• 제목/요약/키워드: D-H Method

검색결과 4,310건 처리시간 0.033초

결정립크기와 집합조직제어를 통한 마그네슘 합금의 기계적 성질 개선 (Improvement of Mechanical Properties of Mg alloys through Control of Grain Size and Texture)

  • 김우진;이종범;김우영;정하국;박종덕
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2006년도 춘계학술대회 논문집
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    • pp.57-58
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    • 2006
  • The effects of lowering ECAP temperature during ECAP process and Post-ECAP annealing on microstructure, texture and mechanical properties of the AZ31 alloys have been investigated in the present study. The as-extruded materials were ECAP processed to 2 passes at 553K prior to subsequent pressing up to 6 passes at 523K or 493K. When this method of lowering ECAP temperature during ECAP was used, the rods could be successfully deformed up to 6 passes without any surface cracking. Grain refinement during ECAP process at 553K might have helped the material to endure further straining at lower deformation temperatures probably by increasing the strain accommodation effect by grain boundary sliding, causing stress relaxation. Texture modification during ECAP has a great influence on the strength of Mg alloys because HCP metals have limited number of slip systems. As slip is most prone to take place on basal planes in Mg at room temperature, the rotation of high fraction of basal planes to the directions favorable for slip as in ECAP decreases the yield stress appreciably. The strength of AZ31 Mg alloys increases with decrease of grain size if the texture is constant though ECAP deformation history is different. A standard positive strength dependence on the grain size for Mg alloys with the similar texture (Fig. 1) supports that the softening of ECAPed Mg alloys (a negative slope) typically observed despite the significant grain refinement is due to the texture modification where the rotation of basal planes occurs towards the orientation for easier slip. It could be predicted that if the original fiber texture is restored after ECAP treatment yielding marked grain refinement, yield stress as high as 500 MPa will be obtained at the grain size of ${\sim}1{\mu}m$. Differential speed rolling (DSR) with a high speed ratio between the upper and lower rolls was applied to alter the microstructure and texture of the AZ31 sheets. Significant grain refinement took place during the rolling owing to introduction of large shear deformation. Grain size as small as $1.4{\mu}m$ could be obtained at 423K after DSR. There was a good correlation between the (0002) pole intensity and tensile elongation. This result indicates that tensile ductility improvement in the asymmetrically rolled AZ31 Mg alloys is closely related to the weakening of basal texture during DSR. Further basal texture weakening occurred during annealing after DSR. According to Hall-Petch relation shown in Fig. 1, the strength of the asymmetrically rolled AZ31 is lower than that of the symmetrically rolled one when compared at the same grain size. This result was attributed to weakening of fiber texture during DSR. The DSRed AZ31, however, shows higher strength than the ECAPed AZ31 where texture has been completely replaced by a new texture associated with high Schmid factors.

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$^{90}Sr$ 방사성 동위원소를 이용한 전리함의 대기 보정계수 측정 (Air Density Correction of Ionization Chamber using $^{90}Sr$ Radioactive Check Device)

  • 박성용;김우철;신동오;지영훈;권수일;이길동;조영갑;노준규
    • Journal of Radiation Protection and Research
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    • 제23권4호
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    • pp.267-271
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    • 1998
  • 전리함을 사용한 흡수선량 측정시 대기 보정계수의 측정은 필수적인 요소이다. 일반적으로는 기압계 및 온도계를 이용하여 대기 보정계수를 얻고 있는데 본 실험에서는 $^{90}Sr$ 방사성 등위원소를 사용하여 보정계수를 얻고 그 값들을 비교하고자 한다. PTW 사의 Radioactive Check Device, Unidos Elecetrometer 및 0.6 co Ion Chamber를 이용하여 각각의 다른 환경 조건하에서 대기 보정계수를 구하고 온도계와 기압계를 사용하여 구한 대기 보정계수를 비교해 본 결과 그들은 0.2 % 이내로 잘 일치가 되었다. 이론적으로 온도계 및 기압계를 사용할 경우 전체 선량의 불확정도는 ${\pm}$1.2 - 1.6 % 인데 반하여 $^{90}Sr$ 방사성 동위원소를 사용할 경우 전체 선량의 불확정도는 ${\pm}1.02%$로 계산할 수 있다. $^{90}Sr$ 방사성 동위원소를 사용한 방법은 온도계 및 기압계의 정기적인 검교정이 없을 경우 발생할 수 있는 오차를 줄일 수 있으며 보다 정확한 보정계수를 얻을 수 있다.

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지지적 접촉과 환자교육이 수술후 동통에 미치는 영향에 관한 연구 (A Study on the Effects of Supportive Touch and Patient Educative on the Patient이s Post-operative Pain)

  • 김주희
    • 대한간호학회지
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    • 제15권3호
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    • pp.5-20
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    • 1985
  • The purpose of this study was to assess the value-of post-operative treatment in terms of nursing care in the allevation of pain. More specifically, the effects of supportive touch and patient education were examined. On the date before each patient's operation, the Bevels of anxiety, depression and affiliation were examined. The post-operative treatment was adminis. tered after an initial measurement of the patient's fain, according to the experimental category for the three days following the operation. On the final day, the level of anxiety and depression were again measured. The subjects of this study were 138 patient from the general surgical and gynecological wards in H university Hospital in Seoul. The study was conducted over a three-month period from June 24, 1984 to September 18, 1984. All patients had undergone laparatomies. Various standard instruments were used to measure the pain, anxiety, depression and affiliation levels. for pain, 5 grate Simple Descriptive Scale, and the Mclachlan four-range Observational Pain Scale were employed. For anxiety and depression, respectively the Spielberger State Anxiety Inventory and Beck Depression Inventory (B.D.I.) were used. Lastly, the affiliation was determined by the Mehrabian Affiliation Scale. The outcome of the research was as follows: 1. The first hypothesis concerning the existence of lower pain levels of Experimental Group A and Experimental Group B than the pain levels of Control Croup C was not supported. 2. The second hypothesis concerning the existence if lower anxiety levels of Experimental Group A and Experimental Group B than the anxiety levels of Control Group C was supported at the level of F=3.58 (p=.03). 3. The third hypothesis concerning the existence of lower depression levels of Experimental Group A and Experimental Group B than the depression levels of Control Group C was not supported. 4. The fourth hypothesis concerning the existence of different levels of pain in accordance with the levels of affiliation in Experimental Group A was not supported. 5. A positive correlation did exist between pain and anxiety after surgery (r=.34, p=.0001). Thus, the fifth hypothesis was supported. 6. A positive correlation did exist between pain and depression following surgery(r=.36, p=.0001). Thus, the sixth hypothesis was supported. Based on the above results, it was found that supportive touch and patient education either through human sources or via tape recorder do influence the anxiety of a patient after surgery, that a Positive correlation between pain, anxiety and deparession exist, that affiliation does not alter the influence of supportive touch, and that the graph on which pain levels were depicted indicates the possibility of development even if the effects of supportive touch did not reach a meaningful level. Thus it can be concluded that patient education, regardless of its form, is essential for the patient after surgery and that supportive touch, when reasonably modified and supplemented, can be an effective method of alleviating pain.

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란시아이트-다카네라이트 고용체 결정구조에 대한 분자동역학 시뮬레이션 연구 (A Molecular Dynamics Simulation Study of Ranciéite-takanelite Solid Solution Crystal Structures)

  • 한수연;권기덕
    • 광물과 암석
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    • 제33권1호
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    • pp.19-28
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    • 2020
  • 란시아이트(ranciéite)는 수화된 Ca2+ 양이온이 망간 원자 빈자리를 아래위로 덮고 층간을 채우고 있는 육방정계 층상형 산화망간광물(phyllomanganates)이다. 망간 원자 빈자리를 Mn2+ 양이온이 더 우세하게 채우는 경우, 다카네라이트(takanelite)라는 광물로 구분하며, 란시아이트와 다카네라이트는 서로 고용체를 이룬다. 이 광물들은 입자크기가 매우 작고 다른 광물과 함께 산출되기 때문에 실험만으로 정확한 결정구조를 규명하기 어렵다. 이번 연구에서는 층간 Mn2+/Ca2+ 양이온 비율에 따른 란시아이트-다카네라이트의 결정구조와 층간 구조를 규명하기 위해 고전분자동역학 시뮬레이션(molecular dynamics simulations; MD)을 수행하였다. 연구방법의 적합성을 판단하기 위해 결정구조가 잘 알려진 칼코파나이트 군(chalcophanite group) 광물들에 대해 시뮬레이션 계산을 수행 후 실험 결과와 비교하였다. 이후 층간 양이온 비율에 따른 란시아이트 및 다카네라이트 모델에 대한 MD 시뮬레이션을 수행하여 양이온 함량에 따른 양이온과 물 분자의 분포 및 (001)면간거리를 제시한다.

유한요소 해석을 이용한 정형용 흉·요추 보조기의 형태에 따른 생체역학적 분석 (Biomechanical Analysis of Different Thoracolumbar Orthosis Designs using Finite Element Method)

  • 김영현;전성철;정덕영;이성재
    • 재활복지공학회논문지
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    • 제6권1호
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    • pp.45-50
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    • 2012
  • 흉 요추 보조기는 후만증 관련 증상의 진행을 예방하고 통증을 완화시키기 위한 목적으로 노인성 후만증 환자의 재활을 위하여 이용되고 있다. 최근 다양한 형태의 흉 요추 보조기가 개발되고 있으나 생체역학적 효과에 관한 연구가 미흡한 실정이다. 따라서 본 연구에서는 세 가지 형태 (Type 1, one-connecting frame type; Type 2, two-connecting frame type; Type 3, all-in-one type)의 흉 요추 보조기와 몸통 (trunk)의 유한요소 모델을 구현하여 보조기 착용 후 운동성 변화에 따른 몸통에서의 압력 분포 및 보조기의 응력을 비교 분석하였다. 신전 운동 시 몸통에서 확인되는 압력의 분산은 일체형의 형태를 가지는 Type 3에 의해서 가장 고르게 이루어졌으며 connecting frame 형태의 Type 1과 Type 2의 압력 분포 패턴은 크게 차이가 나지 않았다. 보조기 착용에 따른 몸통의 운동성은 Type 2 ($11.3{\sim}13.9^{\circ}$), Type 1 ($12.1{\sim}15.4^{\circ}$)와 비교하여 Type 3 ($8.5{\sim}9.4^{\circ}$)에 의하여 가장 크게 제한되었다. 모든 Type의 보조기는 20% 미만의 파단 가능성을 보였다. 따라서, 보조기 착용에 따른 등압 분포 및 운동성의 결과로 미루어 볼 때, 일체형의 흉 요추 보조기가 후만증 환자 재활에 있어 높은 효과를 제공할 것으로 사료된다.

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효소분리 및 용매정제법으로 제조한 고농도 Sialic Acid(23%)가 함유된 GMP 가수분해분말의 마우스 골수세포의 소핵시험을 이용한 안전성 평가연구 (In Vivo Evaluation of the Safety of Hydrolyzed GMP Powder containing Highly Concentrated Sialic Acid (23%) produced by Enzyme Separation and Solvent Enrichment Method using Micronucleus Test in Mice)

  • 김희경;조향현;노혜지
    • Journal of Dairy Science and Biotechnology
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    • 제34권2호
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    • pp.83-89
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    • 2016
  • 본 시험물질인 GMP으로부터 sialic acid를 분리 및 이의 농도를 23%로 높게 정제한 GMP 가수분해물(23%-GNANA) 분말에 대해 발암성 유발 유 무 판단의 기초자료를 얻기 위하여 마우스 골수세포를 이용한 소핵시험을 실시하였다. 결과로서, 다염성 적혈구의 소핵출현 적혈구의 출현비율은 음성 대조군과 시험물질 투여군간 평균 차이의 유의성이 없었다(p<0.05). 또한 동물개체별로 관찰한 결과에서도 음성대조군과 시험물질 투여군간 유의성이 없었으며(p<0.05), 시험물질의 용량의존성 반응은 전체적으로 나타나지 않았다. 이러한 결과로 보아, GMP로부터 제조한 23%-GNANA는 고농도로 sialic acid가 농축되었을 뿐, 일반 식품인 GMP 수준에서 마우스 골수세포에 대해 소핵의 유발성이 없는 것으로 판단되었다.

Effects of Maturity at Harvest and Wilting Days on Quality of Round Baled Rye Silage

  • Kim, J.G.;Chung, E.S.;Seo, S.;Ham, J.S.;Kang, W.S.;Kim, D.A.
    • Asian-Australasian Journal of Animal Sciences
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    • 제14권9호
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    • pp.1233-1237
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    • 2001
  • A study was conducted to determine the effects of maturity at harvest and wilting days on the quality of round baled rye (Secale cereale L.) silage. This study was a $3{\times}3$ factorial arrangement in a split plot design with 3 replicates. The main plot was 3 harvesting dates at the stage of boot (20 Apr.), heading (29 Apr.) and flowering (14 May). The subplot was wilting day : 0 (unwilted), 0.5 and 1 day (0, 1, and 2 days at boot stage). Acid detergent fiber (ADF) and neutral detergent fiber (NDF) contents of rye silage were significantly greater than those of rye before ensiling, but crude protein (CP) content and in vitro dry matter digestibility (IVDMD) were vice versa. Buffering capacity (BC) of rye harvested at flowering stage was decreased from 264 to 202 meq/kg at 1 day wilting, however, it was increased when harvested at boot or heading stage. The pH in wilted silage was the highest while that of flowering stage was the lowest. Water soluble carbohydrate (WSC) content of wilting rye was lower than that of unwilted, and the lowest at late harvesting stage. All plots had minimal WSC content for silage fermentation. Wilting treatment and delayed harvesting date caused an increase in dry matter (DM) content of round bale silage. The content of ammonia-N expressed as a portion of total N showed negative correlation with DM content. High quality silage according to ammonia-N content could be obtained from mid-harvest with wilting. There were highly significant differences in each organic acid between harvesting dates and wilting periods. Acetic and butyric acid contents were increased with delayed harvesting and prolonged wilting period, the lactic acid content, however, was decreased. This study demonstrated that harvest of rye from heading to flowering stage with wilting would be a recommendable method for making high quality rye silage using round bale system.

Estimation of Genetic Parameters for Calving Ease by Heifers and Cows Using Multi-trait Threshold Animal Models with Bayesian Approach

  • Lee, D.H.
    • Asian-Australasian Journal of Animal Sciences
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    • 제15권8호
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    • pp.1085-1090
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    • 2002
  • Genetic parameters for birth weights (BWT), calving ease scores observed from calves born by heifers (CEH), and calving ease scores observed from calves born by cows (CEC) were estimated using Bayesian methodology with Gibbs sampling in different threshold animal models. Data consisted of 77,458 records for calving ease scores and birth weights in Gelbvieh cattle. Gibbs samplers were used to obtain the parameters of interest for the categorical traits in two univariate threshold animal models, a bivariate threshold animal model, and a three-trait linear-threshold animal model. Samples of heritabilities and genetic correlations were calculated from the posterior means of dispersion parameters. In a univariate threshold animal model with CEH (model 1), the posterior means of heritabilities for calving ease was 0.35 for direct genetic effects and 0.18 for maternal genetic effects. In the other univariate threshold model with CEC (model 2), the posterior means of heritabilities of CEC was 0.28 for direct genetic effects and 0.18 for maternal genetic effects. In a bivariate threshold model with CEH and CEC (model 3), heritability estimates were similar to those in unvariate threshold models. In this model, genetic correlation between heifer calving ease and cow calving ease was 0.89 and 0.87 for direct genetic effect and maternal genetic effects, respectively. In a three-trait animal model, which contained two categorical traits (CEH and CEC) and one continuous trait (BWT) (model 4), heritability estimates of CEH and CEC for direct (maternal) genetic effects were 0.40 (0.23) and 0.23 (0.13), respectively. In this model, genetic correlation estimates between CEH and CEC were 0.89 and 0.66 for direct genetic effects and maternal effects, respectively. These estimates were greater than estimates between BWT and CEH (0.82 and 0.34) or BWT and CEC (0.85 and 0.26). This result indicates that CEH and CEC should be high correlated rather than estimates between calving ease and birth weight. Genetic correlation estimates between direct genetic effects and maternal effects were -0.29, -0.31 and 0.15 for BWT, CEH and CEC, respectively. Correlation for permanent environmental effects between BWT and CEC was -0.83 in model 4. This study can provide genetic evaluation for calving ease with other continuous traits jointly with assuming that calving ease from first calving was a same trait to calving ease from later parities calving. Further researches for reliability of dispersion parameters would be needed even if the more correlated traits would be concerned in the model, the higher reliability could be obtained, especially on threshold model with property that categorical traits have little information.

Investigation of PCR-RFLPs within Major Histocompatibility Complex B-G Genes Using Two Restriction Enzymes in Eight Breeds of Chinese Indigenous Chickens

  • Xu, R.F.;Li, K.;Chen, G.H.;Qiang, B.Y.Z.;Mo, D.L.;Fan, B.;Li, C.C.;Yu, M.;Zhu, M.J.;Xiong, T.A.;Liu, Bang
    • Asian-Australasian Journal of Animal Sciences
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    • 제18권7호
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    • pp.942-948
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    • 2005
  • New polymorphism of major histocompatibility complex B-G genes was investigated by amplification and digestion of a 401bp fragment including intron 1 and exon 2 using polymerase chain reaction-restriction fragment length polymorphism (PCR-RFLP) technique with two restriction enzymes of Msp I and Tas I in eight breeds of Chinese indigenous chickens and one exotic breed. In the fragment region of the gene, three novel single nucleotide polymorphisms (SNPs) were detected at the two restriction sites. We found the transition of two nucleotides of A294G and T295C occurred at Tas I restriction site, and consequently led to a non-synonymous substitution of asparagine into serine at position 54 within the deduced amino acid sequence of immunoglobulin variable-region-like domain encoded by the exon 2 of B-G gene. It was observed at rare frequency that a single mutation of A294G occurring at the site, also caused an identical substitution of amino acid, asparagine 54-to-serine, to that we described previously. And the transversion of G319C at Msp I site led to a non-synonymous substitution, glutamine 62-to-histidine. The new alleles and allele frequencies identified by the PCR-RFLP method with the two enzymes were characterized, of which the allele A and B frequencies at Msp I and Tas I loci were given disequilibrium distribution either in the eight Chinese local breeds or in the exotic breed. By comparison, allele A at Msp I locus tended to be dominant, while, the allele B at Tas I locus tended to be dominant in all of the breeds analyzed. In Tibetan chickens, the preliminary association analysis revealed that no significant difference was observed between the different genotypes identified at the Msp I and Tas I loci and the laying performance traits, respectively.

Surface Characteristics of Type II Anodized Ti-6Al-4V Alloy for Biomedical Applications

  • 이수원;정태곤;양재웅;정재영;박광민;정용훈
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2017년도 춘계학술대회 논문집
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    • pp.77-77
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    • 2017
  • Titanium and its alloys offer attractive properties in a variety of applications. These are widely used for the field of biomedical implants because of its good biocompatibility and high corrosion resistance. Titanium anodizing is often used in the metal finishing of products, especially those can be used in the medical devices with dense oxide surface. Based on SAE/AMS (Society of Automotive Engineers/Aerospace Material Specification) 2488D, it has the specification for industrial titanium anodizing that have three different types of titanium anodization as following: Type I is used as a coating for elevated temperature forming; Type II is used as an anti-galling coating without additional lubrication or as a pre-treatment for improving adherence of film lubricants; Type III is used as a treatment to produce a spectrum of surface colours on titanium. In this study, we have focused on Type II anodization for the medical (dental and orthopedic) application, the anodized surface was modified with gray color under alkaline electrolyte. The surface characteristics were analyzed with Focused Ion Beam (FIB), Scanning Electron Microscopy (SEM), surface roughness, Vickers hardness, three point bending test, biocompatibility, and corrosion (potentiodynamic) test. The Ti-6Al-4V alloy was used for specimen, the anodizing procedure was conducted in alkaline solution (NaOH based, pH>13). Applied voltage was range between 20 V to 40 V until the ampere to be zero. As results, the surface characteristics of anodic oxide layer were analyzed with SEM, the dissecting layer was fabricated with FIB method prior to analyze surface. The surface roughness was measured by arithmetic mean deviation of the roughness profile (Ra). The Vickers hardness was obtained with Vickers hardness tester, indentation was repeated for 5 times on each sample, and the three point bending property was verified by yield load values. In order to determine the corrosion resistance for the corrosion rate, the potentiodynamic test was performed for each specimen. The biological safety assessment was analyzed by cytotoxic and pyrogen test. Through FIB feature of anodic surfaces, the thickness of oxide layer was 1.1 um. The surface roughness, Vickers hardness, bending yield, and corrosion resistance of the anodized specimen were shown higher value than those of non-treated specimen. Also we could verify that there was no significant issues from cytotoxicity and pyrogen test.

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