• Title/Summary/Keyword: Correlation formulas

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Improvement of Analysis Methods for Fatty Acids in Infant Formula by Gas Chromatography Flame-Ionization Detector (GC-FID를 이용한 조제유류 중 지방산 분석법 개선 연구)

  • Hwang, Keum Hee;Choi, Won Hee;Hu, Soo Jung;Lee, Hye young;Hwang, Kyung Mi
    • Journal of Food Hygiene and Safety
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    • v.36 no.1
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    • pp.34-41
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    • 2021
  • The purpose of this research is to improve analysis methods of determining the contents of fatty acids in infant formulas and follow-up formulas. A gas chromatography (GC) method was performed on a GC system coupled to flame ionization detector, with a fused silica capillary column (SP2560, 100 m×0.25 mm, 0.20 ㎛). The method was validated using standard reference material (SRM, NIST 1849a). Performance parameters for method validation such as specificity, linearity, limits of detection (LOD) and quantification (LOQ), accuracy and precision were examined. The linearity of standard solution with correlation coefficient was higher than 0.999 in the range of 0.1-5 mg/mL. The LOD and LOQ were 0.01-0.06 mg/mL and 0.03-0.2 mg/mL, respectively. The recovery using standard reference material was confirmed and the precision was found to be between 0.8% and 2.9% relative standard deviation (RSD). Optimized methods were applied in sample analysis to verify the reliability. All the tested products had acceptable contents of fatty acids compared with component specification for nutrition labeling. The result of this research will provide efficient experimental information and strengthen the management of nutrients in infant formula and follow-up formula.

Analysis of the Correlation between Geological Characteristics and Water Withdrawals in the Laterals of Radial Collector Well (방사형집수정의 수평집수관에서 지질특성과 취수량의 상관관계 분석)

  • Kim, Tae-Hyung;Jeong, Jae-Hoon;Kim, Min;OH, Se-Hyoung;Lee, Jae-Sung
    • The Journal of Engineering Geology
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    • v.24 no.2
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    • pp.201-215
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    • 2014
  • This study was performed to investigate the correlation between hydraulic conductivity and the flow rate of an aquifer, with the flow rate calculated from the laterals of the radial collector well using data obtained by the development project of riverbank filtration (Second Phase) in Changwon City. The hydraulic conductivity was empirically calculated from unconsolidated sediments collected from a sandy gravel layer along the middle-to-downstream sections of the Nakdong River. The Beyer equation produced the most suitable hydraulic conductivity from the various empirical formulas employed. The calculated hydraulic conductivity ranged from 0.083 to 0.264 cm/s, with an average value of 0.159 cm/s, suggesting that the aquifer in the study area possesses a high permeability with a good distribution of sandy gravel. The relationship between the calculated hydraulic conductivity in the aquifer and the entrance velocity into the screen, the flow rate was analyzed through the linear regression analysis. From the result of regression analysis, it showed that the hydraulic conductivity and the entrance velocity into the screen and the flow rate have a linear regression equation having about 72% of the high correlation. The result of verification in the measured data between each variable showed a high suitability from being consistent with the approximately 72% in the linear regression analysis. This study demonstrates that the groundwater flow rate can be estimated within the laterals of the radial collector well using a linear regression equation, if the hydraulic conductivity of the aquifer is known. This methodology could thus be applicable to other aquifers with hydraulic conductivity and permeability parameters similar to those in the present study area.

Assessment of Daily steps, Activity coefficient, Body composition, Resting Energy Expenditure and Daily Energy Expenditure in Female University Students (여대생의 1일 보행수, 활동계수, 신체조성, 휴식대사량 및 에너지 소비량의 평가)

  • Choe, Hyeon-Jeong;Song, Ju-Mi;Kim, Eun-Gyeong
    • Journal of the Korean Dietetic Association
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    • v.11 no.2
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    • pp.159-169
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    • 2005
  • The purpose of this study was to assess the energy expenditure and investigate the relationship between related variables in 70 female university students. Resting energy expenditure estimated by Harris-Benedict formula, WHO/NAO/FAO formula and various formulas based on body weight and body surface area were 1366.9$\pm$74.4kcal/day, 1287.8$\pm$106.6kcal/day, 1171.4$\pm$155.8kcal/day and 1342.0$\pm$97.4kcal/day. Measured resting energy expenditure by indirect calorimetry(Model : Metavine and TrueOne2400) were 1582.0$\pm$150.1kcal/day and 1268.2$\pm$152.9kcal/day, respectively. Average step number per day was 11981.2$\pm$3014.4 steps and average step number per hour was 746.1$\pm$198.0 steps/hr. Daily energy expenditure by using Harris-Benedict formula, body weight formula, body surface area formula, WHO/NAO.FAO formula and 15-min check list formula were 2374.7$\pm$249.6kcal, 2033.5$\pm$313.2kcal, 2331.2$\pm$266.0kcal, 2240.8$\pm$185.5kcal and 2195.5$\pm$398.3kcal. Meanwhile energy intake of subjects was 1714.9$\pm$551.2 kcal. Daily energy expenditure has positive correlation(r=0.262) with daily step number. And there was significant positive correlations(r=0.35-0.68) between various daily energy expenditures and muscle mass. These results suggested that increase of daily step number by using pedometer is good method to increase daily energy expenditure. In particular, increase in step number can reinforce the amounts of muscle.

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The Availability Examination for Vegetation Measurement of The SLR Digital Camera (SLR 디지털카메라의 식생관측센서로서의 유효성 검토)

  • Kim, Jong-Hwan;Kim, Eung-Nam;Jun, Byung-Dug;K., Sugiyama
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.27 no.1
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    • pp.683-692
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    • 2009
  • On-site remote sensing technique by using single lens reflex(SLR) digital camera will be expected as the useful tool for the vegetation measurement field such as a crop growth management, the monitoring of revegetation slope and the evaluation of environment. We reviewed the availability of the vegetation measurement using a digital camera which is sailed for general-purpose. As a result, we could analysis relationship with the illuminance of image plane and incidence energy of multitemporal observation images by doing gamma correction and exposure compensation. And also, we proposed the model formulas for the correction of influences of capturing angle and illuminance. In addition, we obtained high correlation of normalized difference vegetation index(NDVI) between digital camera and spectral photometer.

Application of Enzymatic method to Determine Choline Concentration in Bovine Blood and Muscle (소의 혈액 및 근육 중 choline 농도 분석을 위한 효소측정법의 적용기법의 개발)

  • Kim, Young-Il;Jung, Won-Chul;Shon, Ho-Yeong;Kim, Suk;Hur, Yoen;Lee, Hu-Jang
    • Journal of Food Hygiene and Safety
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    • v.23 no.3
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    • pp.271-275
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    • 2008
  • Choline is important an organic compound for normal membrane function, acetylcholine synthesis, lipid transport, and methyl metabolism. In biological tissues and foods, there are multiple choline compounds that contribute to choline content. There are so many analytical methods for choline determination, such as radioisotopic, high-performance liquid chromatography, and gas chromatography/mass spectrometry. However, these existing methods are expensive, unmanageable, and time-consuming. In this study, we modified enzymatic method, which is applicable for the determination of choline in milk and infant formulas, and applied to bovine serum and muscle. The calibration curves were linear with higher correlation coefficients than 0.994. Recoveries obtained by calibration curves from the spiked bovine serum and muscle samples varied between 70.6 and 85.2%. The method may be suitable for use as a routine method in the determination of choline for biological tissue and food samples.

Strength Evaluation of a Doubler Plate of Ship Structure subjected to the Biaxial In-plane Compression (양축방향 면내 압축하중을 받는 선박 이중판의 강도 평가)

  • Juh-Hyeok Ham
    • Journal of the Society of Naval Architects of Korea
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    • v.38 no.1
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    • pp.72-85
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    • 2001
  • A study for the structural strength evaluation on the doubler plate subjected to the biaxial in-plane compression has been performed through the systematic evaluation process. In order to estimate the proper static strength of doubler plate, elasto-plastic large deflection analysis is introduced including the contact effect between main plate and doubler. The characteristics of stiffness and strength variation are discussed based on their results. A1so, in order to compare the doubler structure with the original strength of main plate without doubler, a simple formula for the evaluation of the equivalent flat plate thickness is derived based on the additional series analysis of flat plate structure. Using this derived equation, the thickness change of a equivalent flat plate is analyzed according to the variation of various design parameters of doubler plate and some design guides are suggested in order to maintain the original strength of main plate without doubler reinforcement. Finally, correlation between derived equivalent flat plate formula and the developed buckling strength formulas by author et a1. is discovered and these relations are formulated for the future development of simple strength evaluation formula of doubler plate structure.

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Study on the Ideal Adapted Body Weight of Korean Adults Men with reference to 30-39, 40-49 and 50-59 Age-group (한국성인남자(韓國成人男子)의 정상적응체중치(正常適應體重値)에 관(關)한 연구(硏究) -30대(代), 40대(代), 50대군(代群)을 중심(中心)으로-)

  • Park, Soon-Young
    • Journal of Preventive Medicine and Public Health
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    • v.10 no.1
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    • pp.44-51
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    • 1977
  • In order to determine values for the body weight by height groups for Korean adults men who are fully grown up 4,028 (30-39 age-group ; 2,318, 40-49 age-group 1,340, and 50-59 age group : 370) apparently healthy males subjects were randomly selected for the measurement of body weight by height groups. 1) The avergae body height and weight of Korean adult men were $168.3{\pm}4.6cm$ and $63.4{\pm}7.1kg$ in 30-39 age group, $167.7{\pm}4.7cm$ and $63.4{\pm}7.4kg$ in 40-49 age group, and $167.3{\pm}5.2cm$ and $63.3{\pm}8.0kg$ in 50-59 age group. 2) A correlation coefficient of r=+0.52(P<0.001) between body height and weight was found in 30-39 age group of 2,318 subject, r=+0.48(P<0.001) in 40-49 of 1,340 and r=+0.53(P<0.001) in 50-59 of 370 with the aid of there coefficients of linear regression equation body weight and height were established for male as follow; for 30-39 age group, Y(weight in kg)=0.81X(height in cm)-73.02, 40-49 age group, Y(weight in kg)=0.74X(height in cm)-61.82, 50-59g age-group, Y(weight in kg)=0.82X(height in cm)-73.83. 3) With the aid of above listed various equation standard values for body weight by height group, with over weighing and under weighing values were established. 4) Standard bodyweight of Korean was lower than those of American, Japanese and several other formulas for ideal body weight.

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On the Height Growth of Several Species growing in the Middle Korea (국내주요수종의 수고생장에 대하여)

  • Ma, Sang-Kyu
    • Journal of Korean Society of Forest Science
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    • v.21 no.1
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    • pp.39-45
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    • 1974
  • The objects of this study are to induce the experimental equation suitable to estimate the height growing process, and to get some information that could be to reduce the error percent on determining the site index. The height growing process per sample plot were made up from the height age curve getted through the stem-analysis of the dominant tree. The 11 equations were calculated in the functional formulas between the age and the dominant height of Alnus hirsuta, Larix leptolepsis, L. Gmelini, P. koraiensis, Abies holophylla, P. rigida, Q. acutissima and Q. aliena. The suitable equation for estimating the guide curve were selected with the highest correlation and the low standard error with comparision on the age-height distributed map as Fig. 2. The suitable equation is different between the species as their calculated results as follows; The growing process of tree height are occasionally found to be polymorphous in the growth pattern as Fig. 3. By this result, the site index are practically found to be always not constant but shows variation to age in same plot as example 5. So, that the site index are estimated from the height-growth curve to age drawing by the stem-analysis or the polymorphic-curve, are concluded to be suitable on the study of site evaluation.

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Quantitative Determination of the Bioactive Marker Components in Gyeji-tang Using LC-ESI-MS/MS (LC-ESI-MS/MS를 이용한 계지탕 중 주요 성분 분석)

  • Seo, Chang-Seob;Ha, Hyekyung
    • Korean Journal of Pharmacognosy
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    • v.49 no.1
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    • pp.76-83
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    • 2018
  • A traditional herbal formula, Gyeji-tang has been used to treat the early colds, headache, chills, and fever in Asian countries. In this study, we were performed simultaneous determination of the 14 bioactive marker compounds, gallic acid, spinosin, paeoniflorin, albiflorin, liquiritin apioside, liquiritin, 6'''-feruloylspinosin, liquilitigenin, coumarin, cinnmamic acid, benzoylpaeoniflorin, cinnamaldehyde, glycyrrhizin, and 6-gingerol in Gyeji-tang using an ultra-performance liquid chromatography-electrospray ionization-mass spectrometry (UPLC-ESI-MS/MS). Analytical column was used a Waters Acquity UPLC BEH $C_{18}$ analytical column ($2.1{\times}100mm$, $1.7{\mu}m$) and maintained at $45^{\circ}C$ with a flow rate of 0.3 mL/min. The mobile phase consists of 0.1% (v/v) formic acid in water and acetonitrile with gradient elution. The MS analysis was conducted using multiple reaction monitoring in the positive and negative modes by a Waters ACQUITY TQD LC-MS/MS system. The calibration curves of 14 bioactive marker compounds showed linearity with correlation coefficients ${\geq}0.9798$. The limits of detection and quantification values were in the range of 0.11-6.66 ng/mL and 0.34-19.99 ng/mL, respectively. As a result of the analysis using the established LC-MS/MS method, the amounts of tested 14 compounds in the lyophilized Gyeji-tang sample were detected up to $85.7{\mu}g/g$. These results may be useful for quality assessment of a traditional herbal formulas.

Journal PageRank Calculation in the Korean Science Citation Database (국내 인용 데이터베이스에서 저널 페이지랭크 측정 방안)

  • Lee, Jae-Yun
    • Journal of the Korean BIBLIA Society for library and Information Science
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    • v.22 no.4
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    • pp.361-379
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    • 2011
  • This paper aims to propose the most appropriate method for calculating the journal PageRank in a domestic citation database. Korean journals show relatively high journal self-citation ratios and have many outgoing citations to external journals which are not included in the domestic citation database. Because the PageRank algorithm requires recursive calculation to converge, those two characteristics of domestic citation databases must be accounted for in order to measure the citation impact of Korean journals. Therefore, two PageRank calculation methods and four formulas for self-citation adjustment have been examined and tested for KSCD journals. The results of the correlation analysis and regression analysis show that the SCImago Journal Rank formula with the cr2 type self-citation adjustment method seems to be a more appropriate way to measure the relative impact of domestic journals in the Korean Science Citation Database.