• Title/Summary/Keyword: Diamond like carbon

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Effect of Si Interlayer on the Roughness of Diamond-like Carbon Films (다이아몬드상 탄소박막의 조도에 미치는 Si Interlayer의 영향)

  • Jeong, Jae-In;Yang, Ji-Hun;Park, Yeong-Hui;Lee, Gyeong-Hwang
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2007.11a
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    • pp.37-38
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    • 2007
  • Si Interlayer의 두께가 DLC (Diamond-like Carbon) 박막의 조도 및 미세 조직에 미치는 영향을 AFM 및 TEM을 이용하여 조사하였다. DLC 박막은 이온빔 소스를 이용하여 벤젠가스를 플라즈마 분해하여 기판에 증착하였고 기판에는 2kV의 펄스전원을 인가하였다. 기판은 Si Wafer와 초경을 이용하였으며 초경의 경우 평균조도가 20nm이하가 되도록 연마하여 사용하였다. Si Interlayer는 스퍼터링 소스를 이용하여 제조하였고 증착 시간에 따라 두께를 달리하여 약 90nm까지 변화시켰다. Si Interlayer만 증착하였을 경우 조도에 큰 차이를 나타내었으나 Interlayer 위에 DLC가 코팅되면 조도가 감소하여 Si 두께와는 상관이 없는 것으로 나타났다. 본 연구에서는 Interlayer에 두께에 따른 조도변화와 함께 피막의 조직 및 경도 변화 등에 대해 고찰하였다.

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Study of coating process for mass production of non-hydrogen Diamond like carbon films using filtered vacuum arc method (자장 여과 진공 아크법으로 증착되는 수소 없는 DLC 막의 양산을 위한 코팅 공정 연구)

  • Kim, Jong-Guk;Kim, Gi-Taek;Kim, Dong-Sik;Gang, Yong-Jin;Lee, Seong-Hun
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2015.05a
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    • pp.72-72
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    • 2015
  • 최근 비철소재 가공용 공구의 이형성 향상 코팅 및 자동차 부품의 고온 환경에서 사용할 수 있는 코팅으로 유망한 수소가 없는 비정질 다이아몬드 카본 막 (Non-Hydrogen Diamond Like Carbon films : ta-C)을 양산할 수 있는 코팅 시스템에 대한 연구 결과를 발표하고자 한다. 본 시스템은 Diamet-600이라고 하며 ta-C의 처리폭은 350 mm, 직경 450 mm 8축 공자전 치구에서 400nm/h의 증착률을 가지며, 막의 경도는 최대 65GPa을 달성하였다.

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Field Emission characteristics of Multi-layered Diamond-Like carbon films (다층구조 유사다이아몬드 박막의 전계방출 특성연구)

  • 김종탁
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.13 no.5
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    • pp.426-430
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    • 2000
  • We have studied the field emission characteristics of multi-layered diamond-like-carbon (DLC) films deposited by vertical electrodes type plasma enhanced chemical vapor deposition with CH$_4$ and H$_2$ mixture. We deposited a thin layer of DLC on the p$^{+}$-Si substrate and then turned off plasma before another deposition of a new DLC layer. The thickness and the number of DLC layers are varied. The emission characteristics of multi-layered DLC films were compared with conventional one. The multi-layered DLC film shows higher emission current than conventional one.e.

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Deposition of hard coatings on polycarbonate substrate by high frequency ion beam

  • Kim, Sung-Ryong;Song, Jun-Seob;Choi, Young-Joon;Kim, Jong-Hun
    • Journal of Korean Vacuum Science & Technology
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    • v.2 no.2
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    • pp.101-106
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    • 1998
  • The poor wear and scratch properties of polycarbonate have limited its application in many fields. In order to improve the wear and scratch properties of polycarbonate we have deposited diamond like carbon (DLC) coatings. The diamond like carbon coatings were made using a high frequency ion beam gun by introducing H2 and CH4 gases. The coatings were characterized with Raman spectroscopy, scanning electron microscope, ellipsometer, microscratch tester and hazemeter. Polymeric hard coating was applied onto the polycarbonate substrate before depositing a DLC coating to investigate the effect of interlayer on the system's failure mode.

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Effect of Contact Conditions on the Micro-adhesion Characteristics using SPM (SPM을 이용한 접촉조건 변화에 따른 미소응착 특성 연구)

  • 윤의성;박지현;양승호;공호성
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2000.11a
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    • pp.18-22
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    • 2000
  • An experimental study was carried out to investigate the effect of nano-contact condition on the nano-adhesion phenomena. SPM(scanning probe microscope) tips with different radius of curvature were fabricated by a series of masking and etching processes. DLC(diamond-like carbon) and W-DLC (tungsten-incorporated diamond-like carbon) were coated on (100) silicon wafer by PACVD(plasma assisted chemical vapor deposition). Pull-off forces of Pure Si-wafer, DLC and W-DLC were measured with SPM(scanning probe microscope). Also, the same series of tests were carried out with the tips with different radius of curvature. Results showed that DLC and W-DLC showed much lower pull-off force than Si-wafer and Pull-off force increased with the tip radius.

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Field emission from diamond-like carbon films studied by scanning anode

  • Ahn, S.H.;Jeon, D.;Lee, K.-R.
    • Journal of Korean Vacuum Science & Technology
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    • v.3 no.1
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    • pp.54-58
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    • 1999
  • We deposited diamond-like carbon (DLC) films using ion beam sputtering of a graphite target on flat substrates for use as a thin film field emitter. An n-type silicon wafer, titanium-coated silicon, and indium tin oxide (ITO) coated glass were used as a substrate. All films exhibited a sudden increase in the emission after a breakdown occurred at high voltage. The morphology of the films after the breakdown depended on the substrate. On ITO and Ti substrates, the DLC film peeled off upon breakdown, but on the Si substrate the surface melting due to breakdown resulted in the formation of various structures such as a sharp point, mound, and crater. By scanning the deformed surface with a tip anode, we found that the emission was concentrated at the deformed sites, indicating that the field enhancement due to the morphology change was responsible for the increased emission.

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Deposition of diamond film at low pressure using the RF plasma CVD (고주파 플라즈마 CVD에 의한 저 압력에서의 다이아몬드 막의 성장)

  • Koo, Hyo-Geun;Park Sang-Hyun;Park Jae-Yoon;Kim Kyoung-Hwan
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.50 no.2
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    • pp.49-56
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    • 2001
  • Diamond thin films have been deposited on the silicon substrate by inductively coupled radio frequency plasma enhanced chemical vapor deposition system. The morphological features of thin films depending on methane concentration and deposition time have been studied by scanning electron microscopy and Raman spectroscopy. The diamond particles deposited uniformly on silicon substrate($10{\times}10[mm^2]$) at the pressure of 1[torr], a methane concentration of 1[%], a hydrogen flow rate of 60[sccm], a substrate temperature of $840\{sim}870[^{\circ}C]$, an input power of 1[kw], and a deposition time of 1[hour]. With increasing deposition time, the diamond particles grew, and than about 3 hours have passed, the graphitic phase carbon thin film with "cauliflower-like" morphology deposited on the diamond thin films.

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