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경면 연삭기 베드를 위한 레진 콘크리트에 관한 연구

  • 김현석;김기수;이대길
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 1993년도 춘계학술대회 논문집
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    • pp.108-113
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    • 1993
  • The material for the machine tool structure should have high static stiffiness and damping in its property to improve both the static and dynamic performances. The static stiffness of a machine tool can be inceased by using either higher modulus material in the structure of a machine tool. However, the machine tool structrue with high stiffness but low damping is vulnerable to vibration at the resonance frequencies of the structure . For the high precision and highsped machine tool structure, therefore, the high damping capacity is most important in order to suppress vibration. The damping of a machine tool can not be increased by increasing the static stiffness. The best way to increase the damping capacity of the machine tool structure is to use a composite material which is composed of on material with high stiffness with low damping and another material with low stiffness with high damping. Therefore, in this paper, the bed of the ultra high precision grinding machine for mirror surface machining of brittle materials such as ceramics and composite materials was designed and manufactured with the epoxy concrete material. The epoxy concrete material was prepared by mixing epoxy resin with different size sands and gravels. The modulus, compressive strength, coefficient of thermal expansion, specific heat, and damping factor were measured by varying the compaction ratio, sizes and contents of the ingredients to assess the effect of the processing parameters on the mechanical properties of the material. Based of the measured properties, the prototype epoxy resin concrete bed for the mirror surface CNC grinding machine was designed and manufactured.

Influence of sine material gradients on delamination in multilayered beams

  • Rizov, Victor I.
    • Coupled systems mechanics
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    • 제8권1호
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    • pp.1-17
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    • 2019
  • The present paper deals with delamination fracture analyses of the multilayered functionally graded non-linear elastic Symmetric Split Beam (SSB) configurations. The material is functionally graded in both width and height directions in each layer. It is assumed that the material properties are distributed non-symmetrically with respect to the centroidal axes of the beam cross-section. Sine laws are used to describe the continuous variation of the material properties in the cross-sections of the layers. The delamination fracture is analyzed in terms of the strain energy release rate by considering the balance of the energy. A comparison with the J-integral is performed for verification. The solution derived is used for parametric analyses of the delamination fracture behavior of the multilayered functionally graded SSB in order to evaluate the effects of the sine gradients of the three material properties in the width and height directions of the layers and the location of the crack along the beam width on the strain energy release rate. The solution obtained is valid for two-dimensional functionally graded non-linear elastic SSB configurations which are made of an arbitrary number of lengthwise vertical layers. A delamination crack is located arbitrary between layers. Thus, the two crack arms have different widths. Besides, the layers have individual widths and material properties.

$(La,\;Sr)MnO_{3+{\delta}$ 합성에 있어서 출발물질에 따른 양극특성 (Cathode Characteristics in the Synthesis of $(La,\;Sr)MnO_{3+{\delta}$ of Precursor)

  • 이미재;김세기;지미정;최병현;박상선
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2006년도 추계학술대회
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    • pp.360-363
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    • 2006
  • We synthesized $(La,\;Sr)MnO_{3+{\delta}$ as a cathode for SOFC by glycine nitrate process(GNP) and knew the different properties of $(La_{1-x}Sr_x)MnO_3$ by using nitrate solution and oxide solution as starting material. In case of using nitrate solution as a starting material, main crystal phase peak of $LaMnO_3$ increased as Sr content added up and a peak of $Sr_2MnO_4\;and\;La_2O_3$ was showed as a secondary phase. We added Mn excess to control a crystal phase. In this case, the electrical conductivity had a high value 210.3S/cm at $700^{\circ}C$ On the other side, when we used oxide solution as a starting material, we found main crystal phase of $LnMnO_3$ to increase as Sr content added up and a peak of $La_2O_3$ as a secondary phase. Similary, we added Mn excess to control a crystal phase in this case. We knew $(La,\;Sr)MnO_3$ powder to sinter well and the electrical conductivity of the sintered body at $1200^{\circ}C$ for 4hrs was 152.7s/cm at $700^{\circ}C$. The sintered $(La,\;Sr)MnO_3$ powder at $1000^{\circ}C$ for 4hrs got the deoxidization peak, depending on the temperature md in case of using nitrate solution as a start ing material the deoxidization peak was showed at $450^{\circ}C$ which is lower than used a oxide solution as a starting material. As a result, when $(La,\;Sr)MnO_3$ powder was synthesized to add Mn excess and to use nitrate solution as a starting material, we found it to have the higher deoxidization property and considered it as a cathode for m properly. And we found it to have different electrical conduct ivity the synthesized $(La,\;Sr)MnO_3$ powder by using different start ing materials like nitrate solution and oxide solution which influence a sintering density and crystal phase.

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GNP법에 의해 합성한 (La1-xSrx)Mn1+yO3−δ 분말의 출발물질에 따른 특성 (Effect of Starting Materials on the Characteristics of (La1-xSrx)Mn1+yO3−δ Powder Synthesized by GNP)

  • 이미재;김세기;지미정;최병현;박상선;이경희
    • 한국세라믹학회지
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    • 제44권1호
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    • pp.52-57
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    • 2007
  • We synthesized $(La_{1-x}Sr_x)MnO_3$ as a cathode for SOFC by glycine nitrate process (GNP) and knew the different properties of $(La_{1-x}Sr_x)MnO_3$ by using nitrate solution and oxide solution as a starting material. In case of using nitrate solution as a starting material, main crystal phase peak of $LaMnO_3$ increased as Sr content added up and a peak of $Sr_2MnO_4\;and\;La_2O_3$ was showed as a secondary phase. We added Mn excess to control a crystal phase. In this case, the electrical conductivity had a high value 210.3 S/cm at $700^{\circ}C$. On the other side, when we used oxide solution as a starting material, we found main crystal phase of $LaMnO_3$ to increase as Sr content added up and a peak of $La_2O_3$ as a secondary phase. Similary, we added Mn excess to control a crystal phase in this case. We knew $(La,Sr)MnO_3$ powder to sinter well and the electrical conductivity of the sintered body at $1200^{\circ}C$ for 4 h was 152.7 S/cm at $700^{\circ}C$. The sintered $(La,Sr)MnO_3$ powder at $1000^{\circ}C$ for 4 h got the deoxidization peak, depending on the temperature and in case of using nitrate solution as a starting material, the deoxidization peak was showed at $450^{\circ}C$ which is lower than used a oxide solution as a starting material. As a result, when $(La,Sr)MnO_3$ powder was synthesized to add Mn excess and to use nitrate solution as a starting material, we found it to have the higher deoxidization property and considered it as a cathode for SOFC properly. And we found it to have different electrical conductivity the synthesized $(La,Sr)MnO_3$ powder by using different starting materials like nitrate solution and oxide solution which influence a sintering density and crystal phase.

Influence of wound closure on volume stability with the application of different GBR materials: an in vitro cone-beam computed tomographic study

  • Naenni, Nadja;Berner, Tanja;Waller, Tobias;Huesler, Juerg;Hammerle, Christoph Hans Franz;Thoma, Daniel Stefan
    • Journal of Periodontal and Implant Science
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    • 제49권1호
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    • pp.14-24
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    • 2019
  • Purpose: To assess the influence of using different combinations of guided bone regeneration (GBR) materials on volume changes after wound closure at peri-implant dehiscence defects. Methods: In 5 pig mandibles, standardized bone defects were created and implants were centrally placed. The defects were augmented using different combinations of GBR materials: xenogeneic granulate and collagen membrane (group 1, n=10), xenogeneic granulate and alloplastic membrane (group 2, n=10), alloplastic granulates and alloplastic membrane (group 3, n=10). The horizontal thickness was assessed using cone-beam computed tomography before and after suturing. Measurements were performed at the implant shoulder (HT0) and at 1 mm (HT1) and 2mm (HT2) below. The data were statistically analysed using the Wilcoxon signed-rank test to evaluate within-group differences. Bonferroni correction was applied when calculating statistical significance between the groups. Results: The mean horizontal thickness before suturing was $2.55{\pm}0.53mm$ (group 1), $1.94{\pm}0.56mm$ (group 2), and $2.49{\pm}0.73mm$ (group 3). Post-suturing, the values were $1.47{\pm}0.31mm$ (group 1), $1.77{\pm}0.27mm$ (group 2), and $2.00{\pm}0.48mm$ (group 3). All groups demonstrated a loss of horizontal dimension. Intragroup changes exhibited significant differences in group 1 (P<0.001) and group 3 (P<0.01). Intergroup comparisons revealed statistically significant differences of the relative changes between groups 1 and 2 (P=0.033) and groups 1 and 3 (P=0.015). Conclusions: Volume change after wound closure was minimized by using an alloplastic membrane. The stability of the augmented horizontal thickness was most ensured by using this type of membrane irrespective of the bone substitute material used for membrane support.

Influence of Heating Rate and Temperature on Carbon Structure and Porosity of Activated Carbon Spheres from Resole-type Phenolic Beads

  • Singh, Arjun;Lal, Darshan
    • Carbon letters
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    • 제10권3호
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    • pp.181-189
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    • 2009
  • Activated carbon spheres (ACS) were prepared at different heating rates by carbonization of the resole-type phenolic beads (PB) at $950^{\circ}C$ in $N_2$ atmosphere followed by activation of the resultant char at different temperatures for 5 h in $CO_2$ atmosphere. Influence of heating rate on porosity and temperature on carbon structure and porosity of ACS were investigated. Effect of heating rate and temperature on porosity of ACS was also studied from adsorption isotherms of nitrogen at 77 K using BET method. The results revealed that ACS have exhibited a BET surface area and pore volume greater than $2260\;m^2/g$ and $1.63\;cm^3/g$ respectively. The structural characteristics variation of ACS with different temperature was studied using Raman spectroscopy. The results exhibited that amount of disorganized carbon affects both the pore structure and adsorption properties of ACS. ACS were also evaluated for structural information using Fourier Transform Infrared (FTIR) Spectroscopy. ACS were evaluated for chemical composition using CHNS analysis. The ACS prepared different temperatures became more carbonaceous material compared to carbonized material. ACS have possessed well-developed pores structure which were verified by Scanning Electron Microscopy (SEM). SEM micrographs also exhibited that ACS have possessed well-developed micro- and meso-pores structure and the pore size of ACS increased with increasing activation temperature.

$TiO_2$의 소결조건의 변화가 염료감응 태양전지의 효율에 미치는 영향 (Influence on DSSC efficiency with different sintering conditions of $TiO_2$)

  • 정웅재;박미주;윤덕용;이성욱;김형진;홍병유
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 추계학술대회 논문집 Vol.21
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    • pp.433-434
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    • 2008
  • Until now, many studies have been carried out on $TiO_2$ electrode, counter electrode, sensitizer and electrolyte to improve dye-sensitized solar cell(DSSC)'s performance. It was known that surface area of the $TiO_2$ are of paramount importance in determining the cell efficiency. In this experiment, $TiO_2$ working electrodes were sintered at four different temperatures (400, 450, 500 and $550^{\circ}C$) for 55 minutes in ambient atmosphere. Also these electrodes were sintered at four different times (40, 55, 70, 85minutes) in temperature where shows the highest efficiency. I-V characteristics of DSSC made up of different working electrodes were studied using solar simulator.

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카본블랙에 의한 천연고무 물성치와 피로수명 변화에 대한 실험적 연구 (An Experimental Study on the Change of the Material Properties and the Fatigue Life of Natural Rubber due to Carbon Black)

  • 김재훈;김영학;정현용
    • 대한기계학회논문집A
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    • 제25권11호
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    • pp.1887-1894
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    • 2001
  • The effects of carbon black on the material properties and the fatigue life of the carbon-black filled natural rubbers were investigated. Different kinds of carbon blacks resulted in different fatigue lives, hysteresis, and critical J-values. It was noticed that the hysteresis was inversely proportional to the difference between DBPA and CTAB, and the critical J-value was almost the same regardless of the length of a precrack. In addition, different kinds of carbon blacks resulted in different fracture morphologies, and micro-scale and macro-scale roughnesses. The critical J-value was proportional to the micro-scale roughness. and it seemed relate to the size distribution of carbon black particles. By reviewing all the experimental data. it was finally noticed that the logarithmic value of the fatigue life could be linearly expressed by a multiplication of the critical J-value and the logarithmic value of the hysteresis.

ATH 의 입도에 따른 실리콘 고무의 특성 (Properties of Silicone Rubber According to the Addition of Different Particle Size of ATH)

  • 박효열;강동필;안명상;김대환;이후범;오세호
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2002년도 추계학술대회 논문집 Vol.15
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    • pp.216-219
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    • 2002
  • Much quantity of anti-tracking agent, ATH is added to the silicone rubber for the protection of silicone rubber against surface discharge. Hydrophobicity recovery properties of silicone rubber could be different by the content, surface treatment state and particle size of ATH. Because hydrophobicity of silicone rubber is depend much on the surface state of ATH. In this paper, the properties of silicone rubber is investigated according to the addition of different particle size of ATH to the silicone rubber. Hydrophobicity recovery properties and arc resistance of silicone rubber were investigated according to the addition of different particle size of ATH. Hydrophobicity recovery properties of silicone rubber were evaluated by the measurement of contact angle.

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슬러리와 패드변화에 따른 텅스텐 플러그 CMP 공정의 최적화 (An Optimization of Tungsten Plug Chemical Mechanical Polishing(CMP) using the Different Sets of Slurry and Pad)

  • 김상용;서용진;이우선;이강현;장의구
    • 한국전기전자재료학회논문지
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    • 제13권7호
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    • pp.568-574
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    • 2000
  • We have been optimized tungsten(W) plug CMP(chemical mechanical polishing) characteristics using two different kinds of component of slurry and two different kinds of pad which have different hardness. The comparison of oxide film roughness on around W plug after polishing has been carried out. And W plug recess for consumable sets and dishing effect at dense area according to the rate of over-polishing has been investigated. Also the analysis of residue on surface after cleaning have been performed. As a experimental result we have concluded that the consumable set of slurry A and hard pad was good for W plug CMP process. After decreasing the rate of chemical reaction of silica slurry and adding two step buffering we could reduce the expanding of W plug void however we are still recognizing to need a more development for those kinds of CMP consumables.

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