• Journal of the Korean Ceramic Society
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• v.35 no.12
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• pp.1308-1315
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• 1998

Effects of particle size of alumina on densification behavior during liquid-phase sintering of alumina-talc system were investigated with emphasis on particle rearrangement process. In the case of using coarse alu-mina powder densiication of specimens was rapidly accelerated after formation of liquid phase due to easy particle rearrangement process with addition of talc and increase of sintering temperature. On the contrary when fine alumina powder was used premature densification of alumina matrix region formed before for-mation of liquid phase rigid skeleton structure and then it seemed to inhibit rearrangement process during crease of sintering temperature. As results the densification of specimens using coarse alumina powder was higher than that of the case of using fine one.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.30 no.11 s.254
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• pp.1376-1383
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• 2006

Densification behavior of various metal and ceramic powders was investigated under cold compaction. The Cap model was proposed by using the parameters involved in the yield function for sintered metal powder and volumetric strain evolution under cold isostatic pressing. The parameters for ceramic powder can also be obtained from experimental data under triaxial compression. The Cap model was implemented into a finite element program (ABAQUS) to compare with experimental data for densification behavior of various metal and ceramic powders under cold compaction. The agreement between finite element calculations from the Cap model and experimental data is very good for metal and ceramic powder under cold compaction.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.22 no.4
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• pp.924-938
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• 1998

Densification behavior of ceramic powder under cold compaction was investigated. Experimental data were obtained for zirconia powder and alumina powder under triaxial compression with various loading conditions. A special form of the Cap model was proposed from experimental data under triaxial compression for a yield function of ceramic powder. The proposed yield function was inplemented into a finite element program (ABAQUS) to study densification behaviors of zirconia and alumina powders under die compaction. The effect of friction between the powder and die wall was also investigated. Density distributions of powder compacts were measured and compared with finite element results.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.21 no.8
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• pp.1175-1187
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• 1997

Densification behavior and grain growth of zirconia powder compacts are investigated under high temperature. Experimental data are obtained for zirconia powder under pressureless sintering, sinter forging and hot isostatic pressing. The constitutive equations by Kwon et al. are used for diffusional creep and grain growth. The constitutive equations by McMeeking and co-workers are also included to study the effect of power-law creep. These constitutive equations are implemented into a finite element program (ABAQUS) to investigate the friction effect during sinter forging and the canning effect during hot isostatic pressing. The agreements between experimental data and finite element results are very good in pressureless sintering and hot isostatic pressing, but not as good in sinter forging.

• Journal of Powder Materials
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• v.4 no.2
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• pp.90-99
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• 1997

Densification behavior and grain growth of tool steel powder compacts during pressureless sintering, sinter forging, and hot isostatic pressing were investigated. Experimental data were compared with results of finite element calculations by using the constitutive model of Abouaf and co-workers and that of McMeeking and co-workers. Densification and deformation of tool steel powder compacts were studied by implementing power-law creep, diffusional creep, and grain growth into the finite element analysis. The shape change of a powder compact in the container during hot isostatic pressing was also studied. The theoretical models did not agree well with experimental data in sinter forging, however, agreed well with experimental data in hot isostatic pressing.

• Journal of Powder Materials
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• v.10 no.1
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• pp.40-45
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• 2003

Sintering behavior of 2xxx series Al alloy was investigated to obtain full densification and sound microstructure. The commercial 2xxx series Al alloy powder. AMB2712, was used as a starting powder. The mixing powder was characterized by using particle size analyzer, SEM and XRD. The optimum compacting pressure was 200 MPa, which was the starting point of the "homogeneous deformation" stage. The powder compacts were sintered at $550~630^{\circ}C$ after burn-off process at $400^{\circ}C$. Swelling phenomenon caused by transient liquid phase sintering was observed below $590^{\circ}C$ of sintering temperature. At $610^{\circ}C$, sintering density was increased by effect of remained liquid phase. Further densification was not observed above $610^{\circ}C$. Therefore, it was determined that the optimum sintering temperature of AMB2712 powder was $610^{\circ}C$.}C$.

• Journal of Powder Materials
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• v.1 no.2
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• pp.190-197
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• 1994

The densification behavior during a sintering of M2 and T15 grade high speed steel powder compacts was reported. Sintered densities over 98% theoretical were achieved by a liquid phase sintering in vacuum for both grades. The optimum sintering temperature range where full densification could be achieved without excessive carbide coarsening and incipient melting was much narrower in M2 than in T15 grade. The sintering response was mainly affected by the type of carbides present. The primary carbides in M2 were identified as $M_6C$ type whereas those in T15 were MC type which provides wider sintering range. The addition of elemental carbon up to 0.3% lowered the optimum sintering temperature for both grades, but had little effect on expanding the sintering range and sintered structure.

• Korean Journal of Metals and Materials
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• v.47 no.9
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• pp.567-572
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• 2009

The densification behaviors of mixtures of copper and steel powders during cold die compaction were investigated. We proposed the pressure-dependent yield function based on the rule of the mixtures of each yield function of a critical relative density type. The constitutive equations were implemented into a finite element program (DEFORM2D) to analyze the densification and deformation behavior of powder mixtures, and the simulated results are in good agreement with the experimental results in reference studies.

• Journal of the Korean Ceramic Society
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• v.39 no.11
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• pp.1083-1089
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• 2002

Densification and grain growth behavior of MgO and -doped alumina ceramics were investigated. MgO was found to inhibit grain growth and to promote densification, but acted to promote grain growth more than densification. The density which showed the maximum shrinkage rate was investigated in the plot of shrinkage rate versus density. The data suggests that the maximum shrinkage rate separates the two kinetic regimes, below the density of maximum shrinkage, the regime associated with densification and above the maxima, the regime associated with the grain growth. The plot exhibits a maximum which shifts to higher temperatures with MgO doping and to lower with doping.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.22 no.2
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• pp.330-342
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• 1998

The effect of rubber mold on densification behavior of pure iron powder was investigated under cold isostatic pressing. The thickness effect of rubber mold was also studied. The elastoplastic constitutive equation based on the yield function of Shima and Oyane was implemented into the finite element program(ABAQUS) to predict compaction responses of metal powder under cold isostatic pressing. The hyperelastic constitutive equation based on Moony-Rivlin and Ogden strain energy potentials was also employed to analyze deformation of rubber mold. The coefficients of the strain energy potentials were obtained from tension and volumetric compression data of rubber. Finite element results were compared with experimental data for densification of pure iron powder under cold isostatic pressing.