• 대한전기학회:학술대회논문집
• /
• 대한전기학회 2005년도 제36회 하계학술대회 논문집 C
• /
• pp.1915-1917
• /
• 2005

PZT(40/60) and PZT(60/40) powders, prepared by the sol-gel method, were mixed with an organic vehicle and the PZT(40/60)/PZT(60/40) heterolayered thick films were fabricated by the screen-printing method on $Pt/Al_2O_3$ substrates. The structural properties such as DTA, X-ray diffraction and microstructure, were examined as a function of the applied pressure. In the DTA analysis, the formation of the polycrystalline perovskite phase was observed at around $880^{\circ}C$. The average thickness of the PZT heterolayered thick films which were coated five times was approximately $95-100{\mu}m$.

• 대한전기학회:학술대회논문집
• /
• 대한전기학회 2005년도 제36회 하계학술대회 논문집 C
• /
• pp.1918-1920
• /
• 2005

PZT(20/80) and PZT(80/20) powders, prepared by the sol-gel method, were mixed with an organic vehicle and the PZT(20/80)/PZT(80/20) heterolayered thick films were fabricated by the screen-printing method on $Pt/Al_2O_3$ substrates. The structural properties such as DTA, X-ray diffraction and microstructure, were examined as a function of the sintering temperature. In the DTA analysis, the formation of the polycrystalline perovskite phase was observed at around $880^{\circ}C$. The average thickness of the PZT heterolayered thick films was approximately $80-90{\mu}m.$

• 한국전기전자재료학회논문지
• /
• 제14권6호
• /
• pp.460-465
• /
• 2001

(Ba$_{0.6-x}$Sr$_{0.4}$Ca$_{x}$)TiO$_3$(x=1.10,0.15,0.20) specimens were fabricated by the solid state reaction method and then the structural and dielectric properties as a function of he composition ratio and sintering temperature were studied. As a result of the differential thermal analysis(DTA), exothermic peak was observed at around 102$0^{\circ}C$ due to the formation of the polycrystalline perovskite phase. The BSCT(50/40/10) specimen sintered at 150$0^{\circ}C$ showed the highest average grain size(18.25${\mu}{\textrm}{m}$). The Curie temperature and dielectric constant at room temperature decreased with increasing Ca content. The dielectric constant and dielectric loss of the BSCT(50/40/10) specimen, sintered at 145$0^{\circ}C$, were about 4324 and 0.972% at 1KHz, respectively.ively.

• 한국군사과학기술학회지
• /
• 제14권6호
• /
• pp.1018-1025
• /
• 2011

The improved properties of corrosion for 90Cu10NiFe alloy in natural seawater were explained by sodium diethyl dithio carbamate(NaDDC), namely organic compound, which is reagent for heavy metal extractions of waste water. The efficiency of NaDDC as corrosion inhibitor for 90Cu10NiFe alloy has been investigated in seawater after immersion in various concentrations of NaDDC solutions for 12~36hrs at pH 8.2 by weight loss test and electrochemical techniques including potentiodynamic polarization and SEM-EDS measurements. The results showed that the corrosion resistance of 90Cu10NiFe alloy improves with the increasing concentration of NaDDC but it did not improves with increasing time any more, so the highest inhibition efficiency was 93% at 100mg/L, 36hrs. The results obtained from weight losses and corrosion rates in polarization curve measurements were in good agreement. Therefore, it showed that NaDDC is a good inhibitor for copper corrosion of 90Cu10NiFe alloy.

• 한국전기전자재료학회논문지
• /
• 제29권2호
• /
• pp.101-105
• /
• 2016

The basic characteristics of glass are highly fragile and brittle consequences the ultimate purpose of glass manufacturing is to make a transparent glass with complex shape. In order to solve this problem, mechanical properties of glass can be increased by crystallization of its amorphous glass. However, glass-ceramics has become opaque through crystallization process due to the distracted interface of glass by precipitated particles. This study has been investigated thermal processing conditions of LAS transparent glass-ceramic by using DTA (differential thermal analysis), in order to control size of precipitated particle and then fabricate transparent glass-ceramic. DTA indicated that crystallization peak area was declined with increased nucleation temperature. Subsequently, we have been established optimum temperature for crystallization depending on the nucleation temperature. The transmission and thermal expansion were measured after crystallization, and the size of precipitated particle was identified in range of 20~100 nm by FE-SEM. In addition, by setting the optimized crystallization condition, with high transmission and low thermal expansion glass was synthesized through this experiment.

• 분석과학
• /
• 제8권3호
• /
• pp.341-350
• /
• 1995

Melt-spinning법을 이용하여 $Nd_{14}Fe_{80}B_6$ 조성의 리본합금을 제조하고 각 제조조건별 시편에 대한 자기적 특성을 분석하였다. 리본합금의 미세구조와 자기적 특성은 냉각속도 및 열처리 조건에 민감하게 변화하였다. As-quenched 상태의 경우 wheel 속도 20m/sec에서 가장 좋은 자기적 특성을 나타내었으며, 비정질 상태의 리본시편에 대한 열처리 효과는 22m/sec에서 제조된 리본시편을 $600^{\circ}C$에서 30분간 진공열처리하였을 때 가장 좋은 결과를 얻을 수 있었다. 또한 $Nd_2Fe_{14}B$상의 결정화 온도는 DTA 분석결과 $595^{\circ}C$ 부근이었다.

• 한국산학기술학회논문지
• /
• 제22권1호
• /
• pp.372-378
• /
• 2021

방탄조끼는 전투원의 안전과 생명에 직결되는 군수품으로서, 방탄성능에 대한 요구조건의 충족여부가 무엇보다 중요하다. 우리 군에서는 방탄조끼의 요구 성능을 미 법무성 사업연구소(National Institute of Justice, NIJ)에서 발간한 NIJ STD-0101.06에서 규정하는 Level IIIA 수준으로 요구하고 있으며, 매 로트마다 수락시험을 진행하고 있다. 방탄성능을 평가하는 요소로 사격 시 관통여부 뿐만 아니라, 미 관통 시에도 후면 지지재료의 후면변형 기준인 44 mm 이하에 대한 충족여부도 고려하여 요구 성능에 대한 일치/불일치를 평가하고 있다. 후면변형은 지지재료의 물리적 성질과 탄속에 따른 충격량의 변화 등과 같이 다양한 시험요인이 시험 결과에 영향을 미치게 되는데, 본 연구에서는 이러한 외부인자의 영향성을 제거하기 위한 데이터 처리 시 분산분석을 도입하여 동일한 조건을 갖는 데이터를 추출 하였고, 이를 통해 방탄성능에 대한 분석을 수행하였다. 분석결과, 후면변형과 탄속, 환경처리 유/무 그리고 방호면적과의 상관관계를 확인하였을 뿐만 아니라, 로트별 후면변형 구간 추정을 통해서 양산 공정분석을 수행하였다. 이를 통해서 방탄성능평가에 대한 새로운 방법론을 제시하고, 향후 품질보증 관련 활동에 적용하기 위한 새로운 패러다임을 제시하고자 하였다.

• Elastomers and Composites
• /
• 제35권1호
• /
• pp.12-18
• /
• 2000

환경에 대한 관심과 정부의 규제 강화로 에폭시 코팅 산업 분야에서 발생되는 휘발성 유기 물질 방출을 최소화하기 위하여 꾸준히 기술 개발을 해오고 있다. 환경 친화적인 기술 개발의 일환으로 본 연구에서는 amine-epoxy adduct (AEA)형의 수용성 에폭시 경화제를 합성하였고, 그의 구조를 FT-IR, GPC, TG/DTA로 확인하였으며, 합성한 수용성 경화제를 이용하여 KER-828 그리고 KER-500과의 경화 물성을 비교 조사하였다. 실험 결과에 의하면 건조시간은 KER-828이 KER-500보다 빨랐으나 접착력 및 내 충격성은 KER-500이 우수하였다.

• 한국군사과학기술학회지
• /
• 제15권3호
• /
• pp.231-240
• /
• 2012

During the past two decades, Metal Injection Molding(MIM) has become a very competitive technology to fabricate small, precise and complex-shaped parts in large quantities. In this research, the applicability of MIM technology in the mass-production of the high precision fuze parts to save manufacturing cost was investigated. The water-atomized 17-4PH stainless steel powder, one of the best corrosion-resistant high strength materials, was injection-molded into real-shape fuze part and flat tensile specimens. The injection-molded parts were thermally debound in hydrogen gas flow without solvent extraction. Sintering of the debound parts was carried out in vacuum at temperatures ranging from $1150^{\circ}C$ to $1370^{\circ}C$. The sintering behavior, mechanical properties, dimensional precision, corrosion resistance of the MIMed 17-4PH stainless parts were investigated. It was found that almost all the properties of the MIMed parts were comparable to those of the mechanically machined parts. Also, actual military field tests using both MIMed and mechanically machined fuze parts were performed as well and were found to be very successful.

• 대한전기학회논문지:전기물성ㆍ응용부문C
• /
• 제49권1호
• /
• pp.8-12
• /
• 2000

The properties variation by deterioration of the 600V grade heat-resistant polyvinyl chloride insulated wire(HIV) was analyzed. The weight variation of the thermal deteriorated HIV was about 42% at 80$0^{\circ}C$ and over. From the analysis result of the metallurgical microscope photographs it shows that the sorface of normal wire showed the elongated structures. However the elongated structures did not appear at $900^{\circ} and over and we could observe that particles were grown. The grown oxidized substances in the thermally deteriorated electric wire were observed by SEM. The CuL, CuK, $CuK_b$, OK and CIK spectra of the thermally deteriorated HIV at $300^{\circ}C$ were uniform regardless of the scanning length, but the spectra of CIK could not found at above $700^{\circ}. At the DTA analysis, the endothermic reactions were occurred around $3006{\circ}C\; and\; 400^{\circ}C$ and the exothermic reactions were occurred around $470^{\circ}, respectively.