• 한국재료학회지
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• 제28권2호
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• pp.89-94
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• 2018

The properties of 18 K red gold solder alloys were investigated by changing the content of In up to 10.0 wt% in order to replace the hazardous Cd element. Cupellation and energy dispersive X-ray spectroscopy (EDS) were used to check the composition of each alloy, and FE-SEM and UV-VIS-NIR-Colormeter were employed for microstructure and color characterization. The melting temperature, hardness, and wetting angle of the samples were determined by TGA-DTA, the Vickers hardness tester, and the Wetting angle tester. The cupellation result confirmed that all the samples had 18K above 75.0wt%-Au. EDS results showed that Cu and In elements were alloyed with the intended composition without segregation. The microstructure results showed that the amount of In increased, and the grain size became smaller. The color analysis revealed that the proposed solders up to 10.0 wt% In showed a color similar to the reference 18 K substrate like the 10.0 wt% Cd solder with a color difference of less than 7.50. TGA-DTA results confirmed that when more than 5.0 wt% of In was added, the melting temperature decreased enough for the soldering process. The Vickers hardness result revealed that more than 5.0 wt% In solder alloys had greater hardness than 10.0 wt% Cd solder, which suggested that it was more favorable in making a wire type solder. Moreover, all the In solders showed a lower wetting angle than the 10.0 wt% Cd solder. Our results suggested that the In alloyed 18 K red gold solders might replace the conventional 10.0 wt% Cd solder with appropriate properties for red gold jewelry soldering.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2009년도 춘계학술대회 논문집
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• pp.266-269
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• 2009

Iron-based soft magnetic materials are widely used as cores, such as transformer transformers, motors, and generators. Reducing losses generated from soft magnetic materials of these applications results in improving energy conversion efficiency. Recently, the new P/M soft magnetic material realized an energy loss of 68 W/kg with a drive magnetic flux of 1 T, at a frequency of 1 kHz, rivaling general-purpose electromagnetic steel sheet in the low frequency range of 200 Hz to 1 kHz. In this research, the effect of rolling parameters on soft magnetic properties of Fe-based powder cores was investigated. The Fe-based soft magnetic plates were produced by the hot powder rolling process after both pure Fe and Fe-4%Si powders were canned, evacuated, and sealed in Cu can. The soft magnetic properties such as energy loss and coercive power were measured by B-H curve analyzer. The soft magnetic properties of rolled sheets were measured under conditions of a magnetic flux density of 1 T at a frequency of 200 kHz. It was found that rolling reduction ratio is the most effective parameter on reducing both energy loss and coercivity because of increasing aspect ratio with reduction ratio. By increasing aspect ratio from 1 to 9 through hot rolling of pure Fe powder, a significant loss reduction of one-third that of SPS sample was achieved.

• 한국분말재료학회지
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• 제11권5호
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• pp.412-420
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• 2004

The purpose of the present study is to determine an optimum composition using cheaper powders keeping with high performance of hard rock cutting diamond saw blade. With 50Fe-20(Cu . Sn)-30Co specimen, a part of Co was replaced by Ni(5%, 10%, and 15%, respectively). These specimens were hot pressed and sintered for predetermined time at various temperature. Sintering is performed by two different methods of temperature controlled method and specimen dimension controlled method. In order to determine the property of the sintered diamond saw blade, 3 point bending tester, X-ray diffractometer, and SEM were used. As the Co in the bond alloy was replaced by Ni, the hardness of the specimen increased. Thus the 50Fe-20(CuㆍSn)-15Co-15Ni specimen showed the maximum hardness of 104(HRB). The results of 3 point bending test showed that flexure strength decreased along with increase in Ni content. This is attributed to the formation of intermetallic compound(Ni$_{x}$Sn) determined by X-ray diffraction. The fracture surface after 3 point bending test showed that diamond was fractured in the specimen containing 0%, 5%, and 10%Ni, and the fracture occurred at the interface between diamond and matrix in the specimen containing 15%Ni. The cutting ability test showed that the abrasive property was not changed in the specimen containing 0%, 5%, and 10%Ni. The optimum composition determined in this study is 50Fe-20(CuㆍSn)-20Co-10Ni.

• 한국정보통신학회논문지
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• 제13권12호
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• pp.2662-2670
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• 2009

반사기 형태에 따른 경사진 빗살무늬 변환기 SAW 필터 특성을 비교하기 위해 모의실험을 통해 Langasite 기판위에 전극을 형성시켰으며, 전극재료로는 Al-Cu를 사용하였다. 모의실험을 바탕으로 입력단에는 IDT를 직렬형태로 연결시킨 block 형태로 하중을 가하는 전극 방법을 쓰고 출력단은 withdrawal 형태로 하중을 가하는 방법을 써서 제작하였다. 이를 바탕으로 광대역의 SAW 필터 전극 설계 방식에 대한 적절한 위상조건도 얻고자 시도하였다. Langasite 기판위에 형성시킨 입 출력빗살무늬 변환기 전극수는 50쌍, 두께는$5000{\AA}$으로 하였으며, 반사기 폭과 간격은 각각 $3.6{\mu}m$ 및 $2.0{\mu}m$으로 하였다. 제작한필터의 주파수 특성은 중심주파수가 대략 190MHz정도, 대역폭은 8.0MHz 정도로 측정되었으며, matching 후 return-loss는 -16dB 이하이고, 리플 특성은 4dB 정도이며, 반사에 의한 잔향은 -20dB 이하로 측정되었다.

• 한국주조공학회지
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• 제17권4호
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• pp.347-355
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• 1997

It is well known that the coarse primary Si in hypereutectic Al-Si alloys deteriorate castability, machinability, and mechanical properties. So, many treatment has been tried to refine the primary Si increasing cooling rate and adding refinement agent. Therefore. the purpose of our work was the observation of the effect on the refinement of primary Si and the analysis of the trend to apply to the casting process by changing the amount of P addition and the cooling rate while fixing the temperature at $750^{\circ}C$ of P addition and the type of AlCuP. In the condition of amount of P addition was fixed, primary Si was finer as cooling rate increased but in case of cooling rate was fixed, the effect of refinement was resisted as incersed the amount of P addition. At a relatively slow cooling rate of $22^{\circ}C/sec$, refinement was governed by the amount of P addition rather than cooling rate. At elevated cooling rate of $51^{\circ}C/sec$ and $99^{\circ}C/sec$, the undercooling due to faster cooling rate promoted nucleation of primary Si rather than P addition more significantly.

• 한국정보통신학회논문지
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• 제8권3호
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• pp.686-693
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• 2004

WCDMA용 SAW 필터를 제작하기 위하여 mathematica package를 이용한 모의 실험기를 개발하였으며, 전극재료로는 Al-Cu를 사용하였다. 모의실험한 자료를 바탕으로 전극에서 발생하는 ultimate rejection을 줄이기 위해 SFIT형태의 필터를 설계 및 제작하였다. 회절에 의한 현상을 최소화하기 위해 필터의 입력단은 block weighted IDT 형태로, 출력단은 withdrawal weighted IDT형태로 구성하였다. Langasite 기판위에 형성시킨 입 출력 빗살무늬 변환기 전극 수는 50쌍, 두께와 폭은 5000$\AA$와 1λ4(((equation omitted) 3.6$\mu\textrm{m}$)로 하였으며, IDT 전극 폭과 전극간격 은 각각 1λ/16와 1λ/8로 하였다. 제작한 SAW 필터의 특성은 중심주파수는 190MHz, 통과대역은 4MHz이며 저지대역은 -60dB이하로 측정되었다.

• Transactions on Electrical and Electronic Materials
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• 제1권2호
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• pp.32-37
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• 2000

Effect of alloying element additions to Ag on thermal conductivity and electrical conductivity of sheath materials for Bi-Pb-Sr-Ca-Cu-O(BSCCO) tapes has been characterized. The thermal conductivity at low temperature range (10~300K) of Ag and Ag alloys were evaluated by both direct and indirect measurement techniqueas and compared with each other, It was observed that the thermal conductivity decreases with increasing the content of alloying element such as Au, Pd and Mg. Thermal conductivity of pure Ag at 3 0K was measured to be 994.0 W(m.K) on the other hand, the corresponding values of $Ag_{0.9995}Mg_{0.0005}$, $Ag_{0.974}$, $Au_{0.025}$, $Mg_{0.001}$, $Ab_{0.973}$, $Au_{0.025}$, $Mg_{0.002}$ and $Ag_{0.92}$, $Pb_{0.06}$, $Mg_{0.02}$ were 342.6, 62.1, 59.2 and 28.9 W(m.K), respectively, indicating 3 to 30 times lower than that of pure Ag. In addition, the thermal conductivity of pure Ag measured by direct and indirect measurement techniques was 303.2 and 363.8 W(m.K) The difference in this study is considered to be within an acceptable error range compared to the reference data.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2009년도 제38회 동계학술대회 초록집
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• pp.277-277
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• 2010

The capacity of the carbonaceous materials reached ca. $350\;mAhg^{-1}$ which is close to theorestical value of the carbon intercalation composition $LiC_6$, resulting in a relatively low volumetric Li capacity. Notwithstanding the capacities of carbon, it will not adjust well to the need so future devices. Silicon shows the highest gravimetric capacities (up to $4000\;mAhg^{-1}$ for $Li_{21}Si_5$). Although Si is the most promising of the next generation anodes, it undergoes a large volume change during lithium insertion and extraction. It results in pulverization of the Si and loss of electrical contact between the Si and the current collector during the lithiation and delithiation. Thus, its capacity fades rapidly during cycling. We focused on electrode materials in the multiphase form which were composed of two metal compounds to reduce the volume change in material design. A combination of electrochemically amorphous active material in an inert matrix (Si-M) has been investigated for use as negative electrode materials in lithium ion batteries. The matrix composited of Si-M alloys system that; active material (Si)-inactive material (M) with Li; M is a transition metal that does not alloy with Li with Li such as Ti, V or Mo. We fabricated and tested a broad range of Si-M compositions. The electrodes were sputter-deposited on rough Cu foil. Electrochemical, structural, and compositional characterization was performed using various techniques. The structure of Si-M alloys was investigated using X-ray Diffractometer (XRD) and transmission electron microscopy (TEM). Surface morphologies of the electrodes are observed using a field emission scanning electron microscopy (FESEM). The electrochemical properties of the electrodes are studied using the cycling test and electrochemical impedance spectroscopy (EIS). It is found that the capacity is strongly dependent on Si content and cycle retention is also changed according to M contents. It may be beneficial to find materials with high capacity, low irreversible capacity and that do not pulverize, and that combine Si-M to improve capacity retention.

• 대한기계학회논문집
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• 제12권5호
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• pp.1083-1091
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• 1988

본 연구에서는 위의 두번째 연구동향과 맥락을 같이하는 것으로서 스테인리스 강(SUS304)에 대한 진공브레이징 연구 및 탄소강의 진공 브레이징에 대한 연구결과들 을 토대로 하여 SUS304와 탄소강과의 진공브레이징 현상을 연구하였는데 특히 모재의 탄소함유량, 브레이징시간 및 접합부 틈새(joint clearance)등에 따라 접합부에 나타 나는 여러 금속학적 현상의 규명 및 접합강도(joint strength)에 대해 변수들이 미치 는 영향을 연구 하였다.

• 한국정보통신학회논문지
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• 제11권12호
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• pp.2374-2381
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• 2007

표면 탄성파 필터 적절한 임피던스 정합 조건도 얻고자 단상 단방향성 및 양방향성 변환기형 필터를 제작하였다. 그리고 경사진 빗살무의 변환기 형태인 표면 탄성파 필터 제작하기 위하여 Langasite 기판위에 빗살무의 전극들을 형성시켜 모의실험을 수행하였으며, 전극재료로는 Al-Cu를 사용하였다. Langasite 기판위에 형성시킨 단상 단방향성 필터의 전극 수는 50쌍, 두께는 $5000{\AA}$으로 하였으며, 반사기 폭은 $3.6{\mu}m$이고 전극 폭과 전극과 반사기 사이의 간격은 각각 $1.2{\mu}m$로 하였다. 양방향성 필터에서는 전극 폭과 간격은 각각 $1.8{\mu}m$로 하였다. 제작한 필터의 임피던스 정합 후 주파수 특성에서 중심 주파수는 190MHz, 대역폭은 5.3MHz정도로 측정되었으며, 리플 특성은 0.3dB 이하이고, -20dB 정도의 삽입 손실이 측정되었다.