• 대한금속재료학회지
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• 제49권2호
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• pp.104-111
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• 2011

An ultrafine grained Mg-9Al-1Zn magnesium alloy with the mean grain size less than $1{\mu}m$ was produced by using high-ratio differential speed rolling. The processed alloy exhibited excellent superplasticity at relatively low temperatures. The micro-forming tests were carried out using a micro-forging apparatus with micro V-grooved shaped dies made of silicon and the micro-formability was evaluated by means of micro-formability index, $R_f$ ($=A_f/A_g$, $A_f$: formed and inflowed area into the V-groove, $A_g$: area of the V-groove). The $R_f$ value increased with temperature up to $280^{\circ}C$ and then decreased beyond $300^{\circ}C$. The decrease of the $R_f$ value at $300^{\circ}C$ was attributed to the accelerated grain coarsening. Increasing the micro-forging pressure increased the $R_f$ values. At a given die geometry, die filling ability decreased as the die position moved away from the die center to the end. FEM simulation predicted this behavior and a method of improving this problem was proposed.

• 지질공학
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• 제27권3호
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• pp.233-244
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• 2017

주입액의 점성도와 응력상태에 따른 균열전파 특성을 분석하기 위해 실험실 규모의 수압파쇄시험을 실시하였다. 시험에 사용된 시료는 시멘트 몰탈을 사용하여 제작되었으며, 각 변의 길이가 20 cm인 정육면체 형태이다. 제작된 시료는 최대강도를 갖기 위해 수중에서 약 1달간 양생과정을 거쳤다. 독립적인 가압시스템을 가지고 있는 진삼축압축장치로 시료에 압력을 가하여, 실제의 지반에서 작용하는 원위치응력 상태를 재현하였다. 시추 환경 재현을 위해 시료에 소형 시추공을 천공한 후, 일정한 주입속도로 수압파쇄시험을 실시하였다. 수압파쇄시험 과정에서 시추공에 주입된 유체의 압력을 실시간으로 측정하였으며, 동시에 미소파괴음(AE) 신호를 측정하였다. 수압파쇄시험의 모든 과정이 끝난 후 생성된 균열의 형태를 육안으로 관찰하였다. 일차파쇄압력은 주입액의 점성도 증가에 따라 지수형태를 보이며 증가하였다. 수압파쇄시험으로 인해 생성된 균열의 형태는 최대주응력과 최소주응력의 차이인 편차응력의 크기에 따라 서로 다른 양상을 보였다. 낮은 편차응력의 조건에서는 단일의 균열이 아닌 다중 균열이 생성되거나, 균열 성장과정에서 방향이 휘어지는 경향을 보였고, 이에 반해 높은 편차응력의 조건에서 생성된 균열은 단일 면상의 균열이 발생하였다. AE 분석에서도 편차응력이 클수록 미세균열이 단일 면상으로 집중되어 발생되는 경향을 보였다. 이러한 연구결과는 수압파쇄 방법을 이용한 암반파쇄에서 편차응력이 클 때보다 작을 때 더 복잡한 균열이 발생된다는 것을 보여준다. 따라서 셰일가스를 개발할 때 생산량을 높이기 위해서는 복잡한 균열을 발생시킬 수 있는 편차응력이 작은 조건에서 수압파쇄가 적용되는 것이 효과적일 것으로 판단된다.

• 대한기계학회논문집
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• 제1권2호
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• pp.73-81
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• 1977

It is well known fact that there is a theoretical analogous relation ship in terms of differential equation between the stress distribution of a bar under pure torsional moment and the deflection of a membrane subjected to a uniform pressure. This relationship has been applied to the experimental determination of torsional stresses with troublesome and elaborative measuring procedure since Griffith's invention of the soap-film apparatus. In this paper, the soap-film was replaced by a highly polished steel plate and whole visualable deflectional contour-line-map was able to obtain by using Michelson Interferometer with Ne-He Gas Laser lignt source enabling to determine the stress distribution in the vicnity of the symmetrical inner-boundary in a section. Experimental results were satisfactory and the margin of error in the measurement was lower than 1%.

• 한국안전학회지
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• 제13권2호
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• pp.88-95
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• 1998

Five parts of the automotive interior materials were sampled to determine their combustion characteristics. Oxygen Indexer, Smoke chamber, Differential Scanning Calorimeter(DSC) were used as the analysis apparatus. All LOI values of samples appear less than 21. The combustion phenomena of the interior materials primarily depends on properties of each layer material. The amount of generated smoke are reached the maximum value within 30 - 90sec after ignition. The experimental results of combustion characteristics and DSC of H/Line also indicated that the layer of foam was melt first and it caused the propagation of flame through the sample. The combustion characteristics of multi-layer materials primarily depends on thermal characteristics of single layer material.

• 한국인쇄학회지
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• 제14권1호
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• pp.115-131
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• 1996

The PVT(pressure-volume-temperature) relation of main-chain dimer liquid crystals having structures such as $\alpha$,$\omega$-bis[(4,4`-cyanobiphenyl) oxy] alkane(CBA-n with=9, 10) were studied. these dimer liquid crystals are known to form an enantiotropic nematic mesophase. In this work, we have determined the volume change as a function of temperature and pressure by using a GNOMIX PVT apparatus. In the V-Tcurves obtaind from isobaris mearements on various pressures, volume changes were observed at the nematic-isotropiz and nematic-crystal phase transitions. The volume changes at the transition exhibit slight odd-even effect with respect to the number of methylene unit n. The values of the (S)v obtained at the NI transition for CBA-9 and -10 were 6.9 and 12.6J/mol k. The valuesof (S)v for the CN transition were estimated on the basis of DSC(differential scanning calorimetry) data: 58.8(CBA-9) and 65.3J/mol k (CBA-10). For both transition, it was found that the correction about the volume change is significant, ranging from 40% to 60% of the total transition entropy observed under constant pressure.

• Journal of Advanced Marine Engineering and Technology
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• 제30권3호
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• pp.382-388
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• 2006

This study experimented to understand the effect of transporting ice slurry through in pipe with valve. And at this experiment it used ethylene glycol-water solution and a concentration is 30wt%. The experimental apparatus was constructed of ice slurry generation tank, turbo flow meter, manometers for differential pressure measuring, PIV system for flow pattern measuring. illumination and along a horizontal circular tube with valve as test section. The experiments were carried out under various conditions, with velocity of fluid at the entry ranging from 0.5 to 1.5 m/s and concentration of IPF is 30%. Also valve open rate is 50%, 75%, 100%.

• Journal of Magnetics
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• 제6권1호
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• pp.27-30
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• 2001

We present a new procedure to evaluate the residual life of 1Cr-1Mo-0.25V steel from reversible magnetic permeability. The method is based on the existence of first harmonics in the differential magnetization around the coercive force. The apparatus is based on the detection of the voltage induced in a coil using a lock-in amplifier tuned to the frequency of the exciting coil. Results obtained for the first harmonics and Vickers hardness on aged samples show that the peak interval of reversible permeability and Vickers hardness decrease as aging time increases. The correlation between Vickers hardness and the peak interval of the reversible permeability may be used to evaluate the residual life of 1Cr-lMo-0.25V steel, nondestructively.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2000년도 하계학술대회 논문집 C
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• pp.1593-1595
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• 2000

We present a new procedure to evaluate the degradation in a lCr-lMo-0.25V steel. The method is based on the existence of the peak of reversible permeability in the differential magnetization around the coercive field strength. The apparatus is based on the detection of the voltage induced in a surface type coil using a lock-in amplifier tuned to a frequency to the exciting one. Results obtained the reversible permeability and Vickers hardness on the annealed samples show the peak interval of reversible permeability and Vickers hardness decreased as ageing time increased. The correlation between Vickers hardness and the peak interval of reversible permeability could well be evaluated non destructively.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.442-443
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• 2006

Vacuum carbonization of nanometer tungsten powder was investigated in a simple designed apparatus. An X-Y recorder was used to plot differential thermal analysis (DTA) curves to determine starting temperature of carbonization of four samples with different specific surface area. The product was detected by X-ray Diffraction (XRD) and small angle X-ray scattering (SAXS). The results show that finer tungsten powder has lower starting temperature of carbonization. Tungsten powder, which BET surface area is $32.97m^2/g$, is completely carbonized to tungsten carbide at $1050^{\circ}C$, although the starting temperature is $865^{\circ}C$. Particle grows sharply before carbonization.

• 한국화재소방학회:학술대회논문집
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• 한국화재소방학회 1997년도 International Symposium on Fire Science and Technology
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• pp.211-218
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• 1997

Five parts of vehicle upholsteries were sampled to determine its combustion characteristics. Oxygen Indexer, Smoke chamber, Differential Scanning Calorimetry(DSC) are applied as the analysis apparatus. All LOI values of samples appear less than 21. The combustion phenomena of vehicle upholster primarily depends on properties of each layer material. The amount of smoke generated is the experiment reached the maximum value within 30-90sec after ignition. The experimental results of combustion characteristics and DSC of H/Line also indicated that the layer of foam was melt first and it caused the propagation of flame through the sample. The combustion characteristics of multi layer materials primarily depend on thermal characteristic of single layer material.