• Title/Summary/Keyword: Crystal temperature

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An Experimental Study on Temperature and Velocity Fields of the Turbulent Flows Horizontal Cylindrical Tube by Using Thermo-sensitive Liquid Crystal (수평원통 관에서 감온액정을 이용한 난류유동의 온도 및 속도장에 관한 실험적 연구)

  • 장태현;도덕희
    • Journal of Advanced Marine Engineering and Technology
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    • v.27 no.7
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    • pp.921-929
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    • 2003
  • An experimental investigation was performed to study the characteristics of turbulent water flow in a horizontal circular tube by using liquid crystal. To determine some characteristics of the turbulent flow, 2D PIV technique is employed for velocity measurement and liquid crystal is used for heat transfer experiments in water. Temperature visualization was made quantitatively by calibrating the color of the liquid crystal versus temperature using various approaches (TLC technique: Thermochromic Liquid Crystal), and a neural-network algorithm was applied to the color-to-temperature calibration. This study shoud the temperature and time-mean velocity distribution for Re = 2,436, 2,500 and 2,724 along longitudinal sections and the results appear to be physically reasonable.

Comparison of numerical simulation and experiment for the OiSF-Ring diameter in czochralski-grown silicon crystal

  • Oh, Hyun-Jung;Wang, Jong-Hoe;Yoo, Hak-Do
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.10 no.5
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    • pp.356-361
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    • 2000
  • The radial position of OiSF-ring has been meaningful data in industry. Thus it's position was calculated by application of (V/G)/sub crit/ = 0.138 ㎟/minK and point defect dynamics for industrial scale grower with various pull rates. After the calculation, compared with experimental result. OiSF-ring diameters expected with calculation were good agreement with experimental results. In order to show validity of the predicted temperature distribution using STHAMAS which is one of the global simulator for Cz crystal growing, temperature was measured along the axis of crystal using thermocouples, and compared with the calculated temperature. We found the effective thermal conductivity K/sub m/ (r) which gives in accordance with the temperature distribution at the axis of crystal and crystal/melt interface shape between experimental and computational results. Therefore, effective thermal conductivity K/sub m/ (r) was applied instead of solving melt convection problem.

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Thermal Stresses Near the Crystal-Melt Interface During the Floating-Zone Growth of CdTe Under Microgravity Environment (미세중력장 CdTe 흘로우팅존 생성에서 결정체-용융액 계면주위의 열응력)

  • Lee Kyu-Jung
    • Journal of computational fluids engineering
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    • v.3 no.1
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    • pp.100-107
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    • 1998
  • A numerical analysis of thermal stress over temperature variations near the crystal-melt interface is carried out for a floating-zone growth of Cadmium Telluride (CdTe). Thermocapillary convection determines crystal-melt interfacial shape and signature of temperature in the crystal. Large temperature gradients near the crystal-melt interface yield excessive thermal stresses in a crystal, which affect the dislocations of the crystal. Based on the assumption that the crystal is elastic and isotropic, thermal stresses in a crystal are computed and the effects of operating conditions are investigated. The results show that the extreme thermal stresses are concentrated near the interface of a crystal and the radial and the tangential stresses are the dominant ones. Concentrated heating profile increases the stresses within the crystal, otherwise, the pulling rate decreases the stresses.

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Crystallization of High Purity Ammonium Meta-Tungstate for production of Ultrapure Tungsten Metal

  • Choi, Cheong-Song
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1997.10a
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    • pp.1-5
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    • 1997
  • The growth mechanism of AMT(Ammonium Meta-Tungstate) crystal was interpreted as two-step model. The contribution of the diffusion step increased with the increase of temperature, crystal size, and supersaturation. The crystal size distribution from a batch cooling crystallizer was predicted by the numerical solution of a mathematical model which uses the kinetics of nucleation and crystal growth. Temperature control of a batch crystallizer was studied using Learning control algorithm. The purity of AMT crystal producted in this investigation was above 99.99%.

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Magnetic field effects of silicon melt motion in Czochralski crystal puller (초크랄스키 단결정 장치내 실리콘 용융액 운동의 자기장효과)

  • Lee, Jae-Hee
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.15 no.4
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    • pp.129-134
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    • 2005
  • A numerical analysis was performed on magnetic field effects of silicon melt motion in Czochralski crystal puller. The turbulent modeling was used to simulate the transport phenomena in 18' single crystal growing process. For small crucible angular velocity, the natural convection is dominant. As the crucible angular velocity is increased, the forced convection is increased and the distribution of temperature profiles is broadened. The cusp magnetic field reduces effectively the natural and forced convection near the crucible and the temperature profiles of the silicon fluids is similar in the case of conduction.

The Variation of Radiative Equilibrium Temperatures with the Ice Crystal Habits and Sizes in Cirrus Clouds (권운 내 빙정의 종류와 크기에 따른 복사 평형 온도 변화)

  • Jee, Joon-Bum;Lee, Won-Hak;Lee, Kyu-Tae
    • Atmosphere
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    • v.20 no.4
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    • pp.427-436
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    • 2010
  • The single-scattering optical properties of ice crystals in cirrus clouds by the aircraft measurement data were investigated, and the radiative equilibrium temperatures and radiative fluxes were calculated and analyzed by radiative convective model with the variations of ice crystal habits and sizes in cirrus clouds. The homogeneous cloud is assumed to be in the layer 200~260 hPa with an ice crystal content of $10gm^{-2}$ for the flux calculation. The profiles of temperature, humidity, and ozone typical of mid-latitude summer are used. The surface albedo is assumed to be 0.2 for all spectral bands and the cosine of solar zenith angles is 0.5. The result of radiative equilibrium temperature at surface was less than surface temperature of the standard atmosphere data in case of smaller effective ice crystal size and larger optical thickness. The column, aggregation and plate in 6 ice crystal habits were the most effective in positive greenhouse effect and bullet-4 was the worst in it. At the surface, the maximum difference of equilibrium temperature by 6 kinds of ice crystal habits were about 3~15 K with 30 sample aircraft measurement data.

Effects of Berberis koreana Palibin on Sleep Duration and Rectal Temperature in Mouse (매자나무성분이 마우스 수면 및 체온에 미치는 영향)

  • Cho Sun-Hee;Kim Chung-Il
    • The Korean Journal of Pharmacology
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    • v.10 no.1 s.15
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    • pp.61-65
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    • 1974
  • Berberis koreana Palibin belonging to Berberidaceae family, a common herb in Korea, has been contained some quantity of Berberine analogue and other ingredients. Authors therefore paid attention to its pharmacological actions and examined the effects on sleep duration and rectal temperature in mouse with crystal (A) from Berberis koreana Palibin in Korean native plans. The experiment searching for the effect on sleep duration was performed with pretreatment of Berberis Koreana Palibin crystal (A) 30 min before the administration of 25 % ethanol, and its crystal were also administered intraperitoneally with the intention to examine the effect on rectal temperature in mouse. The results of the experiment were as follows; 1. Crystal (A) from Berberis koreana Palibin was made by extraction with ethanol and HCI. 2. Crystal (A) enhanced the hypnotic activity of alcohol in concentratins of 0.1 mg/10g or 0.15 mg/10g. 3. Rectal temperatures in mice were significantly reduced with administration of crystal (A) in concentrations of 0.1 mg/10g or 0.15 mg/10g. 4. The maximal reduction of rectal temperature and potentiation of the hypnotic activity were observed at 30 min after its administration. From the above results, it is clear that crystal (A) from Berberis koreana Palibin exerts the potentiation of hypnotic action of alcohol and reduction of rectal temperature in normal mouse. Its pharmacological effects are probably derived from the action upon the central nervous system.

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Crystal Structures of Ba-ferrites Synthesize by Coprecipitation-Oxidation Method (공침-산화법으로 합성된 바륨페라이트의 결정구조)

  • 신형섭
    • Journal of the Korean Ceramic Society
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    • v.34 no.10
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    • pp.1045-1052
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    • 1997
  • Barium ferrites (BaFe12O19) were synthesized at the various temperature by the coprecipitation-oxidation method. X-ray diffraction Rietveld analysis for barium ferrites were performed, their microstructures were observed and their magnetic properties were measured, in order to analyze the crystal structures and determine the optimal temperature of heat-treatment. The barium ferrite, its average particle size 80 nm, was formed at 600℃ through the hematite (α-Fe2O3), but the site occupations of the Fe's in tetrahedral and bipyramidal sites and of the Ba relatively low. Increasing the heating temperature, these occupations and the magnetization increased, and the crystal c-axis decreased. These changes were very small at the heat treatment of above 800℃, but the particles were rapidly grown. It is suggested that the optimal temperature of heat-treatment is 800℃, at which temperature crystal structure is relatively stable and the particles hardly ever grow.

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A Study of Nucleation and Growth in Zinc Crystal Glaze by Firing Conditions (아연결정유의 제조에 있어서 소성조건에 따른 결정생성과 성장에 관한 연구)

  • Lee, Chi-Youn;Lee, Byung-Ha
    • Journal of the Korean Ceramic Society
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    • v.46 no.3
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    • pp.253-262
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    • 2009
  • The purpose of this study is to find out optimum conditions for zinc crystalline glaze under variables of firing: maximum firing temperature, crystal growth temperature, temperature increasing speed, annealing speed, holding time at maximum temperature and holding time at crystal growth temperature. Ferro Frit3110, ZnO and Quartz were used as starting materials and tested by three component system. The best result of test was selected and extended to its vicinity as five glaze formulas. And then the specimens were experimented by variable firing conditions and analyzed by crystal appearance observation, XRD, FT-IR and Raman spectroscopy. In result, main crystal was willemite in the zinc glazes. Some gahnite was detected in specimens which were fired at $1230^{\circ}C$, $1250^{\circ}C$ and $1270^{\circ}C$, however gahnite was not identified at $1300^{\circ}C$. Optimum zinc crystalline glaze was gained by following firing condition: temperature increasing speed $5^{\circ}C$/min, holding 1 h at $1270^{\circ}C$, annealing speed $3^{\circ}C$/min till $1170^{\circ}C$, holding 2 h at $1170^{\circ}C$ then naturally annealed.

Czochralski crystal growth by the accelerated crystal rotation technique (결정봉 회전 가속화 기법에 의한 초크랄스키 결정 성장)

  • 김승태;최정일;성형진
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.1
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    • pp.18-28
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    • 1998
  • A laboratory experiment was made of a control of temperature oscillation in Czochralski convection. Numerical computation was also made to delineate the control of temperature oscillation. The suppression of temperature oscillation was achieved by varying the rotation rate of crystal rod ($\Omega=\Omega_0(1+A sin 2{\pi}ft/t_p)$), where A denotes the amplitude of rotation rate and f the frequency factor. Based on the inherent dimesionless time period of temperature oscillation ($t_p$), the suppression rate of temperature oscillation was characterized by the mixed convection parameter ($0.217{\leq}Ra/PrRe^2{\leq}1.658$). The optimal values of A and f were also scrutinized. To understand the suppression mechanism of temperature oscillation, the controls of isotherm($\theta$) and equi-vorticity($\omega$) were investigated.

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