68-72
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    • 1991
  • In this study, to improve temperature stability 0.05 Pb(Sn$\_$$\frac{1}{2}$/Sb$\_$$\frac{1}{2}$/O$_3$ - 0.35PbTiO$_3$ - 0.60PbZrO$_3$ + 0.4[wt%]MnO$_2$ piezoelctric oeramics of low dielectric constant and large mechanical quality factor were manufactured with the addition of Cr$_2$O$_3$by Hot Press method. And the SAW delay line was fabricated and the propagation characteristics of SAW was investigated, and the SAW filter was fabricated on C4 added by 0.2[wt%] Cr$_2$O$_3$and its frequency characteristics was investigated. The specimen, whose propagation characteristics of surface acoustic wave were the best, was C4 added by 0.2[wt%] Cr$_2$O$_3$, and its electromechanical coupling factor(ks$^2$) was 3.11[%] and its temperature coefficient of the center frequency (C$\_$fo/) was -21.27[ppm/$^{\circ}C$]. The 31[MHz] SAW IF filter of C4 scarcely had diffraction phenomena and its group delay time was 1.4673 ${\pm}$40[ns] in the pass band, and the insertion loss was -24.419[dB] on no impedance matching.