• Title/Summary/Keyword: Detection techniques

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Analysis of some pesticides in urine by GC/MS (GC/MS를 이용한 뇨중 몇가지 농약의 분석)

  • Park, Seong-Soo;Park, Song-Ja;Pyo, Hee-Soo;Cho, Jung-Hee;Kim, Hye-Soo;Park, Taek-Kyu
    • The Korean Journal of Pesticide Science
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    • v.4 no.1
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    • pp.1-10
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    • 2000
  • The purpose of this study is to establish the assessment techniques of hazardous chemicals by the development of analytical method of biological samples. In this study, we have developed an extraction method of nine pesticides used for rice paddy that resulted in high recovery from the spiked human urine by the liquid-liquid extraction with diethyl ether at pH 7.0. Calibration curve obtained from each pesticide standard using by gas chromatography/mass spectrometry/selected ion monitoring has shown good linearity and detection limits were the range of $0.4{\sim}2.0$ ng/mL in urine. As a biological monitoring, urine samples of local farmers exposed directly to nine pesticides in the field were collected and analyzed by GC/MS. Of the tested pesticides, metabolites of phenthoate assumed were identified by GC/MS analysis. No parent compound was detected.

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Simultaneous Analytical Techniques for Determination of 8 Synthetic Food Colors in Foods by HPLC (HPLC를 이용한 식품중 식용타르색소 8종의 동시분석)

  • Park, Sung-Kwan;Lee, Chang-Hee;Park, Jae-Seok;Yoon, Hae-Jung;Kim, So-Hee;Hong, Yeun;Lee, Jong-Ok;Lee, Chul-Won
    • Analytical Science and Technology
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    • v.13 no.3
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    • pp.378-384
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    • 2000
  • This Study has been carried out to develop a method of analysis of 8 permitted synthetic food colors [including Brilliant Blue FCF(B1), Indigocarmine (B2), Fast green FCF(G3), Amaranth (R2), Erythrosine (R3), Allura red (R40), Tartrazine (Y4), Sunset Yellow FCF (Y5)] in Korean foods by HPLC. After adjusting to 0.5% HCl, each of the food colors extracted was eluted by Sep-pak $C_{18}$ cartridge. Eluates were then determined by high performance liquid chromatograph with a UV-VIS detector. Recoveries of the 8 synthetic food colors were found to be 81.2-98.0% for soft drinks, 80.6-96.1% for candy, 79.8-96.3% for chewing gum, 76.5-91.7% for cereals, 79.9-93.8% for ice cream and 78.6-94.7% for jelly, respectively. The detection limits were $0.05-0.1{\mu}g/g$.

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A Personal Information Security System using Form Recognition and Optical Character Recognition in Electronic Documents (전자문서에서 서식인식과 광학문자인식을 이용한 개인정보 탐지 및 보호 시스템)

  • Baek, Jong-Kyung;Jee, Yoon-Seok;Park, Jae-Pyo
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.5
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    • pp.451-457
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    • 2020
  • Format recognition and OCR techniques are widely used as methods for detecting and protecting personal information from electronic documents. However, due to the poor recognition rate of the OCR engine, personal information cannot be detected or false positives commonly occur. It also takes a long time to analyze a large amount of electronic documents. In this paper, we propose a method to improve the speed of image analysis of electronic documents, character recognition rate of the OCR engine, and detection rate of personal information by improving the existing method. The analysis speed was increased using the format recognition method while the analysis speed and character recognition rate of the OCR engine was improved by image correction. An algorithm for analyzing personal information from images was proposed to increase the reconnaissance rate of personal information. Through the experiments, 1755 image format recognition samples were analyzed in an average time of 0.24 seconds, which was 0.5 seconds higher than the conventional PAID system format recognition method, and the image recognition rate was 99%. The proposed method in this paper can be used in various fields such as public, telecommunications, finance, tourism, and security as a system to protect personal information in electronic documents.

Surgical Treatment of Gastric Cancer

  • Kim, Sang-Woon
    • Journal of Yeungnam Medical Science
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    • v.20 no.2
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    • pp.105-116
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    • 2003
  • Definitely, treatment for gastric cancer is primarily surgical. Detection in early stage of disease and complete surgical resection is the best way to cure gastric cancer. If surgery is planned, careful preoperative evaluation and corrections of physiologic and psychologic abnormalities are essential to reduce perioperative morbidity or mortality. Basic principle of gastrectomy for gastric cancer is an en bloc resection of tumor with adequate margins of normal tissue and with regional lymph nodes and omental tissues. To complete these principles, regional lymph nodes and all omental tissues should be removed altogether during performing various types of gastric resection. The lymph node dissection is one of the most effective procedures for gastric cancer to achieve curative resection. The basic types of gastric resection are distal subtotal gastrectomy and total gastrectomy according to the condition of primary lesions and the status of lymph node metastases. When the primary lesion is located near the esophagogastric junction, it is sometimes hard for a surgeon to select adequate surgical method. Postoperative quality of life in a patient has become a very important factor to be considered in every step of surgical therapy. With increasing incidence of early gastric cancer, a number of surgical trials for limited surgery or endoscopic procedures have been performed, but the long-term clinical results should be carefully analyzed to define the clinical relevance of these new techniques. For patients with disseminated gastric cancer, a palliative procedure can be performed to improve quality of life of patients and to avoid immediate death due to the cancer-related complications.

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Effects of Red Deer Antlers on Cutaneous Wound Healing in Full-thickness Rat Models

  • Gu, LiJuan;Mo, EunKyoung;Yang, ZhiHong;Fang, ZheMing;Sun, BaiShen;Wang, ChunYan;Zhu, XueMei;Bao, JianFeng;Sung, ChangKeun
    • Asian-Australasian Journal of Animal Sciences
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    • v.21 no.2
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    • pp.277-290
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    • 2008
  • The process of wound repair involves an ordered sequence of events such as overlapping biochemical and cellular events that, in the best of circumstances, result in the restoration of both the structural and functional integrity of the damaged tissue. An important event during wound healing is the contraction of newly formed connective tissues by fibroblasts. The polypeptide growth factors, like transforming growth factor-${\beta}$(TGF-${\beta}$, insulin-like growth factor I (IGF- I) and epidermal growth factor (EGF), play very important mediator roles in the process of wound contraction. Deer antlers, as models of mammalian regeneration, are cranial appendages that develop after birth as extensions of a permanent protuberance (pedicle) on the frontal bone. Antlers contain various growth factors which stimulate dermal fibroblast growth. They are involved in digestion and respiration and are necessary for normal wound healing and skin health. In order to investigate and evaluate the effects of red deer antlers on skin wound site, the speed of full-thickness skin wound healing and the expression of IGF-I, TGF-${\beta}$ and EGF in skin wounds, three groups of skin full-thickness rat models with a high concentration of antler ointment, a low concentration of antler ointment and without antler ointment were compared. At post-injury days 0, 2, 4, 8, 16, 20, 32, 40 and 60, the skin wound area was measured, the expressions of IGF-I, TGF- ${\beta}$ and EGF mRNA were detected by reverse transcriptase polymerase chain reaction (RT-PCR) and collagen formation by sirius red dye and the localization of IGF-I, TGF-${\beta}$ and EGF peptides were inspected by histological immunohistochemical techniques. Wound healing was significantly more rapid in antler treated skins. In addition, the wound treated with a high concentration antler ointment, a low concentration antler ointment, and the control closed completely at post-injury day 40, day 44 and day 60, respectively. Via RT-PCR, the expressions of IGF-I (day 8 and day 16), TGF-${\beta}$(day 8, day 16 and day 20) and EGF (day 4, day 8, day 16, and day 32) were obviously up-regulated in high concentration antler-treated skins compared to control skins. Similar results could be seen in the histological detection of collagen dye and immunohistochemical methods using the corresponding polyclone antibodies of IGF-I, TGF-${\beta}$ and EGF. These results illustrate that antlers stimulate and accelerate the repair of cutaneous wounds.

Multi-layer Caching Scheme Considering Sub-graph Usage Patterns (서브 그래프의 사용 패턴을 고려한 다중 계층 캐싱 기법)

  • Yoo, Seunghun;Jeong, Jaeyun;Choi, Dojin;Park, Jaeyeol;Lim, Jongtae;Bok, Kyoungsoo;Yoo, Jaesoo
    • The Journal of the Korea Contents Association
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    • v.18 no.3
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    • pp.70-80
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    • 2018
  • Due to the recent development of social media and mobile devices, graph data have been using in various fields. In addition, caching techniques for reducing I/O costs in the process of large capacity graph data have been studied. In this paper, we propose a multi-layer caching scheme considering the connectivity of the graph, which is the characteristics of the graph topology, and the history of the past subgraph usage. The proposed scheme divides a cache into Used Data Cache and Prefetched Cache. The Used Data Cache maintains data by weights according to the frequently used sub-graph patterns. The Prefetched Cache maintains the neighbor data of the recently used data that are not used. In order to extract the graph patterns, their past history information is used. Since the frequently used sub-graphs have high probabilities to be reused, they are cached. It uses a strategy to replace new data with less likely data to be used if the memory is full. Through the performance evaluation, we prove that the proposed caching scheme is superior to the existing cache management scheme.

Application of CNN for steering control of autonomous vehicle (자율주행차 조향제어를 위한 CNN의 적용)

  • Park, Sung-chan;Hwang, Kwang-bok;Park, Hee-mun;Choi, Young-kiu;Park, Jin-hyun
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2018.05a
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    • pp.468-469
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    • 2018
  • We design CNN(convolutional neural network) which is applicable to steering control system of autonomous vehicle. CNN has been widely used in many fields, especially in image classifications. But CNN has not been applied much to the regression problem such as function approximation. This is because the input of CNN has a multidimensional data structure such as image data, which makes it is not applicable to general control systems. Recently, autonomous vehicles have been actively studied, and many techniques are required to implement autonomous vehicles. For this purpose, many researches have been studied to detect the lane by using the image through the black box mounted on the vehicle, and to get the vanishing point according to the detected lane for control the autonomous vehicle. However, in detecting the vanishing point, it is difficult to detect the vanishing point with stability due to various factors such as the external environment of the image, disappearance of the instant lane and detection of the opposite lane. In this study, we apply CNN for steering control of an autonomous vehicle using a black box image of a car.

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Development of Quantitative Analytical Method for Isoflavonoid Compounds from Fruits of Cudrania Tricuspidata (꾸지뽕나무 열매 isoflavonoid 화합물에 대한 정량분석법 개발)

  • Yoon, Sun Young;Kim, Seok Ju;Sim, Su Jin;Lee, Hak-Ju
    • Journal of the Korean Wood Science and Technology
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    • v.44 no.3
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    • pp.337-349
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    • 2016
  • In this study, an analytical method to evaluate the quality of isoflavonoid compounds purified and isolated from the fruits of Cudrania tricuspidata was developed and validated using Ultra Performance Liquid Chromatography (UPLC). The fruits of C. tricuspidata were extracted with methanol and further fractioned with n-hexane, ethyl acetate and water. The resulting ethyl acetate extract separated into four isoflavonoid compounds by a combination of silica gel and sephadex LH-20 column chromatography. The structures of the compounds were elucidated as alpinumisoflavone, 6,8-diprenyl genistein, 6,8-diprenyl orobol, 4'-O-methylalpinumisoflavone by various techniques such as UV-Vis, ESI-MS, $^1H\;NMR$ and $^{13}C\;NMR$ spectroscopy. Finally, a method to characterize the compounds was developed by using the UPLC equipped with a $C_{18}$ column and a gradient mobile phase system consisting of 2% acetic acid in water (solvent A) and 2% acetic acid in methanol (solvent B). The developed method was validated with the parameters such as selectivity, linearity, limit of detection, limit of quantitation, accuracy, and precision, which are defined by the ICH (International Conference on Harmonization). Using the validated method, the compounds in the fruits harvested in different months were also quantitatively analyzed. We propose this approach this approach can readily be utilized as an efficient evaluation method to quantify the extracts of C. tricuspidata.

Analysis of radiation induced hydrocarbons by electron-beam irradiation in dried squid (Todarodes pacificus) and octopus (Paroctopus dofleini) (전자선 조사한 건조된 오징어와 문어에서 유도된 지방분해산물의 분석)

  • Hong, Young Shin;Ryu, Keun Young;Kim, Kyong Su
    • Food Science and Preservation
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    • v.21 no.3
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    • pp.381-387
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    • 2014
  • Food irradiation is one of the successful modern techniques used to preserve food. However, it needs very careful control. Detection of irradiated food is of prime importance to facilitate global trade and consumer assurance, choice, and protection. This study was performed to evaluate the radiation-induced hydrocarbon content of dried squid and octopus by e-beam irradiation. The samples were collected from supermarkets all over South Korea and irradiated with an e-beam at 0, 1, 3, 5, 7, and 10 kGy doses. Lipids were extracted with soxhelt, and the hydrocarbons induced with irradiation were separated via solid phase extraction (SPE) and identified via gas chromatography mass spectrometry (GC/MS). The major induced hydrocarbons in the irradiated dried squid and octopus were 1-tetradecene and pentadecane derived from palmitic acid and 1-hexadecene and heptadecane from stearic acid. The concentration of hydrocarbons differed from the composition of the fatty acid at the same radiation and increased according to the level of the radiation dose. The hydrocarbons induced by e-beam irradiation, including 1-tetradecene, 1-hexadecene, and heptadecane, were confirmed to have been the irradiation marker compounds. Therefore, they can be used to distinguish the e-beam-irradiated dried squid and octopus from the non-irradiated ones.

Interpretation on Raw Material Characteristics and Manufacturing Techniques of Brown-glazed Stonewares and Roof Tiles from Hong Nang Sida Temple, Laos (라오스 홍낭시다 유적 출토 갈유도기와 기와의 원료특성과 제작기술 해석)

  • Jin, Hong Ju;Jang, Sungyoon;Kim, Su Kyoung;Lee, Myeong Seong;Moon, Dong Hyeok;Chun, Yu Gun
    • Journal of the Mineralogical Society of Korea
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    • v.32 no.4
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    • pp.273-285
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    • 2019
  • This study is aimed to interpret the raw material characteristics and manufacturing technology through physical, mineral and geochemical analysis of the brown-glazed stonewares and roof tiles excavated from the Hong Nang Sida temple in Laos, which was built in the 12th century. The glaze of brown-glazed stoneware is a typical lime serial with CaO content of more than 15 % and they were vitrified. The body is the combination of quartz, mullite and cristobalite, but had not vitrified texture, and therefore, which is assumed to have been fired more than 950 ℃. Meanwhile, The roof tiles are unglazed and its outer color is reddish brown, whitish grey and bluish grey. The bluish gray tiles has sandwich structure, which seem to experience imperfect reducing environment. The tile samples with a number of amorphous iron oxide nodule had a very similar chemical composition. In conclusion, it is assumed that the clay source was made from raw material produced from the same bedrock. The firing temperature of roof tiles were divided into less than 900 ℃, 900~950 ℃ and greater than 950 ℃ according to detection of micas, hercynite and mullite.