• Title/Summary/Keyword: Delta Method

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Development of Quantification Method and Stability of ${\Delta}^9$-Tetrahydrocannabinol and 11-Nor-9-carboxy-${\Delta}^9$-Tetrahydrocannabinol in Oral Fluid (타액 중 ${\Delta}^9$-Tetrahydrocannabinol 및 11-Nor-9-carboxy-${\Delta}^9$-Tetrahydrocannabinol의 분석법 확립 및 안정성 검토)

  • Choi, Hye-Young;Baeck, Seung-Kyung;Jang, Moon-Hee;Choi, Hwa-Kyung;Chung, Hee-Sun
    • YAKHAK HOEJI
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    • v.54 no.4
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    • pp.226-231
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    • 2010
  • Oral fluid has become increasingly popular as an alternative specimen in the field of driving under the influence of drugs (DUID) and work place drug testing. In this study, an analytical method for the detection and quantification of ${\Delta}^9$-tetrahydrocannabinol (THC) and its metabolite, 11-nor-9-carboxy-${\Delta}^9$-tetrahydrocannabinol (THC-COOH) in oral fluid by SPE and GC-MS was established and fully validated. The stability of THC and THC-COOH in oral fluid during storage was also determined by examining the THC and THC-COOH concentration changes depending on time and container materials. Oral fluid samples were kept over 21 days at room temperature, $-4^{\circ}C$ and $-20^{\circ}C$ in two different specimen collection tubes; glass and polypropylene tubes. Three replicates for each condition with different temperature and types of a container were analyzed at five different time points over 21 days. When oral fluid samples were stored in glass tubes, the loss of both THC and THC-COOH was less than 10% at all room temperature, $-4^{\circ}C$ and $-20^{\circ}C$. However, in polypropylene tubes, the loss of both THC and THC-COOH increased significantly over the study period. In particular, the concentration of THC decreased more rapidly than that of THC-COOH at room temperature and the maximal percentage of THC lost was 90.3% after 21 days. The result indicates that it would be necessary to collect oral fluid samples in glass containers and cool the samples until analysis in order to prevent the degradation of analytes.

Characteristics of SrCo1-xFexO3-δ Perovskite Powders with Improved O2/CO2 Production Performance for Oxyfuel Combustion

  • Shen, Qiuwan;Zheng, Ying;Luo, Cong;Zheng, Chuguang
    • Bulletin of the Korean Chemical Society
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    • v.35 no.6
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    • pp.1613-1618
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    • 2014
  • Perovskite-type oxides are promising oxygen carriers in producing oxygen-enriched $CO_2$ gas stream for oxyfuel combustion. In this study, a new series of $SrCo_{1-x}Fe_xO_{3-{\delta}}$ (x = 0.2, 0.4, 0.6, 0.8) was prepared and used to produce $O_2/CO_2$ mixture gas. The phase, crystal structure, and morphological properties of $SrCo_{1-x}Fe_xO_{3-{\delta}}$ were investigated through X-ray diffraction, specific surface area measurements, and environmental scanning electron microscopy. The oxygen desorption performance of $SrCo_{1-x}Fe_xO_{3-{\delta}}$ was studied in a fixed-bed reactor system. Results showed that the different x values of $SrCo_{1-x}Fe_xO_{3-{\delta}}$ have no obvious effects on crystalline structure. However, the oxygen desorption performance of $SrCo_{1-x}Fe_xO_{3-{\delta}}$ is improved by Co doping. Moreover, $SrCo_{0.8}Fe_{0.2}O_{3-{\delta}}$ synthesized via a new EDTA method has a larger BET surface area ($40.396m^2/g$), smaller particle size (48.3 nm), and better oxygen production performance compared with that synthesized through a liquid citrate method.

Estimation of Coefficient of Consolidation Using Piezocone Dissipation Test in Normally Consolidated Clays (정규압밀점토에서의 피에조 콘 소산시험을 이용한 수평압밀계수의 산정)

  • 임형덕;이우진;김대규
    • Journal of the Korean Geotechnical Society
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    • v.19 no.5
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    • pp.145-154
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    • 2003
  • In this study, the variation in excess pore pressure during dissipation is estimated by using successive cavity expansion theory and finite difference technique based on axisymmetric uncoupled linear consolidation theory with separate consideration of magnitude and initial distribution $\Delta{u}_{oct}$induced by changes of octahedral normal stress, and $\Delta{u}_{shear}$ induced by changes of octahedral shear stress. The coefficient of consolidation is also estimated by trial and error procedure until the predicted dissipation curve matches the measured curve at a typical degree of dissipation. The proposed method is applied to the results of miniature piezocone tests at Louisiana State University calibration chamber system. Based on the results of interpretation and the comparison with experimental measurements and those from other solutions, the prediction dissipation curves show a good match with those measured during dissipation tests and the values of coefficient of consolidation estimated by proposed method are more close to the range of laboratory measurements than those of other theories.

Analysis of Thermodynamics in BiSrCaCuO Thin Films Fabricated by Using the i-beam sputtering method (i-beam 스퍼터링 법으로 제작한 BiSrCaCuO 박막의 열역학분석)

  • Kim, Tae-Gon;Park, yong-Pil
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.11 no.1
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    • pp.89-94
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    • 2007
  • High duality BiSrCaCuO thin films fabricated by using the i-beam sputtering method at various substrate temperatures, $T_{sub}$ and oxidation gas pressures, $pO_3$. The correlation diagrams of the BiSrCaCuO phases with Tsub and $pO_3$ are established in the 2212 and 2223 compositional films. In spite of 2212 compositional sputtering, Bi2201 and Bi2223 as well as Bi2212 phases come out as stable phases depending on $T_{sub}$ and $pO_3$. From these results, the thermodynamic evaluation of ${\Delta}H$ and${\Delta}S$, which are related with Gibbs' free energy change for single Bi2212 or Bi2223 phase, was performed.

A Study on Image Recognition based on the Characteristics of Retinal Cells (망막 세포 특성에 의한 영상인식에 관한 연구)

  • Cho, Jae-Hyun;Kim, Do-Hyeon;Kim, Kwang-Baek
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.11 no.11
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    • pp.2143-2149
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    • 2007
  • Visual Cortex Stimulator is among artificial retina prosthesis for blind man, is the method that stimulate the brain cell directly without processing the information from retina to visual cortex. In this paper, we propose image construction and recognition model that is similar to human visual processing by recognizing the feature data with orientation information, that is, the characteristics of visual cortex. Back propagation algorithm based on Delta-bar delta is used to recognize after extracting image feature by Kirsh edge detector. Various numerical patterns are used to analyze the performance of proposed method. In experiment, the proposed recognition model to extract image characteristics with the orientation of information from retinal cells to visual cortex makes a little difference in a recognition rate but shows that it is not sensitive in a variety of learning rates similar to human vision system.

The Clinical Significance of ${\gamma}{\delta}$ T lymphocytes in patients with pleural tuberculosis (결핵환자에서 말초혈액과 흉막액내 ${\gamma}{\delta}$ T 림프구의 의의)

  • Song, Kwang Seon;Shin, Kye Chul;Kim, Do Hun;Hong, Ae Ra;Kim, Hee Seon;Yong, Suk Joong
    • Tuberculosis and Respiratory Diseases
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    • v.44 no.1
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    • pp.44-51
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    • 1997
  • Background : The changes of the composition in the T-lymphocyte are important as an immunological abnormality in the pathogenesis of tuberculosis. Previously, the second type of TCR dimer(${\gamma}{\delta}$ T lymphocyte) that did not express CD4 or CD8 molecules was found. In other reports the presence of this type of lymphocytes was increased in the initial stage of tuberculous infections. Method : To determine whether there are some differences in the T-lymphocyte subsets in the peripheral blood or pleural effusion between pleural tuberculosis and other pleurisy. Thirty patients with pleural effusion among the forty-nine patients were examined T-lymphocyte subset analysis(CD4+T-cell,CD8+ T-cell,${\gamma}{\delta}$ T-lymphocytes) with anti- Leu4, anti-Leu3a, anti-Lea2a, anti HLA-DR and anti-TCR-${\gamma}{\delta}$-1(Becton & Dickinson Co.). Results : The average age of the patients was 50 years old(17-81year). There were 33 males and 16 female patients. Patiensts with tuberculosis are 30cases(tuberculous pleurisy 15), lung cancer 12cases(malignant effusion 9) and pneumonia 7cases(parapneumonic effusion 6cases) In T lymphocyte subsets of pleural effusion, helper T lymphocyte(54.6 + 13.8 %) of tuberculous pleurisy was higher than that(36.2 + 25.3 %) of non-tuberculous pleurisy(p=0.04). The peripheral blood ${\gamma}{\delta}$ T-lymphocytes in tuberculousis was insignificantly higher than non-tuberculous patients(p= 0.24). The peripheral blood ${\gamma}{\delta}$ T-lymphocytes and pleural ${\gamma}{\delta}$ T-Iymphocytes in tuberculous pleurisy was insignificantly higher than in non-tuberculous pleurisy(p= 0.16, p= 0.12). Conclusion : The percentage of -${\gamma}{\delta}$ T lymphocytes among the total T-lymphocytes is not significantly increased in the peripheral blood or pleural effusion of the pleural tuberculosis. ${\gamma}{\delta}$ T lymphocytes is less useful as a diagnostic method of pleural tuberculosis.

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High performance metal-only fan-beam reflectarray with a delta source applicable for an electromagnetic fence

  • Cho, Yong-Heui
    • International Journal of Contents
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    • v.7 no.4
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    • pp.44-49
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    • 2011
  • The scattering solutions for multiple rectangular metallic gratings in a perfectly conducting plane excited by the TE and TM delta sources are presented using an overlapping T-block method. A reflectarray composed of rectangular metallic gratings shows fanbeam radiation patterns that are useful for an electromagnetic fence. The scattering characteristics of multiple rectangular gratings were computed in terms of total radiated power and antenna directivity. The design method of a fan-beam reflectarray to obtain high directivity was also compared with superdirective radiation and parabolic reflector phase.

Design of Multivalued Logic Functions Using $I^2L$ Circuits ($I^2L$회로에 의한 다식논리함수의 설계)

  • 김흥수;성현경
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.22 no.4
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    • pp.24-32
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    • 1985
  • This paper presents the design method for multivalued logic functions using $I^2L$ circuits. First, the a비orithm that transforms delta functions into discrete functions of a truncated difference is obtained. The realization of multivalued logic circuits by this algorithm is discussed. And then, the design method is achieved by mixing discrete functions and delta functions using the modified algorithm for given multivalued truth tables. The techniques discussed here are easily extended to multi-input and multi-output logic circuits.

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