• 한국표면공학회지
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• 제48권5호
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• pp.205-210
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• 2015

NbN coatings were prepared by ICP (inductively coupled plasma) assisted magnetron sputtering from a Nb metal target in $Ar+N_2$ atmosphere at various ICP powers. Effect of ICP on the microstructure, crystalline structure and mechanical properties of NbN coatings was investigated by field emission electron microscopy, X-ray diffraction, atomic force microscopy and nanoindentation measurements. The results show that ICP power has a significant influence on coating microstructure, structure and mechanical properties of NbN coatings. With the increasing of ICP power, coating microstructure evolves from the columnar structure of DC process to a highly dense one. Crystalline structure of NbN coatings were changed from cubic ${\delta}$-NbN to hexagonal ${\beta}-Nb_2N$ with increase of ICP power. The maximum nano hardness of 25.4 GPa with Ra roughness of 0.5 nm was obtained from the NbN coating sputtered at ICP power of 200 W.

• 산업기술연구
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• 제21권B호
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• pp.141-147
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• 2001

For the preparation of calcium carbonate particles from aqueous $Ca(OH)_2$ slurry, carbonation reaction of aqueous $Ca(OH)_2$ slurry was carried out by batch method the $CO_2$ into reactor filled with aqueous slurry of $Ca(OH)_2$. The concentration of $Ca(OH)_2$ varies from 1.00 to 7.00wt%, reactor temperature at 20 and $40^{\circ}C$, and reactor pressure from atmospheric pressure to $6.0kg_f/cm^2$. Crystal structure of calcium carbonate was of calcite, the particle size were about $0.05{\sim}2.0{\mu}m$, and the particle shape was cubic and spindle. When reactor temperature was higher, particle size of calcium carbonate was bigger and particle shape was varied, but reaction rate was increased. When reactor pressure was higher, particle size of calcium carbonate was smaller, particle shape was cubic, and reaction rate was increased.

• 대한기계학회논문집B
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• 제28권6호
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• pp.672-681
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• 2004

Direct numerical simulation was carried out to study the vortical structures of the flow around a wall-mounted cube in a channel at Re=1,000 and Re=3,500 based on cubic height and bulk mean velocity. The cubic obstacle is situated in the entrance region of the channel flow where the boundary layers are developing. Upstream of the obstacle, steady and unsteady laminar horseshoe vortex systems are observed at Re=1,000 and Re=3,500, respectively; the near-wake flow is turbulent in both cases. The flow separates at each leading sharp edge of the cube, and subsequent vortex roll-up is noticed in the corresponding free-shear layer. The vortex shedding from the upper leading edge (upper vortices) and that from the two lateral leading edges (lateral vortices) are both quasi-periodic and their frequencies are computed. The upper and lateral vortices further develop into hairpin and Λ vortices, respectively. A series of instantaneous contours of the second invariant of velocity gradient tensor helps us identify spatial and temporal behaviors of the vortices in detail. The results indicate that the length and time scales of the vortical structures at Re=3,500 are much shorter than those at Re:1,000. Correlations between the upper and lateral vortices are also reported.

• 한국세라믹학회지
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• 제32권8호
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• pp.915-921
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• 1995

The morphotropic phase boundary and phase transitions of the solid solutiion system, (1-x)(Na1/2Bi1/2)TiO3-PbTiO3＋xPbTiO3 were studied by investigating changes in crystal structure, variations in permittivity with temperature, and calorimetric behavior. It was observed that the morphotropic phase boundary (MPB) of this solid solutiion system was at near 14 mol% of PbTiO3. Compositions containing less than 10mol% PbTiO3 (x<0.1) exhibited a phase transition, i.e. ferroelectric rhombohedrallongrightarrowparaelectric paraelectric cubic, with increasing temperature. Composition containing more than 14 mol% PbTiO3 (x 0.14) showed a phase transition from ferroelectric tetragonal to paraelectric cubic. In the composition range of 0.1$\varepsilon$ (T) curve, which coincided with a phase transition from ferroelectric rhombohedral to an intermediate phase, was also found.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2000년도 춘계학술대회논문집A
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• pp.148-152
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• 2000

The aluminum alloy 6061-T6 has been successfully used in structural applications especially the pressure vessel of the Advanced Neutron Source research reactor. And aluminum alloys, including 6061-T6, have a face-centered-cubic crystals structure. Under normal circumstances face-centered-cubic crystal structures do not exhibit cleavage fractures even at very lo9w temperatures. In aluminum-based structures, plates frequently find use as connecting links. Mechanical fasteners are often utilized in instances where ease of application, familiarity with fabrication processes, and severe dynamic loading are of concern. Plates frequently find use as connecting elements in structures built from aluminum alloys. Many structural elements employ mechanical fasteners. Twenty and twenty aluminum alloy 6061-T6 plates, representing four different bolt patterns, were mechanically deformed. And variable materials such as A1 6061-T6, Al 2024-T3, Carbon/Epoxy, Glass/Epoxy Composite and Woven fiber composite, are used as patch materials. From this experiment, it has been shown that the strength of patch-repaired specimens is different with the patch materials.

• 한국항행학회논문지
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• 제11권2호
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• pp.209-216
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• 2007

본 논문에서는 보행 로봇의 자세 안정화 및 동적 걸음새를 구현하였다. 10개의 RC 서보모터가 로봇 관절에 사용되었고, 각 로봇의 관절은 어떤 걸음새 동작에도 충분히 움직일 수 있게 하였다. 각 관절 궤적은 3차 스플라인 보간법에 의해 생성되며, 궤적의 안정성은 로봇 모델링에 의한 ZMP(Zero Moment Point)를 이용하여 입증하였다. 또한 복잡한 구조와 표현을 피하기 위해 각 가속도를 이용한 ZMP방법을 구현 하였고, 로봇의 안정 상태를 측정하기 위해 기울기 센서와 자이로 센서가 사용되었다. 10개의 서보모터 제어, 궤적 생성, ZMP 보상, 센서 측정 등 과 같은 대부분의 계산 과정은 DSP에서 이루어지며, PC에서는 단순히 로봇의 상태, 데이터 처리 등의 모니터링에 이용하였다.

• 대한기계학회논문집B
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• 제25권12호
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• pp.1861-1868
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• 2001

Vortical structures in the near-wake region of a cubic obstacle are studied using numerical simulation. We consider flow between two parallel plates with a cube mounted on one of the plates. In the turbulent near-wake region of the flow, coherent structures such as hairpin vortices are found. Quasi-periodic behavior of the hairpin vortices is noticed; its dimensionless frequency at Re=1,000 is about 0.82 which is consistent with the result of Elavarasan of et al.'s experiment [Fluid Dyn. Research, 2000, 27] although their geometry is somewhat different from on. In the case of Re=3,500, the dimensionless frequency of the hairpin vortex is about 1.60. It is observed that the translating speed of the head of the hairpin vortex is lower than the streamwise mean velocity at that location. In the vicinity of the lower plate downstream of the cube, various length scales are identified thus less coherent. However, it is noticed that the vortical structures become gradually elongated downstream of the new reattachment.

• 공업화학
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• 제4권2호
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• pp.342-348
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• 1993

1473 K, 대기압하에서 $Sm_{1-x}Sr_xFe^{3+}{_{1-t}}Fe^{4+}{_t}O_{3-y}$ ($0.00{\leq}x{\leq}1.00$) 페라이트계에 대하여 균일상의 시료를 제조하였다. x값의 증가에 따라 $Fe^{4+}$ 이온의 양이 증가하였으며 결정학적 구조는 orthorhombic에서 cubic으로 변화함을 알 수 있었다. $Fe^{4+}$ 이온의 증가에따라 일정온도에서의 전기전도도는 급격히 증가하며, 활성화에너지는 감소한다. x=0.00 시료의$M{\ddot{o}}ssbauer$ spectrum은 six-line 형태를 보이며 팔면체 자리에 $Fe^{3+}$ 이온이 존재함을 확인시켜 주었다.

• 한국진공학회지
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• 제1권1호
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• pp.88-95
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• 1992

고분해능 저에너지 전자회절법(HRLEED)을 이용하여 O/W(110) 표면의 산소흡착층 의 정돈된 p(2 $\times$ 1) 구조가 보이는 2차원 연속적인 상전이계에관한 임계지수 연구를 보고 한다. 이 구조의 (1/2 0) 초격자 회절점의 세기 및 모양을 온도에 대한 함수로 구하여 Tc=708.765K에서 감수율 및 요동상관거리가 차수법칙(power law)에 따르는 발산을 보이는 것이 관측되었다. 이로부터 구한 임계지수는 $\beta$=0.19$\pm$0.05, $\Upsilon=1.48pm$0.34, v=1.23$\pm$0.27 그 리고 η=0.38$\pm$0.12이다. 이들 비보편성을 갖는 임계지수들은 이 계를 지배하는 입방이방성 (cubic anisotropy)를 갖는 2차원 XY 모델로 이해된다.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2012년도 제42회 동계 정기 학술대회 초록집
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• pp.589-589
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• 2012

Indium sulfide thin films have been grown onto glass substrates using radio frequency magnetron sputtering at room temperature. The as-deposited film were annealed in nitrogen atmosphere at different temperatures of 100, 200, 300, 400 and $500^{\circ}C$ with an 1 h annealing time. The effect of annealing temperature on composition, structure, morphology and optical properties of the as-grown In2S3 films has been studied. The XRD results indicate that the as-deposited films are composed by a mixture of both cubic ${\alpha}$ and ${\beta}$ crystalline phases, with some fraction of tetragonal phase. The thermal annealing on the films produces the conversion of the cubic crystalline phases to the tetragonal ${\beta}$ one and a crystalline reorientation of the latter phase. The surface morphological analysis reveals that the films grown at $300^{\circ}C$ have an average grain size of ~ 58 nm. These films show a S/In ratio of 0.99. The optical band gap is found to be direct and the films grown at $300^{\circ}C$ shows a higher optical transmittance of 80% and an energy band gap of 2.52 eV.