• Restorative Dentistry and Endodontics
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• v.20 no.2
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• pp.487-507
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• 1995

Composite resin repair requires strong bond strength between the new and old materials. The objective of the current study was to identify the optimal treatments for sufficient bond strengths. Bondings between same kinds of materials and cross bondings using chemical curing composites and light curing composites were tested. Surface treatments included the methods of sand-blasting, acid etching and coating of bonding agent. Seven kinds cases of combinations from three kinds of methods were experimented and compared with a control group of which surfaces were highly polished. Measurements of shear bond strength and observations of surface morphologic changes using a scanning electron microscope were done. Following conclusions were drawn : 1. The highest bond strength among composite resins were exhibited by the treatment of the sand-blasting and the coating of bonding agent. 2. Acid etched surfaces showed the lowest bond strength. Bond strengths obtained from experimental groups including acid etching were lower than those obtained from same kinds of experimental groups without acid etching. 3. Simple method of the coating of bonding agent produced the slightly increased bond strength on chemical curing composite and reduced bond strength on light curing composite. 4. Bonding surfaces of chemical curing composite resin showed slightly higher bond strengths than light curing composite resin, however significant differences were not confirmed statistically. 5. More significant irregular surfaces were created by sand-blasting method than acid etching method. 6. A principal component of fillers of both resins was silicon. Acid etching method produced the seperations and degradations of fillers, these were significant on light curing composite resins which containing barium fillers.

• Journal of the Korea Institute of Building Construction
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• v.9 no.6
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• pp.113-119
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• 2009

This study is to investigate the fundamental and fireproof qualities of high strength concrete corresponding to changes in the curing factors and the PP fiber ratio. The results were as follows. For the fundamental characteristics of concrete, the fluidity was reduced in proportion to the increase in the PP fiber ratio. The compressive strength was somewhat reduced according to an increase in the PP fiber ratio. However, it had the high strength scope of more than 60 MPa at 7 days and of more than 90 MPa at 28 days. On the spalling mechanism followed by changes of the water content ratio, spalling was prevented in all combinations, except the specimen without PP fiber and subjected to 3.0% of moisture contents. When spalling was prevented at that time, the residual compressive strength ratio was 22%~41% and the mass reduction ratio was 5%~7%, which was relatively favorable. As the spalling mechanism corresponds to changes in the curing method, spalling was prevented in concrete with a PP fiber mixing ratio of more than 0.05% in the event of standard curing, and in concrete with a PP fiber mixing ratio of more than 0.10% in the case of steam curing and autoclave curing. In these cases, when spalling was prevented, the residual compressive strength ratio was 23~42% and the mass reduction ratio was 7~11%. In these results, the ease of spalling prevention in high strength concrete was inversely proportional to the water content ratio. Depending on the curing method, spalling was prevented in concrete with over 0.05% PP fiber with standard curing and in concrete with over 0.1% PP fiber with steam curing and autoclave curing.

• Composites Research
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• v.37 no.1
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• pp.15-20
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• 2024

Since the residual stress of hydrogen tank is directly related to durability, it is very important to reduce it for safety. Type II~IV hydrogen tank are manufactured by the filament winding method, in which the fiber is impregnated with resin and wound around the liner. Residual stress in composite is affected by curing conditions and fiber tension etc. In this study, the effect of curing conditions on residual stress was analyzed when manufacturing a Type III hydrogen tank using carbon fiber filament winding process. First, the curing behavior of the epoxy resin was analyzed using a differential scanning calorimetry. Through this, the curing temperature was set to 140℃. During the same curing time, the specimens were cured under 2-stage curing condition that reached 140℃ earlier and a 4-stage curing condition that reached 140℃ later, respectively. After curing, the residual stress of the composite material was measured by the ring slitting method, and the experimental values were compared with numerical values. It was confirmed that there was a significant difference in residual stress according to the optimization of curing conditions.

• Composites Research
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• v.13 no.4
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• pp.42-53
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• 2000

A study has been made to establish an optimum condition in the surface treatment and curing method that is important for the fabrication of Al 7075/CFRP laminates. PAA(Phosphoric Acid Anodizing) provided a good adhesive strength and FPL(Sulfuric / Sodium Dichromate Acid Etching) had a similar adhesive strength with PAA. On the other hand, the poor adhesive strength was shown on vapor degrease and CAA(Chromic Acid Anodizing). By using the atomic force microscope(AFM), it was found that the PAA oxide surface obviously had a greater degree of microroughness as compared to vapor degrease, CAA and FPL treated surfaces. These results support the concept of a mechanical interlocking of the adhesive with-in the oxide pores as the predominant adhesion mechanism. In curing methods, the adhesive strength of co-curing method was higher than that of secondary curing method. With respect to stability of specimen shape, the secondary curing method was better than co-curing method. DMA(Dynamic Mechanical Analysis) test revealed $T_g$ in curing times over 60 min is nearly same, so it is estimated they will have similar degree of curing and joint durability in using FM300M adhesive film.

• Restorative Dentistry and Endodontics
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• v.25 no.1
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• pp.91-108
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• 2000

Most of cervical abrasion and erosion lesions show gingival margin where the cavosurface angle is on cementum or dentin. Composite resin restoration of cervical lesion shrink toward enamel margin due to polymerization contraction. This shrinkage has clinical problem such as microleakage and secondary caries. Several methods to diminish contraction stress of composite resin restoration, such as modifying cavity form and building up restorations in several increments have been attempted. The purpose of this study was to compare polymerization contraction stress of composite resin in Class V cavity subjected to cavity forms and placement methods. In this study, finite element model of 5 types of Class V cavity was developed on computer tomogram of maxillary central incisor. The types are : 1) Box cavity 2) Box cavity with incisal bevel 3) V shape cavity 4) V shape cavity with incisal bevel 5) Saucer shape cavity. The placement methods are 1) Incisal first oblique incremental curing 2) Bulk curing. An FEM based program for light activated polymerization is not available. For simulation of curing dynamics, time dependent transient thermal conduction analysis was conducted on each cavity and each placement method. For simulation of polymerization shrinkage, thermal stress analysis was performed with each cavity and each placement method. The time-temperature dependent volume shrinkage rate, elastic modulus, and Poisson's ratio were determined in thermal conduction data. The results were as follows : 1. With all five Class V cavifies, the highest Von Mises stress at the composite-tooth interface occurred at gingival margin. 2. With box cavity, V shape cavity and saucer cavity, Von Mises stress at gingival margin of V shape cavity was lower than the others. And that of box cavity was lower than that of saucer cavity. 3. Preparing bevel at incisal cavosurface margin decreased the rate of stress development in early polymerization stage. 4. Preparing bevel at incisal cavosurface margin of V shape cavity increased the Von Mises stress at gingival margin, but decreased at incisal margin. 5. At incisal margin, stress development by bulk curing method was rapid at early stage. Stress development by first increment of incremental curing method was also rapid but lower than that by bulk curing method, however after second increment curing final stress was the same for two placement methods. 6. At gingival margin, stress development by incremental curing method was suddenly rapid at early stage of second increment curing, but final stress was the same for two placement methods.

• Journal of the Korean Society of Industry Convergence
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• v.26 no.4_2
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• pp.629-637
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• 2023

This study aimed to evaluate the effect of post-curing equipment and time on the flexural strength of 3D printing resins produced by a liquid crystal display(LCD) printer. The three 3D printing resins(DENTCA Denture Teeth, DT; C&B 5.0 hybrid, CH; C&B Permanent A2, CP) were divided into four groups according to post-curing time(10 min and 30 min) and equipment with or without vacuum treatment. For the three-point flexural strength test and biaxial strength test were prepared by method according to ISO 10477, ISO 6872, respectively. Flexural strength was measured with universal testing machine. Comparison between post-curing time of each post-curing equipment was analyzed by independent sample t-test and Mann-Whitney U test(α=.05), and comparison between groups according to each 3D printing resin was performed by Kruskal-Wallis test and post-hoc by Bonferroni-Dunn test(α=.05). The flexural strength of the resin post-curing under vacuum was higher than that of the resin post-curing in air. In the comparison according to the post-curing time, in the case of the post-curing equipment without vacuum, the 30 minute curing time showed significantly higher flexural strength than the 10 minute curing time, except for the biaxial flexural strength of CH(P<.05). In the post-curing equipment with vacuum, the three-point flexural strength of all 3D printing resins(DT, CH, and CP) showed a higher value at 30 minute curing time than at 10 minute curing time.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2019.11a
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• pp.27-28
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• 2019

In this study, the characteristics of compressive strength of ultra high strength concrete supplied with moisture from outside by vacuum water absorbing curing method were investigated. Specimens were prepared by replacing the binder(Silifa fume and GGBS) by 25 wt% with respect to the weight of cement at W/B 0.16. Each specimen was subjected to water Vacuum absorbing curing time 0 min, 30 min, 60 min, 90 min and 120 minutes immediately after the demolding. Curing was performed at $20^{\circ}C$ Air-dry curing, $90^{\circ}C$ steam curing, $90^{\circ}C$ steam curing and $180^{\circ}C$ autoclave curing. Experimental results showed that water absorbing degree increased with increasing water absorbing curing time, and BS25 sample had higher water absorbing degree than SF25 sample at same time. Compressive strength tended to increase up to about 40% in water absorbing degree, but compressive strength decreased again in water absorbing more than 40%.

• Proceedings of the Korea Concrete Institute Conference
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• 1996.10a
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• pp.24-30
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• 1996

Nowadays, Government is modifying envioronment regulatons, but PC factories, having been constructed in 1990, are running out heavy cost in disposal of waste concrete, and hardly studying how accelerator curing method affects in compressive strength. In this study, possibility that waste concrete, produced in PC factory, can be used in PC products, is reviewed, and them captures strength characteristics by curing method. The results can be summed as follows. In order to recycle concrete the mix ratio of recycled aggregate to 50 percent of less than must decrease also in summer of four seasons strength gap by curing method is very small.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2009.11a
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• pp.117-120
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• 2009

It has been gradually increased with the use of resin based membrane forming agent for curing method, which plays a role in protecting moisture evaporation by forming resin membrane at the surface of concrete. In this paper, tests were carried out to examine moisture retention capability of cement mortar applying membrane forming agent. Dosages and types of the membrane forming agent were varied. It is found that sheet curing sealed with the surface of concrete closely has favorable moisture retention capability. However, the application of membrane forming curing method had superiority in moisture retention capability at early stage but at later age, its capability is deteriorated. Hence, further study regarding altering application method was necessary to secure enhanced moisture retention capability.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2020.11a
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• pp.109-110
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• 2020

In This study, we tried to review an efficient curing method in consideration of safety and constructability among the problems of winter construction. In other words, as a result of the mock-up test, the measured value of carbon monoxide was 0 ppm in the case of an electric hot air fan. Since there is no carbon monoxide, problems such as suffocation are expected to be solved. In terms of temperature characteristics, electric hot air fans exhibited high thermal efficiency performance with a slight difference in upper/lower temperatures compared to the existing ones. In the future, we plan to conduct thermal efficiency evaluation through actual site performance verification. We will propose an efficient curing method through applicability evaluation.