• Title/Summary/Keyword: Design of mixture experiments

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Fundamental Study on the Application of a Surface Layer using Cold Central-Plant Recycling (플랜트 생산 재활용 상온 혼합물의 도로 표층 적용성에 관한 기초연구)

  • Choi, Jun Seong
    • International Journal of Highway Engineering
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    • v.20 no.1
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    • pp.69-76
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    • 2018
  • PURPOSES : This study determined the optimal usage rate of RAP (reclaimed asphalt pavement) using cold central-plant recycling (CCPR) on a road-surface layer. In addition, a mixture-aggregate gradation design and a curing method based on the proposed rate for the surface-layer mix design were proposed. METHODS : First, current research trends were investigated by analyzing the optimum moisture content, mix design, and quality standards for surface layers in Korea and abroad. To analyze the aggregate characteristics of the RAP, its aggregate-size characteristics were analyzed through the combustion asphalt content test and the aggregate sieve analysis test. Moreover, aggregate-segregation experiments were performed to examine the possibility of RAP aggregate segregation from field compaction and vehicle traffic. After confirming the RAP quality standards, coarse aggregate and fine aggregate, aggregate-gradation design and quality tests were conducted for mixtures with 40% and 50% RAP usage. The optimum moisture content of the surface-layer mixture containing RAP was tested, as was the evapotranspiration effect on the surface-layer mixture of the optimum moisture content. RESULTS : After analyzing the RAP recycled aggregate size and extraction aggregate size, 13-8mm aggregate was found to be mostly 8mm aggregate after combustion. After using surface-chipping and mixing methods to examine the possibility of RAP aggregate segregation, it was found that the mixing method contributed very little for 3.32%, and because the surface-chipping method applied compaction energy directly as the maximum assumption the separation ratio was 15.46%. However, the composite aggregate gradation did not change. Using a 40% RAP aggregate rate on the surface-layer mixture for cold central-plant recycling satisfied the Abroad quality standard. The optimum moisture content of the surface-layer mixture was found to be 7.9% using the modified Marshall compaction test. It was found that the mixture was over 90% cured after curing at $60^{\circ}C$ for two days. CONCLUSIONS : To use the cold central-plant recycling mixture on a road-surface layer, a mixture-aggregate gradation design was proposed as the RAP recycled aggregate size without considering aggregate segregation, and the RAP optimal usage rate was 40%. In addition, the modified Marshall compaction test was used to determine the optimum moisture content as a mix-design parameter, and the curing method was adapted using the method recommended by Asphalt Recycling & Reclaiming Association (ARRA).

Design and Analysis of Mixture Experiments for Ball Mix Selection in the Ball Milling (볼밀링에서 볼 배합비 선택을 위한 혼합물 실험계획 및 분석)

  • Kim, Seong-Jun;Choi, Jai Young;Shin, Hyunho
    • Journal of Korean Society for Quality Management
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    • v.42 no.4
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    • pp.579-590
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    • 2014
  • Purpose: Ball milling is a popular process for obtaining fine powders in the part and material industry. One of important issues in the ball milling is to produce particles with a uniform size. Although many factors affect uniformity of particles, this paper focuses on the choice of ball diameter. Consider a ball milling where balls can be taken with three different diameters. The purpose of this paper is to find a ball mix which minimizes the average particle size. Methods: Ball diameters are selected as 10mm, 3mm, and 0.5mm. In order to find an optimum mixing ratio, the method of mixture experiments is employed in this paper. Taguchi's signal-to-noise ratio (SNR) for smaller-the-better type is also used to analyze experimental data. Results: According to the experimental result, SNR is maximized when the ball mix is taken as either 7:3:0 or 6:4:0. Such mixing ratios can be technically validated in terms of porosity reduction. Conclusion: The ball mixing technique presented in this paper provides a useful way to improve the production efficiency with a low cost.

A Study on the Minimum Paste Volume in the Design of Concrete Mixture

  • Fowler, David W.;Hahn, Michael De Moya;Rached, Marc;Choi, Doo-Sun;Choi, Jae-Jin
    • International Journal of Concrete Structures and Materials
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    • v.2 no.2
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    • pp.161-167
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    • 2008
  • Optimization of concrete mixing system is very important for the production of quality mixture of concrete and requires very complicated, specialized knowledge as there are a variety of variables that influence the result. One of the methods of optimizing the concrete mixing system is to minimize the volume of cement paste which, in turn, means maximizing the volume of aggregate. The purpose of this study is to determine the minimum volume of cement paste used in the design of concrete mixture and to design the optimum concrete mixing system based on the fluidity of mortar and concrete. In determining the minimum volume of cement paste, experiments of mortar and concrete were performed based on their workability, material segregation and bleeding. Type of aggregate, granularity distribution and sand percentage were used as test parameters and measurements were taken of the distribution of granularity, usage of HRWRA, minimum volume of paste and drying shrinkage and compressive strength of concrete.

Literature Review on the Experimental Designs in KSQM for 50 Years (품질경영학회 50주년 특별호: 실험계획법 분야 연구 리뷰)

  • Kim, Sang Ik;Lee, Sang Bok;Lim, Yong Bin;Jang, Dae Heung
    • Journal of Korean Society for Quality Management
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    • v.44 no.2
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    • pp.245-264
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    • 2016
  • Purpose: This article focuses on the reviewing the papers published in the Journal of the Korean Society for Quality Control (JKSQC) and the Journal of the Korean Society for Quality Management (JKSQM) since 1965, in the area of design of experiments. In this paper, moreover, some other contents of another statistical quality control areas is included. Methods: The reviewed articles are classified into the three main categories: theory and application of experimental designs, response surface methodology and mixture experiments, and roust designs. Some omitted papers in the other areas of reviewing works are also included in this paper, and the contents and relationships of the published articles are examined and summarized in each sub-field. Results: We summarize the reviewed papers in the chronological road-maps for each sub-field, and outline the relations of the connected papers. We provide comments on the contents and the contributions of the reviewed papers. The future direction of the research in the theory and application areas of experimental designs can be provided by the contents of this research. Conclusion: The diverse topics on the improving the quality in the various industry fields are studied and published on the theory, methodology and the empirical application in the fields of designs of experiments. We can see that the Korean Society for Quality Management (KSQM) has tremendously contributed on the improvement of quality in the manufacturing and service industries by publishing the reviewed articles in this paper.

An Optimal Process Design U sing a Robust Desirability Function(RDF) Model to Improve a Process/Product Quality on a Pharmaceutical Manufacturing Process (제약공정에서 공정 및 제품의 품질향상을 위해 강건 호감도 함수 모형을 이용한 최적공정설계)

  • Park, Kyung-Jin;Shin, Sang-Mun;Jeong, Hea-Jin
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.33 no.1
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    • pp.1-9
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    • 2010
  • Quality design methodologies have received constituent attention from a number of researchers and practitioners for more than twenty years. Specially, the quality design for drug products must be carefully considered because of the hazards involved in the pharmaceutical industry. Conventional pharmaceutical formulation design problems with mixture experiments have been typically studied under the assumption of an unconstrained experimental region with a single quality characteristic. However, real-world pharmaceutical industrial situations have many physical limitations. We are often faced with multiple quality characteristics with constrained experimental regions. ln order to address these issues, the main objective of this paper is to propose a robust desirability function (RDF) model using a desirability function (DF) and mean square error (MSE) to simultaneously consider a number of multiple quality characteristics. This paper then present L-pseudocomponents and U-pseudocomponents to handle physical constraints. Finally, a numerical example shows that the proposed RDF can efficiently be applied to a pharmaceutical process design.

Design of Experiments for Enhanced Catalytic Activity: Cu-Embedded Covalent Organic Frameworks in 4-Nitrophenol Reduction

  • Sangmin Lee;Kye Sang Yoo
    • Applied Chemistry for Engineering
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    • v.35 no.4
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    • pp.346-351
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    • 2024
  • Chemical reduction using catalysts and NaBH4 presents a promising approach for reducing 4-nitrophenol contamination while generating valuable byproducts. Covalent organic frameworks (COFs) emerge as a versatile platform for supporting catalysts due to their unique properties, such as high surface area and tunable pore structures. This study employs design of experiments (DOE) to systematically optimize the synthesis of Cu embedded COF (Cu/COF) catalysts for the reduction of 4-nitrophenol. Through a series of experimental designs, including definitive screening, mixture method, and central composition design, the main synthesis parameters influencing Cu/COF formation are identified and optimized: MEL:TPA:DMSO = 0.31:0.36:0.33. Furthermore, the optimal synthesis temperature and time were predicted to be 195 ℃ and 14.7 h. Statistical analyses reveal significant factors affecting Cu/COF synthesis, facilitating the development of tailored nanostructures with enhanced catalytic performance. The catalytic efficacy of the optimized Cu/COF materials is evaluated in the reduction of 4-nitrophenol, demonstrating promising results in line with the predictions from DOE.

Binary Mixture Rule for Predicting the Dielectric Properties of Unidirectional E-glass/Epoxy Composite Materials (일방향 유리섬유/에폭시 복합재료의 유전성질 예측을 위한 혼합법칙)

  • Chin Woo Seok;Lee Dai Gil
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2004.10a
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    • pp.175-179
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    • 2004
  • Since the electromagnetic properties of fiber reinforced polymeric composites can be tailored effectively by adding small amount of electromagnetic powders to the matrix of composites, they are plausible materials for fabricating the radar absorbing structures (RAS) of desired performance. In order to design the effective electromagnetic wave (EM) absorber with the fiber reinforced polymeric composites, the electromagnetic characteristics with respect to the constituents of the composite should be available in the target frequency band. In order to describe the dielectric behavior of low loss unidirectional fiber reinforced composite, theoretical models and mixture equations for estimating its dielectric constant were proposed with respect to the fiber, matrix volume fractions and fiber orientations, and verified by the experiments. From the investigation, it was found that the suggested binary mixture rules agreed well with the experimental results.

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SIMULATION OF THE DESIGN METHODOLOGY FOR HIGH PERFORMANCE AND EFFICIENT CAVITATOR (측류유동을 고려한 실린더 주위의 캐비테이션 유동 현상 해석)

  • Lee, B.W.;Park, S.I.;Park, W.G.;Lee, K.C.
    • 한국전산유체공학회:학술대회논문집
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    • 2009.11a
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    • pp.177-184
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    • 2009
  • Cavitating flow simulation is of practical importance for many engineering systems, such as marine propellers, pump impellers, nozzles, injectors, torpedoes, etc. The present work has focused on the simulation of cavitating flow past cylinders with strong side flows. The governing equation is the Navier-Stokes equation based on the homogeneous mixture model. The momentum and energy equation is in the mixture phase while the continuity equation is solved liquid and vapor phase, separately. An implicit dual time and preconditioning method are employed for computational analysis. For the code validation, the results from the present solver have been compared with experiments and other numerical results. A fairly good agreement with the experimental data and other numerical results have been obtained. After the code validation, the strong side flow was applied to include the wake flow effects of the submarine or ocean tide.

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A Study of the Optimization of the MOF-5 Synthesis Process using Design of Experiments (실험계획법을 이용한 MOF-5 합성공정 최적화 연구)

  • Lee, Min Hyung;Lee, Sangmin;Yoo, Kye Sang
    • Applied Chemistry for Engineering
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    • v.33 no.4
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    • pp.402-407
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    • 2022
  • Statistical design of experiments was used to optimize the MOF-5 synthesis process. A mixture design was employed to optimize precursor concentration. The optimal composition of three chemical materials, terephthalic acid, zinc acetate dihydrate, and N,N-dimethylformamide for MOF-5 synthesis was determined by extreme vertices design methods as follows; 1 mol : 2.7 mol : 40 mol. A multilevel factorial design was selected to screen the significance of synthesis reaction conditions such as temperature, time, and stirring speed. Statistical analysis results suggested excluding stirring speed from further investigation. Using a central composition design, the synthesis time and temperature were optimized. The quadratic model equation was derived from 13 synthesis experiments. The model predicted that MOF-5 synthesized at 119 ℃ for 10.4 h had the highest crystallinity.

Investigation of condensation with non-condensable gas in natural circulation loop for passive safety system

  • Jin-Hwa Yang;Tae-Hwan Ahn;Hwang Bae;Hyun-Sik Park
    • Nuclear Engineering and Technology
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    • v.55 no.3
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    • pp.1125-1139
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    • 2023
  • The system-integrated modular advanced reactor 100 (SMART100), an integral-type pressurized water small modular reactor, is based on a novel design concept for containment cooling and radioactive material reduction; it is known as the containment pressure and radioactivity suppression system (CPRSS). There is a passive cooling system using a condensation with non-condensable gas in the SMART CPRSS. When a design basis accident such as a small break loss of coolant accident (SBLOCA) occurs, the pressurized low containment area (LCA) of the SMART CPRSS leads to steam condensation in an incontainment refuelling water storage tank (IRWST). Additionally, the steam and non-condensable gas mixture passes through the CPRSS heat exchanger (CHX) submerged in the emergency cooldown tank (ECT) that can partially remove the residual heat. When the steam and non-condensable gas mixture passes through the CHX, the non-condensable gas can interrupt the condensation heat transfer in the CHX and it degrades CHX performance. In this study, condensation heat transfer experiments of steam and non-condensable gas mixture in the natural circulation loop were conducted. The pressure, temperature, and effects of the non-condensable gas were investigated according to the constant inlet steam flow rate with non-condensable gas injections in the loop.