• 제목/요약/키워드: Conventional sintering

검색결과 426건 처리시간 0.024초

Facile Fabrication of $TiO_2$ Photoelectrodes Using Intense Pulsed Light for Dye-Sensitized Solar Cells

  • 진화영;유기천;이진아;임정아;김지현;고민재
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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    • pp.228-228
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    • 2013
  • Dye-Sensitized Solar Cells (DSSCs) have attracted great interests as they offer high energyconversion efficiencies at low cost. For the conventional fabrication of DSSCs, high temperature sintering is required for the construction of interconnect $TiO_2$. However, more simplified process which can be applicable to large-sized solar cells module, is strongly necessary for the commercialization of DSSCs. In this work, we developed novel sintering method using Intense Pulsed Light (IPL), which can replace the conventional high temperature sintering methods. The photovoltaic properties of DSSCs utilizing IPL methods will be reported.

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fe-Cu-Sn계 입분체의 소결성 향상 (Improvement in Sinterability Iorn-Copper- Tin Compact)

  • 김윤채
    • 한국분말재료학회지
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    • 제7권1호
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    • pp.50-54
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    • 2000
  • In order to reduce the sintering temperature of iron based sintered parts, sinteing properties of iron-copper prealloyed powder were investigated at various temperatures in the range of 700∼890$^{\circ}C$, and than the rusults were compared with those of the conventional iron-copper-tin compact using elemental powders, The using of prealloyed as a new process improved its sintering performance at lower temperature than elemental powder as the conventional process. The relative sintered density and radial crushing stength of the compact using prealloyed were higher than those of using elemental powder at all sintering temperature. For example, the radial curength of the compact using powder was about 50kg/mm2 at 700$^{\circ}C$, while that of the compact using elemental powder sintered at 890$^{\circ}C$ was 43kg/mm2.

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WC-Co 초경합금의 마이크로파 소결 (Microwave Sintering of WC-Co Hard Metals)

  • 송강석;김석범
    • 한국분말재료학회지
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    • 제10권4호
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    • pp.249-254
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    • 2003
  • WC-6wt%Co hard metal powders were sintered by a 2.45 GHz multimode microwave applicator in Ar atmosphere. Microwave sintering of WC-6wt%Co powder lowered the sintering temperature and shortened the processing time in less than two hours than by a conventional method. Microstructures of the sintered specimen were studied with scanning electron microscope (SEM) and no abnormal grain growth was observed. Mechanical properties were similar to the values of the specimens sintered by a conventional method. Specimen sintered at 135$0^{\circ}C$ for 30 minutes ,hewed 99%, 20.5 GPa and 8.1 MPa$\sqrt{m}$ of theoretical density, hardness and fracture strength, respectively.

Microwave로 가열한 알루미나의 소결 및 입성장 거동 (Densification and rain Growth of Alumina Heated by Microwave)

  • 김도형;오성록;김종희
    • 한국세라믹학회지
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    • 제29권4호
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    • pp.305-311
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    • 1992
  • As compared with conventional sintering, rapid heating in microwave system could enhance sinterability and final properties of alumina with a very short sintering time. In this study microwave sintering was performed using zirconia brick as a reaction chamber which was positioned in a 2.45 GHz(700 W) multimode microwave cavity. Microwave-sintered alumina showed high density and smaller grain size than conventionally sintered alumina because the ratio of densification rate/grain growth rate was increased by rapid heating.

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2차원 층상구조를 갖는 소결조제와 이를 활용한 세륨산화물 소결성 향상 (Sintering agents with 2-dimensional layered structure and the enhancement of sinterability of cerium oxide using them)

  • 박지영;오재명;박희정
    • 한국결정성장학회지
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    • 제29권1호
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    • pp.1-5
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    • 2019
  • 산화물을 포함한 세라믹 재료의 물성은 소재 치밀도에 크게 영향을 받는다. 따라서 소재 치밀도를 높이기 위한 다양한 노력들이 진행되어왔다. 이중 많이 사용되는 전략으로 재료 소결 시 소결조제를 첨가하는 것이다. 기존의 소결조제는 3차원 구조를 갖는 구형의 분말이었다. 본 연구에서는 차별화 전략으로 세륨산화물의 소결 밀도를 높이기 위해 2차원 층상구조를 갖는 소결조제를 첨가하였다. 실제로 2차원 층상구조의 조결조제에 의해 소결밀도가 증가되는 것을 확인할 수 있었다. 2차원 층상구조 소재로 초나노 두께(~1 nm)를 갖는 $TiO_x$$MnO_x$ 나노쉬트가 이용되었다.

졸-겔 공정에 의해 제조된 저온소결 $MgCo_2(VO_4)_2$ 세라믹스의 마이크로파 유전특성 (Microwave Dielectric Properties of Low-temperature Sintered $MgCo_2(VO_4)_2$ Ceramics Synthesized by Sol-Gel process)

  • 이지훈;방재철
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 하계학술대회 논문집 Vol.7
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    • pp.288-289
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    • 2006
  • We studied the effect of sol-gel processing and sintering temperature on the microwave properties of $MgCo_2(VO_4)_2$ system(MCV) which is applicable to LTCC(low-temperature cofired ceramics). The MCV was synthesized by sol-gel process using solution that contains precursor molecules for Mg, Co, and V. SEM analysis shows that the average particle size is ${\sim}1{\mu}m$ and size distribution is very uniform compared to the one prepared by conventional solid-state reaction process. Highly dense samples were obtained at the sintering temperature range of $750^{\circ}C{\sim}930^{\circ}C$. The maximum $Q{\times}f_0$ value of 55,700GHz, dielectric constant(${\varepsilon}_r$) of 10.41 and temperature coefficient(${\tau}_f$) of $-85ppm/^{\circ}C$ was obtained at the sintering temperature of $930^{\circ}C$. The superior microwave properties of sol-gel processed MCV relative to conventional solid-state reaction processed one is remarkable especially at lower sintering temperatures such as $750^{\circ}C$ and $800^{\circ}C$.

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랍석분쇄물의 충전성이 그 소결성에 미치는 영향 (Effect of Packing Characteristics on the sintering Propertiesof Pyrophyllite)

  • 지응업;최상욱;류태원
    • 한국세라믹학회지
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    • 제14권4호
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    • pp.236-241
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    • 1977
  • Three kinds of specimen, consisting of the graded pyrophyllite particles alone, a substituent of 8 percent fire clay for the finer portion ($F_2$) of it, and 0.8 percent inorganic binder-added composite were prepared under the following conditions respectively; moisture content=4.5~5.0%, forming pressure=250kg/$\textrm{cm}^2$ and sintering temperature=1, 000~1, 30$0^{\circ}C$. The various properties such as modulus of rupture, apparent porosity, bulk specific gravity, pore size and pore distributiion were measured in order to collaborate with sintering phenomena. The results obtained are as follows: (1) Apparent porosity isgradually decreased with rising the sintering temperature to 1, 25$0^{\circ}C$. (2) The binder-added specimen showed the lowest value in porosity. (3) The optimum sintering temperature of specimens was considered to be 1, 25$0^{\circ}C$. (4) The wider differences between pore volumes of specimens could be obtained by method of mercurypenetration porosimeter than by the conventional method for porosity.

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소결온도에 따른 $Ba(Zn_{1/3}Ta_{2/3})O_3$[BZT] 세라믹스의 구조적 특성 (Structural Properties of $Ba(Zn_{1/3}Ta_{2/3})O_3$[BZT] Ceramics with Sintering Temperature)

  • 이상철;김지헌;김강;이성갑;이영희
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 춘계학술대회 논문집 전자세라믹스 센서 및 박막재료 반도체재료 일렉트렛트 및 응용기술
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    • pp.76-79
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    • 2000
  • The $Ba(Zn_{1/3}Ta_{2/3})O_3$ ceramics were prepared by conventional mixed oxide method. The structural properties of the BZT ceramics with the sintering temperature were investigated by XRD, SEM. The BZT ceramics have a complex-perovskite structure. The BZT ceramics sintered at $1550^{\circ}C$ had a superstructure plane of BZT(100). Increasing the sintering temperature, the bulk density and ordering were increased. The bulk density of the BZT ceramics sintered at $1550^{\circ}C$ was $7.50[g/cm^3]$. Increasing the sintering temperature, the average grain size were increased and pore were decreased.

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분말사출성형한 W-l5wt%Cu 나노복합분말의 초기소결거동 (Initial Sintering Behaviour of the Powder Injection Molded W-15wt%Cu Nanocomposite Powder)

  • 윤의식;유지훈;이재성
    • 한국분말재료학회지
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    • 제5권4호
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    • pp.258-264
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    • 1998
  • The initial sintering behaviour of the powder injection molded (PIMed) W-l5wt%Cu nanocomposite powder was investigated. The W-Cu nanocomposite powder was produced by the mechanochemical process consisting of high energy ball-milling and hydrogen reduction of W blue powder-CuO mixture. Solid state sintering of the powder compacts was conducted at $1050^{\circ}C$ for 2~10 hours in hydrogen at mosphere. The sintering behaviour was examined and discussed in terms of microstructural developments such as W-Cu aggregate formation, pore size distribution and W grain growth. The volume shrinkage of PIM specimen was slightly larger than that of PM(conventional PM specimen), being due to fast local densification in the PIM. Remarkable decrease of carbon and oxygen in the PIM enhanced local densification in the early stage of solid state sintering process with eliminating very fine pores less than 10 nm. In addition, such local densiflcation in the PIM is presumably responsible for mitigating of W-grain growth in the initial stage.

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