• 제목/요약/키워드: Crystal shape

검색결과 583건 처리시간 0.021초

Synthesis and electromagnetic properties of FeNi alloy nanofibers using an electrospinning method

  • Lee, Young-In;Choa, Yong-Ho
    • 한국결정성장학회지
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    • 제22권5호
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    • pp.218-222
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    • 2012
  • FeNi alloy nanofibers have been prepared by an electrospinning process followed by air-calcination and H2 reduction to develop electromagnetic (EM) wave absorbers in the giga-hertz (GHz) frequency range. The thermal behavior and phase and morphology evolution in the synthetic processes were systematically investigated. Through the heat treatments of calcination and H2 reduction, as-spun PVP/FeNi precursor nanofiber has been stepwise transformed into nickel iron oxide and FeNi phases but the fibrous shape was maintained perfectly. The FeNi alloy nanofiber had the high aspect ratio and the average diameter of approximately 190 nm and primarily composed of FeNi nanocrystals with an average diameter of ~60 nm. The FeNi alloy nanofibers could be used for excellent EM wave absorbing materials in the GHz frequency range because the power loss of the FeNi nanofibers increased up to 20 GHz without a degradation and exhibited the superior EM wave absorption properties compared to commercial FeNi nanoparticles.

반정육면체 알고리즘 및 단결성 성장로의 열해석에의 응용 (Hemi-cube algorithm and its application to thermal analysis of crystal growth furnace)

  • 이승복;정진수;고상근
    • 대한기계학회논문집B
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    • 제22권7호
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    • pp.905-914
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    • 1998
  • View factor determination is very important in thermal analysis problems with surface radiation but it is very difficult to determine view factors for complex geometries. Exact calculation of view factors for crystal growth furnace is essential due to not only its high surface temperature but the radiation shield, complicated heating system. In this study, view factor calculation algorithm is introduced and applied to cylindrical crystal growth furnace. This algorithm is based on the Hemi-Cube Algorithm and the results obtained with this algorithm show good agreements with those of analytical solution. As an application of this algorithm, temperature profiles and heating value distributions for various furnaces are calculated and the shape criteria for better furnace are suggested.

화력발전소 잔사회 입도에 따른 에코인공골재의 특성에 관한 연구 (A study on the characteristics of eological lightweight aggregates containing reject ash from the power plant)

  • 김유택;류유광
    • 한국결정성장학회지
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    • 제20권4호
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    • pp.185-191
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    • 2010
  • 잔사회와 준설토를 효과적으로 자원화하기 위하여 8~10 mm 크기의 구형 인공 골재를 성형하였다. 출발원료는 입도 및 조성을 변화시켰으며 $1050{\sim}1250^{\circ}C$ 범위에서 소결하였다. 제조된 골제는 KS에 의거하여 골재의 밀도와 흡수율 시험을 진행하였다. 잔사회와 준설토는 고온에서 철 함유 물질과 알칼리/알칼리토 산화물에 의한 발포 기구가 적용됨을 예측할 수 있었다.

세라믹 애자 건조공정의 유한요소 시뮬레이션 (Finite element simulation of drying process for ceramic electric insulators)

  • 정준호;금영탁;오근호
    • 한국결정성장학회지
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    • 제9권3호
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    • pp.347-352
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    • 1999
  • 세라믹 애자 건조공정의 유한요소 시뮬레이션으로 건조공정중 애자의 온도분포, 습도분포, 습열응력분포, 그리고 변형형상을 예측하였다. 유한요소 수식화에서 온도구배, 습도구배, 전도, 대류 및 증발을 고려하여 불소성 세라믹의 온도분포와 습도분포를 구하였고, 온도 및 습도변화로 인한 체적 변화로부터 습열응력을 구하였다. 유한요소 수식화를 기초로 컴퓨터 프로그램을 개발하고, 개발된 프로그램을 사용하여 세라믹 애자의 건조공정을 시뮬레이션 하였다.

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Y$Ba_{2}$$Cu_{3}$$O_{x}$단결정의 용융온도 및 유지시간에 따른 물리적 특성 변화 (Physical properties with melting temperature and holding time for $YBa_{2}$$Cu_{3}$$O_{x}$ single crystal)

  • 박병삼;한상철;한영희;정년호;윤희중;김경진;오제명;성태현
    • 한국초전도저온공학회:학술대회논문집
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    • 한국초전도저온공학회 2003년도 추계학술대회 논문집
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    • pp.93-95
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    • 2003
  • YBa$_2$Cu$_3$O$_{x}$ (Y123) single crystal was grown by TSMG (top seeded melt growth) method. Physical properties of Y123 single crystal were dependent on the shape and distribution of Y2BaCuOx (Y211) in it and on the oxygenation temperature and the holding time. In this work, It was investigated to an optimal oxygenation condition and a dependence of melting temperature and holding time on physical properties. The optimal oxygenation condition was found that it was heat-treated for 30 hours at 45$0^{\circ}C$, Also it was found that the critical current density and the size of Y211 were increased with the melting temperature and the holding time.e.

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수열합성법에 의한 칼시아 안정화 정방정 지르코니아(Ca-TZP)분말의 제조 (Preparation of Calcia Stabilized Tetragonal Zirconia Powders by Hydrothermal Synthesis Techniques)

  • 곽효섭;백용혁;문기동;이종국
    • 한국결정성장학회지
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    • 제2권2호
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    • pp.33-39
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    • 1992
  • 칼시아를 안정화제로 사용하여 수열 반응법으로 지르코니아 분말을 제조한 결과 상온에서 정방정상으로 존재하는 지르코니아 다결정체(Ca-TZP) 분말을 제조할 수 있었다. 제조된 분말은 구형으로 입경이 9~13nm로 매우 미세하였으며, 비표면적은 $112m^2/g$ 이상, 그리고 응집은 약한 응집(weak agglomeration)특성을 나타내었다.

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Covalent Adaptable Liquid Crystal Elastomers Comprising Thiourea Bonds: Reprocessing, Reprogramming and Actuation

  • Lee, Jin-Hyeong;Park, Sungmin;Kim, Yong Seok;Kim, Dong-Gyun;Ahn, Suk-kyun
    • Elastomers and Composites
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    • 제57권2호
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    • pp.55-61
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    • 2022
  • In this work, we report a highly deformable covalent adaptable-liquid crystal elastomer (CA-LCE) comprising dynamic thiourea bonds that enable macromolecular network rearrangement at elevated temperatures. The exchange of chain network is verified through stress-relaxation analyses and follows Arrhenius-type behavior. The unique capability of rearranging the chain network in the CA-LCE provides useful properties, such as welding, melt reprocessing, and shape reprogramming, that cannot be achieved by the conventional LCE comprising permanent crosslinks. Reversible actuation is further demonstrated by reprogramming the polydomain CA-LCE into a monodomain via mechanical stretching at elevated temperatures.

Burr and Shape Distortion Micro-Grooving of Non-Ferrous Metals Using a Diamond Tool

  • Ahn, Jung-Hwan;Lim, Han-Seok;Son, Seong-Min
    • Journal of Mechanical Science and Technology
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    • 제14권11호
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    • pp.1244-1249
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    • 2000
  • Burr and shape distortion are two main problems in micro-grooving. In this study, a simplified model is proposed based on large thrust force due to the tool edge radius. Experiments are conducted with a single crystal diamond tool on a 3-axis snaper-like machine varying the depth of cuts, and groove angles on brass, aluminum and OFHC. Experiments have shown that the thrust force becomes a dominant variable in burr generation compared to the principal force when the depth of cut is less than 2${\mu}m$. And fewer burrs develop on more brittle materials. Shape distortion is significant only when the groove angle is small and the depth of cut is larger than 30 ${\mu}m$.

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평판 투명 물체의 형상측정을 위한 비접촉식 광센서 개발 (Development of a noncontact optical sensor for measuring the shape of transparent plates)

  • 윤상필;유영기
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 2000년도 제15차 학술회의논문집
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    • pp.214-214
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    • 2000
  • This paper deals with the non contact optical sensor to measure the shape of transparent plates such as glass panel of LCD(Liquid Crystal Display). The conventional methods to obtain the shape or thickness of a transparent plates are contact type sensor such as LVOT(Linear Variable Differential Transformer). Due to the contact between the tip of the sensor and the surface of objects, the tip is abraded. In addition, the high temperature glass casting makes the size of sensor body changed. These reasons makes the sensor degraded. In this paper, to overcome these problem, we proposed a low cost noncontact optical sensor this is composed of the Hologram laser unit of a CD-Pickup and a plastic lens. To evaluate the performance of the proposed optical sensor, a series of experiments were performed for various measurement condition. Based upon observation of the experimental result, the developed sensor shows good result for measuring the shape of transparent plates.

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란타늄 옥살레이트 반응성 결정화에서 반응조건에 따른 결정입자 연구 (Effect of Reaction Conditions on Crystals in the Reaction Crystallization of Lanthanum Oxalate)

  • 김홍주;김운수;김우식
    • 공업화학
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    • 제9권7호
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    • pp.1004-1010
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    • 1998
  • Single-jet 반회분식 결정화 반응기에서 동력투입량, 반응물의 주입시간 및 주입방법등 반응조건의 변화가 란타늄 옥살레이트 결정입자의 반응성 결정화에 미치는 영향에 대해 실험적으로 조사하였다. 란타늄 옥살레이트 결정입자의 크기분포는 반응조건에 관계없이 monomodal 형태의 크기분포를 나타내었으나 평균결정크기는 반응조건에 크게 영향을 받았다. 동력투입량이 증가할수록, 반응물의 주입속도가 빠를수록, 란타늄 옥살레이트의 결정입자크기는 감소하였으나 상대적 유도시간은 증가하였다. 반응물의 주입방법에 있어서 옥살산 용액이 주입되는 경우보다 염화란타늄 용액이 주입되는 경우에 결정입자는 크게 나타났으며 상대적 유도시간은 감소하였다. 그리고 결정입자의 형태는 모두 침상형으로 반응조건의 변화에 크게 영향을 받지 않았다.

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