• Title/Summary/Keyword: Determining the phase

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Fabrication of High Tc Superconductor Using Thermal Pyrolysis (열분해법에 의한 고온 초전도 합성)

  • Lee, Sang-Heon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.85-86
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    • 2006
  • A high Tc superconducting with a nominal composition of $Bi_2Sr_2Ca_2Cu_3O_y$ was prepared by the citarte method. The solid precursor produced by the dehydration of the gel at $120^{\circ}C$ for 12h is not in the amorphous state as expected but in a crystalline state. X-ray diffraction peaks of nearly the same angular position as the peaks of high Tc phase were observed in the precursor. After pyrolysis at $400^{\circ}C$ and calcination at $840^{\circ}C$ for 4h, the (001)peak of the high Tc phase was cleary observed. Experimental results suggest that the intermediate phase formed before the formation of the superconducting phase may be the most important factro in determining whether it is easy to form the high Tc phase or not, because the nucleation barriers of the two superconducting phase may be altered by the variation of the crystal structures of those intermediate phase.

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Product Phase Control During Interdiffusion Reactions (상호 확산 반응 중의 생성상 제어)

  • Park, Joon-Sik;Kim, Ji-Hoon;Perepezko, John R.
    • Journal of Korea Foundry Society
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    • v.26 no.1
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    • pp.27-33
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    • 2006
  • Phase evolutions involving nucleation stages together with diffusional growth have been examined in order to provide a guideline for determining rate limiting stages during phase evolutions. In multiphase materials systems in coatings, composites or multilayered structures, diffusion treatments often result in the development of metastable/intermediate phases at the reaction interfaces. The development of metastable phases during solid state interdiffusion demonstrates that the nucleation reaction can be one controlling factor. Also, the concentration gradient and the relative magnitudes of the component diffusivities provide a basis for a phase selection and the application of a kinetic bias strategy in the phase selection. For multicomponent alloy systems, the identification of the operative diffusion pathway is central to control phase formation. Experimental access to the nucleation and growth stage is discussed in thin film multi layers and bulk samples.

Phase-shedding in Boundary Conduction Mode Converter with Optimal Transition Load-level

  • Choi, Wooin;Baek, Jong-Bok;Cho, Bo-Hyung
    • Proceedings of the KIPE Conference
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    • 2011.11a
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    • pp.73-74
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    • 2011
  • Phase-shedding, one famous technology for multi-phase converters, is implemented in a bi-directional multi-phase converter for ESS. It reduces active operating modules at light load to compensate efficiency. Shedding point, the load level where the converter changes the number of active modules, is important factor that affects the effect of phase-shedding. Loss analysis is done for determining shedding point. Phase-shedding hysteresis is applied so that excessive phase transition is avoided. This paper proposes shedding point correction where the shedding point is adaptively corrected by calculating a new shedding point.

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A Study on the Analytical Methods Using Solid-phase Extraction for the Determination of Phenols in Water

  • Jeon, Chi-Wan;Lee, Jung-Hwa;Lee, Sang-Hak
    • Proceedings of the Korean Environmental Sciences Society Conference
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    • 2003.11a
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    • pp.135-138
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    • 2003
  • Based on solid phase extraction, gas chromatography and mass spectrometry procedure for determining phenol and its derivatives in natural water was presented. In solid phase extraction, three types of techniques using solid phase adsorption material were treated with acid and salt, and converted second portion of acetyl derivatives. Under the these condition, extraction efficiency and detection ability dependent on extraction methods were discussed. Obtained results using optimized solid phase extraction techniques showed more convenience, simplifier and lower cost than the conventional analytical methods with holding wide dynamic range and lower detection limits.

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Electric Perperties of Superconductor Using Pyrolysis Methods (열분해법에 의한 초전도체의 전기적 특성)

  • Lee, Sang-Heon;Lee, Young-Hie
    • Proceedings of the KIEE Conference
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    • 2005.11a
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    • pp.79-80
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    • 2005
  • The solid precursor produced by the dehydration of the gel at $120^{\circ}C$ for 12h is not in the amorphous state as expected but in a crystalline state. X-ray diffraction peaks of nearly the same angular position as the peaks of high Tc phase were observed in the precursor. Experimental results suggest that the intermediate phase formed before the formation of the superconducting phase may be the most important fact in determining whether it is easy to form the superconducting phase or not, because the nucleation barriers of the two superconducting phase may be altered by the variation of the crystal structures of those intermediate phase.

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Synthesis of YBCO Superconducting Precursor using Organic metal salts method for Electric power transmission (유기금속염을 이용한 전력 전송용 YBCO 초전도 전구체 합성)

  • Lee, Sang-Heon
    • Proceedings of the KIEE Conference
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    • 2005.07c
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    • pp.1966-1967
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    • 2005
  • The solid precursor produced by the dehydration of the gel at $120^{\circ}C$ for 12h is not in the amorphous state as expected but in a crystalline state. X-ray diffraction peaks of nearly the same angular position as the peaks of high Tc phase were observed in the precursor. Experimental results suggest that the intermediate phase formed before the formation of the superconducting phase may be the most important fact in determining whether it is easy to form the superconducting phase or not, because the nucleation barriers of the two superconducting phase may be altered by the variation of the crystal structures of those intermediate phase.

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Improvement in Control Performance of a Servo System Compensating Bandwidth Variations at Low Speed

  • Ji, Young-Eun;Park, Je-Wook;Hwang, Seon-Hwan;Baek, Kwang-Ryul;Kim, Jang-Mok
    • Journal of Power Electronics
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    • v.10 no.4
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    • pp.382-387
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    • 2010
  • This paper presents a novel design method for determining the PID gains of a speed controller for a servo system compensating variations in bandwidth at a low speed. The variations in bandwidth of a speed controller are measured at a low speed and the relationship between the bandwidth and the damping ratio are verified by determining the location of the closed loop pole. The proposed algorithm uses the z-transform of a plant and speed controller and applies the time-varying sampling method for determining the PID gains of the speed controller at low speed. The magnitude and the phase condition are considered for finding a suitable control gain. The usefulness and effectiveness of the proposed method is demonstrated through experimental results such as low speed control and robust disturbance responses.

Determining Method of Minimum-capacitance for Self-excited Induction Generator (자기 여자 유도 발전기의 최소 커패시턴스의 결정법)

  • Jin, Chung-Min;Jwa, Chong-Keun
    • Proceedings of the KIEE Conference
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    • 2000.07b
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    • pp.729-731
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    • 2000
  • This paper presents a simple method for determining the minimum value of capacitance required for initiating self excitation in three-phase self-excited induction generator. Based on the steady-state equivalent circuit model, this paper presents simple and direct method to find the minimum capacitance requirement under R-L load. Using the loop impedance and nodal admittance. the minimum capacitance is determined by self excitation condition. These computed values can be used to predict practically the minimum value of the terminal voltage required for self-excitation. To maintain a constant terminal voltage, a method for determining the frequency, terminal capacitance, and exciting reactance is also described.

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The Design of IMC-PID Controller Considering a Phase Scaling Factor (위상 조절 인자를 고려한 IMC-PID 제어기의 설계)

  • Kim, Chang-Hyun;Lim, Dong-Kyun
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.57 no.9
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    • pp.1618-1623
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    • 2008
  • In this paper, a new design method for IMC-PID that adds a phase scaling factor of system identifications to the standard IMC-PID controller as a control parameter is proposed. Based on analytically derived frequency properties such as gain and phase margins, this tuning rule is an optimal control method determining the optimum values of controlling factors to minimize the cost function, integral error criterion of the step response in time domain, in the constraints of design parameters to guarantee qualified frequency design specifications. The proposed controller improves existing single-parameter design methods of IMC-PID in the inflexibility problem to be able to consider various design specifications. Its effectiveness is examined by a simulation example, where a comparison of the performances obtained with the proposed tuning rule and with other common tuning rules is shown.

Effects of Segmented Poles on Exciting Forces for BLDC Motors (세그먼트 극을 가진 BLDC 전동기의 가진력에 관한 연구)

  • Kim, Gyeong-Tae;Hwang, Sang-Mun
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.48 no.10
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    • pp.530-536
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    • 1999
  • This paper investigates effects of segmented poles on exciting forces such as cogging torque, BEMF, phase current, torque ripple and local forces. Cogging torque, BEMF and local force are determined by FEM analysis and phase current is calculated using voltage equations after determining BEMF and phase inductance. Effective dead zones at pole separations result in wider than the physical dead zones due to leakage field during magnetization. Due to the existence of dead zones, there exist additional exciting harmonics of the cogging torque which play adverse effect on vibration and noise performance. The magnitude of BEMF is decreased and the waveforms are also distorted depending on dead zone positions. Segmented poles inevitably cause uneven magnetic field distribution at pole separations which introduces additional harmonics of exciting forces which are detrimental to structural to structural resonances. They also decrease motor efficiency by reducing effective phase BEMF.

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