• 제목/요약/키워드: Diamond-like carbon coating

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Estimation of Nanomechanical Properties of Nanosurfaces Using Phase Contrast Imaging in Atomic Force Microscopy (원자력현미경의 위상차영상을 이용한 나노표면의 미소기계적 특성 평가)

  • Ahn, Hyo-Sok
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.16 no.5
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    • pp.115-121
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    • 2007
  • Phase contrast imaging in atomic force microscopy showed a promise as an effective tool for better understanding of micromechanical properties of surfaces at nano scale. A qualitative estimation model for phase contrast images obtained with a tapping mode AFM was developed. This investigation demonstrated the high efficiency of combined analysis of topography and phase contrast images for characterizing nanosurfaces. Phase contrast images allowed estimation of relative stiffness(elastic modulus) of the sample surface. The phase contrast images revealed a significant inhomogeneity of the nano scale worn surfaces. Phase contrast images are also capable of revealing the formation of tribofilms.

Analysis of Nano-contact Between Nano-asperities Using Atomic Force Microscopy (나노스케일 표면돌기 간의 미세접촉에 대한 해석)

  • Ahn, Hyo-Sok;Jang, Dong-Young
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.18 no.4
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    • pp.369-374
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    • 2009
  • In micro/nano-scale contacts in MEMS and NEMS, capillary and van der Waals forces generated around contacting micro-asperities significantly influence the performance of concerning device as they are closely related to adhesion and stiction of interacting surfaces. In this regard, it is of prime importance to accurately estimate the magnitude of surface forces so that an optimal solution for reducing friction and adhesion of micro/nano-surfaces may be obtained We introduced an effective method to calculate these surface forces based on topography information obtained from an atomic force microscope. This method was used to calculate surface forces generated in the contact interface formed between diamond-like carbon coating and $Si_3N_4$ ball. This method is shown to effectively demonstrate the influence of capillary force in the contact area, especially in humid atmosphere.

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Tribological Properties of DLC film on Modified Surface by TiC Plasma Immersion Ion Implantation and Deposition (TiC 이온 주입 층에 증착된 DLC 박막의 트라이볼로지적 특성)

  • Yi, Jin-Woo;Kim, Jong-Kuk;Kim, Seock-Sam
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.956-960
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    • 2004
  • Effects of ion implantation and deposition on the tribological properties of DLC film as a function of implanted energies and process times were investigated. TiC ions were implanted and deposited on the Si-wafer substrates followed by DLC coating using ion beam deposition method. In order to study tribological properties such as friction coefficient and behavior of DLC film on the modified surface as a function of implanted energies and process times, we used a ball-on-disc type apparatus in the atmospheric environment. From results of wear test, as the implanted energy was increased, the friction coefficient was more stable below 0.1.

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Crack Face Friction Effects on Mode II Stress Intensities for a Surface-Cracked Coating In Two-Dimensional Rolling $Contact^{\copyright}$ (구름접촉 하중시 코팅 표면에 발생한 균열면의 마찰을 고려한 모드II 전파거동에 관한 연구)

  • Moon Byung-Young;Kim Byeong Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.22 no.6 s.171
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    • pp.159-167
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    • 2005
  • This work focuses on the effects of crack free friction on Mode II stress intensity factors, $K_{II}$, for a vertical surface crack in a two-dimensional finite element model of TiN/steel subject to rolling contact. Results indicate that maximum $K_{II}$ values, which occur when the load is adjacent to the crack, may be significantly reduced in the presence of crack face friction. The reduction is more significant for thick coatings than for thin. Crack extension and increased layer thickness result in increased $K_{II}$ values. The effect of crack face friction on compressive $K_I$ values appears negligible. Comparative results are presented for $MoS_2/steel$ and diamond-like carbon(DLC)/Ti systems.

Improved Adhesion of DLC Films by using a Nitriding Layer on AISI H13 Substrate

  • Park, Min-Seok;Kim, Dae-Young;Shin, Chang-Seouk;Kim, Wang Ryeol
    • Journal of the Korean institute of surface engineering
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    • v.54 no.6
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    • pp.307-314
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    • 2021
  • Diamond-like carbon (DLC) is difficult to achieve sufficient adhesion because of weak bonding between DLC film and the substrate. The purpose of this study is to improve the adhesion between substrate and DLC film. DLC film was deposited on AISI H13 using linear ion source. To improve adhesion, the substrate was treated by dual post plasma nitriding. In order to define the mechanism of the improvement in adhesive strength, the gradient layer between substrate and DLC film was analyzed by Glow Discharge Spectrometer (GDS) and Scanning Electron Microscope (SEM). The microstructure of the DLC film was analyzed using a micro Raman spectrometer. Mechanical properties were measured by nano-indentation, micro vickers hardness tester and tribology tester. The characteristic of adhesion was observed by scratch test. The adhesion of the DLC film was enhanced by active screen plasma nitriding layer.

Mechanical Stability of TiN and DLC Coated Instrument of Pedicle Screw System (TiN 및 DLC 코팅된 척추경나사못시스템 수술기구의 기계적 안정성 분석)

  • Kang, Kwan-Su;Jung, Tae-Gon;Yang, Jae-Woong;Woo, Su-Heon;Park, Tea-Hyun;Jeong, Yong-Hoon
    • Journal of the Korean institute of surface engineering
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    • v.52 no.3
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    • pp.163-170
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    • 2019
  • Durability of instrument is one of the most important factor to ensure accurate treatment and decrease failure for the orthopedic surgical operation. Normally, a set-screw driver tip has been processed with hard coating for their higher durability and wear resistance. And several surface modification methods were obtained such as titanium nitride (TiN) coating, diamond like carbon coating, other nitriding, and etc. In this study, we have surface modified on set-screw driver tip with TiN and DLC, investigated whether the TiN and DLC coatings affect the mechanical properties and durability of the set-screw driver tip in the pedicle screw system. The surface morphologies were observed with scanning-electron microscopy (SEM), and the static/dynamic torsional properties were investigated with universal testing machine based on ASTM F543. Coating thickness of each coatings were commonly around $1^{\circ}C$. Static torsional stiffness, and ultimate torque values for DLC and TiN coated samples were significantly higher than those of non-coated sample by the pared T-test. Surface morphology of after the dynamic torsional test was more clean with less scratch or friction traces from DLC coating than that of TiN coating and non-coated sample.

Simulation of the Initial Wear and Lubrication Performance of Marine Engine Components (선박엔진 부품의 성능 향상을 위한 초기 마모 및 윤활 해석 연구)

  • Cha, Su-Bin;Lee, Hyang;Chung, Koo-Hyun
    • Tribology and Lubricants
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    • v.38 no.6
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    • pp.227-234
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    • 2022
  • Recently, the demand for improving energy efficiency has rapidly increased because of the growing concerns over environmental issues. In this work, the tribo-test and simulation for the initial wear and lubrication performance were performed for the piston pin in the small end system of the connecting rod of a marine engine, to obtain useful data for improving the efficiency of marine engine systems. In addition, a diamond-like carbon (DLC) coating was applied to the piston pin to explore feasibility of eliminating the bush used in the system. The initial wear and lubrication characteristics between the uncoated piston pin and bush were compared with that between the DLC-coated piston pin and connecting rod in the tribo-test. The simulation for the wear and lubrication performance according to the wear progression was conducted based on the data obtained from the test. The wear characteristics were quantitatively assessed by the wear depth and wear volume, and the lubrication performance was characterized with the change of pressure and minimum oil film thickness with respect to the crank angle. It was found that the DLC-coated piston pin may provide better initial wear characteristics and lubrication performance. The results of this work may provide fundamental information for marine engines with improved efficiency.

Wear Property of SACM645 Material with DLC Coating (DLC 코팅된 SACM645 소재의 마모 특성)

  • Kim, Nam-Soek;Nam, Ki-Woo;Park, Jong-Nam;Ahn, Seok-Hwan;Kim, Hyun-Soo
    • Journal of Ocean Engineering and Technology
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    • v.24 no.6
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    • pp.76-80
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    • 2010
  • Oil hydraulic piston pumps are being extensively used around the world, because of their simple design, light weight, effective cost, etc. An oil hydraulic pump is likely to have the serious problems of high leakage, friction, and low energy efficiency after a long period of use. In an oil hydraulic piston pump, the clearance between the valve block and piston plays an important role for volumetric and overall efficiency. In this study, the wear property of the SACM645 material with DLC coating used for a hydraulic piston pump was determined by experimentation with variable heat treatment. To investigate the effect according to the piston surface condition, five different types of specimens were prepared. The maximum tensile strengths of the QT and QT Nitration specimens had similar values of about 800 MPa, but the strains indicated a big difference. In a wear test, the wear characteristic of the DLC coating specimen was shown to be excellent. The QT, QT + IH, QT + Nitration, and matirx specimen showed similar wear characteristics. In the case of a dry condition without oil, the DLC coating specimen had good wear resistance, with no wear shown.

Friction and Wear Characteristics of Magneto-rheological Fluid Depend on Surface Coated by DLC and PTFE (DLC와 PTFE표면코팅에 따른 자기유변유체의 마찰 마모 특성)

  • Zhang, Peng;Lee, Kwang-Hee;Lee, Chul-Hee;Choi, JongMyong
    • Tribology and Lubricants
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    • v.31 no.2
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    • pp.62-68
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    • 2015
  • A magnetorheological (MR) fluid is a smart material whose rheological behavior can be controlled by varying the parameters of the applied magnetic field. Because the damping force and shear force of an MR fluid can be controlled using a magnetic field, it is widely employed in many industrial applications, such as in vehicle vibration control, powertrains, high-precision grinding processes, valves, and seals. However, the characteristics of friction caused by iron particles inside the MR fluid need to be understood and improved so that it can be used in practical applications. Surface process technologies such as polytetrafluoroethylene (PTFE) coatings and diamond-like carbon (DLC) coatings are widely used to improve the surface friction properties. This study examines the friction characteristics of an MR fluid with different surface process technologies such as PTFE coatings and DLC coatings, by using a reciprocating friction tester. The coefficients of friction are in the following descending order: MR fluid without any coating, MR fluid with a DLC coating, and MR fluid with a PTFE coating. Scanning electron microscopy is used to observe the worn surfaces before and after the experiment. In addition, energy dispersive X-ray spectroscopy is used to analyze the chemical composition of the worn surface. Through a comparison of the results, the friction characteristics of the MR fluid based on the different coating technologies are analyzed.