• Title/Summary/Keyword: Control of separation

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Experimental Study on Structural and Functional Characteristics of Surface-Modified Porous Membrane (다공성 멤브레인의 표면 개질에 따른 구조 및 성능 특성에 대한 실험 연구)

  • Lee, Sang Hyuk;Kim, Kiwoong
    • Journal of the Korean Society of Visualization
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    • v.19 no.1
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    • pp.50-56
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    • 2021
  • With the advances in recent nanotechnology, mass transport phenomena have been receiving large attention both in academic researches and industrial applications. Nonetheless, it is not clearly determined which parameters are dominant at nanoscale mass transport. Especially, membrane is a kind of technology that use a selective separation to secure fresh water. The development of great separation membrane and membrane-based separation system is an important way to solve existing water resource problems. In this study, glass fiber-based membranes which are treated by graphene oxide (GO), poly-styrene sulfonate (GOP) and sodium dodecyl sulfate (GPS) were fabricated. Mass transport parameters were investigated in terms of material-specific and structure-specific dominance. The 3D structural information of GO, GOP, and GPS was obtained by using synchrotron X-ray nano tomography. In addition, electrostatic characteristic and water absorption rate of the membranes were investigated. As a result, we calculated internal structural information using Tomadakis-Sotrichos model, and we found that manipulation of surface characteristics can improve spacer arm effect, which means enhancement of water permeability by control length of ligand and surface charge functionality of the membrane.

Preparation and Application of Functional Carbon Whisker Membrane for Separation Process

  • Bae, Sang-Dae;Son, Hee-Jong;Jung, Chul-Woo
    • Journal of Environmental Science International
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    • v.17 no.11
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    • pp.1235-1241
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    • 2008
  • Membrane separation is extensively used for water/wastewater treatment because of its efficiency separation processes. However, particles in the feed water can deposit and accumulate on the membrane surface to created cake layer. As a consequence, the selectivity of the membrane and flux through the membrane are decreased, which is called fouling/blocking phenomenon. In order to solve fouling problem, we developed a novel membrane named Carbon Whisker Membrane (CWM) which contains vapor-grown carbon fibers/whiskers on the surface of the membrane and a layer of carbon film coated on the ceramic substrate. We firstly employed polymethyl methacrylate (PMMA) as a testing material to investigate the fouling mechanism. The results suggested that Carbon Whiskers on the surface of the membrane can prevent the directly contact between the membrane body and particles so that the fouling/blocking could not occurred easily compared to the membrane without carbon whiskers. We also researched the relationship with the diameter, density of carbon whisker on the membrane surface and total flux of solutions. Finally, we will be able to control the diameter and density of carbon whiskers on the membrane and existence of carbon whiskers on the membrane, it is important factor, might be prevent fouling/blocking in the water treatment.

DEVELOPMENT AND TESTING OF MEDIUM CAPACITY GRAIN FLOUR SEPARATOR

  • Kachru, Rajinder-P
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 1993.10a
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    • pp.966-978
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    • 1993
  • A power operated 90.5 hp electric motor) grain flour separator was designed and developed for separation of grain (wheat, corn, chickpea and soybean) flour into various fractions based on the size of the particles of the product. The separator agitating mechanism, feed control, cylindrical separator unit and an eccentric mechanism. The machine was tested for wheat ( variety ; Sujata) flour separation into four fractions, viz ; semolina, Gr-I and II, flour (coarse) and white (fine) flour. Wheat samples (6.8% m.c., db) were first pearled by CIAE pearler for 15.8% bran removal . The pearled wheat grains were then milled for semolina by a burre mill. The product and machine characteristics were determined at different capacities varying from 24 kg/h to 143 kg/h. It was found that 76 kg/h capacity gave reasonably best results in terms of purity and recovery of semolina vis-a-vis the market product. The energy requirement of the machine at no-load was found to be 230 W and at load c nditions, it varied between 36.3-6.4 KJ per kg of fead seperation. The macine could be used by small flour millers small/medium size traders and retailers and other processors for making available various flour products of different particle size in the market for ready use of the consumers.

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Diversity and Active Mechanism of Fengycin-Type Cyclopeptides from Bacillus subtilis XF-1 Against Plasmodiophora brassicae

  • Li, Xing-Yu;Mao, Zi-Chao;Wang, Yue-Hu;Wu, Yi-Xing;He, Yue-Qiu;Long, Chun-Lin
    • Journal of Microbiology and Biotechnology
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    • v.23 no.3
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    • pp.313-321
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    • 2013
  • Bacillus subtilis XF-1, a strain with demonstrated ability to control clubroot disease caused by Plasmodiophora brassicae, was studied to elucidate its mechanism of antifungal activity against P. brassicae. Fengycin-type cyclopeptides (FTCPs), a well-known class of compounds with strong fungitoxic activity, were purified by acid precipitation, methanol extraction, and chromatographic separation. Eight homologs of fengycin, seven homologs of dehydroxyfengycin, and six unknown FTCPs were characterized with LC/ESI-MS, LC/ESI-MS/MS, and NMR. FTCPs (250 ${\mu}g/ml$) were used to treat the resting spores of P. brassicae ($10^7/ml$) by detecting leakage of the cytoplasm components and cell destruction. After 12 h treatment, the absorbencies at 260 nm ($A_{260}$) and at 280 nm ($A_{280}$) increased gradually to approaching the maximum of absorbance, accompanying the collapse of P. brassicae resting spores, and nearly no complete cells were observed at 24 h treatment. The results suggested that the cells could be cleaved by the FTCPs of B. subtilis XF-1, and the diversity of FTCPs was mainly attributed to a mechanism of clubroot disease biocontrol.

Airspace Safety Assessment for Implementation of the Japanese Domestic Reduced Vertical Separation Minimum

  • Amai, Osamu;Nagaoka, Sakae
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • v.1
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    • pp.435-440
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    • 2006
  • The Reduced Vertical Separation Minimum (RVSM), which is the reduced minimum from 2,000 ft to 1,000 ft at flight levels (FL) between 290 and FL410 inclusive, was implemented in 30 September 2005 within the Japanese domestic airspace. Prior to the implementation, safety assessment for the airspace in assumed RVSM environments was carried out. Some model parameter values of collision risk model were estimated using flight plan (progress) data and radar data. An estimate of vertical collision risk including operational risk was calculated using these together with given parameter values. The results obtained from this analysis are as follows. (1) Contribution of the vertical collision risk for the crossing routes is about 9 percents of the total technical risk. (2) The estimate of the collision risk is $4.1{\times}10^{-9}$ [fatal accidents / flight hour] and the value is smaller than a maximum allowable level of collision risk, i.e. $5{\times}10^{-9}$ [fatal accidents / flight hour], called the Target Level of Safety.

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Cleaning Model of Head-feeding Combine (자탈형 콤바인의 선별모델)

  • Kim, S.H.;Kang, W.S.;Gregory, James M.
    • Journal of Biosystems Engineering
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    • v.19 no.1
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    • pp.22-32
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    • 1994
  • The combine harvester is considered as an important but complicated and costly machine. The appropriate size of combine has to be developed to use efficiently in Korea. But the combine is such a complicated machine that a complete design model to develop a new type is impossible without understanding the relationship between each factor. The combine capacity is generally limited by the cleaning shoe performance. So a design model for a cleaning shoe has to be developed first for the complete combine design. The objective of this research was to develop a cleaning model of head-feeding combine to predict grain separation from chaff and broken straw on a sieve. A developed physically based model can explain the situation which can happen during separation process. A test apparatus based on the field going machine was developed. The test materials were paddy rice and barley. The data obtained were analyzed by the hand and the video camera. The developed model was verified as an adequate model through the test with $R^2$ of 0.934 and 0.837. The model can be used to evaluate design and operation alternatives of combine and also applied to the automatic control of separation unit of combine with a loss monitering sensors.

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HPLC SEPARATION AND QUANTITATIVE DETERMINATION OF GINSENOSIDES FROM PANAX GINSENG, PANAX QUINQUEFOLIUM AND FROM GINSENG DRUG PREPARATIONS

  • Soldati F
    • Proceedings of the Ginseng society Conference
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    • 1980.09a
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    • pp.59-69
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    • 1980
  • A new HPLC-method for separation and quantitative determination of ginsenosides in Panax ginseng, Panax quinquefolium and in pharmaceutical drug preparations is elaborated. A reversed-phase-system with ${\mu}Bondapak\;C_{18}$ column (3.9 mm $I.D.{\times}30\;cm$) using acetonitrile-water (30:70) 2 ml/min and acetonitrile-water (18:82) 4 ml/min is suitable for the base-line separation of $Rb_1,\;Rb_2,\;Rc,\;Rd,\;Rf,\;Rg_2,\;respectively\;Re,\;Rg_1$ in 30 minutes. The ginsenosides are directly detected at 203 nm (without derivatization) with the LC-55 or LC-75 spectrophotometer (Perkin-Elmer) at $100\%$ transmission. Detection limit is 300 ng at a signal-to-noise ratio of 10:1. The ginsenosides-peak identification is carried out with HPTLC (high performance thin layer chromatography), with MIR-IR (multiple internal reflection-IR-spectros-copy) and with FD-MS (field desorption mass spectrometry). The calibration curve of each ginsenoside has a correlation coefficient very near to 1. Relative standard deviation for quantitative determinations depends upon the amount of ginsenosides and is approximately 1\%$ for ginsenoside contents of 1\%$. This method is adaptable for routine analysis in quality control laboratories.

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Effect of internal stress on cyclic fatigue failure in K3 (K3에 축적된 내부 응력이 피로 파절에 미치는 영향)

  • Kim, Jun-Young;Kim, Jin-Woo;Cho, Kyung-Mo;Park, Se-Hee
    • Restorative Dentistry and Endodontics
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    • v.37 no.2
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    • pp.74-78
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    • 2012
  • Objectives: This study aimed to evaluate the relationship between the cyclic fatigue of a K3 file and internal stress intentionally induced until the activation of the autostop function of the torque-controlled motor. Materials and Methods: K3 (Sybron Endo) .04 and .06 taper, size 25, 30, 35, 40 and 45 were used in this study. To give the internal stress, the K3 files were put into the .02 taper Endo-Training-Bloc (Dentsply Maillefer) until the activation of the auto-stop function of the torque-controlled motor. The rotation speed was 300 rpm and torque value was 1.0 $N{\cdot}cm$. K3 were grouped by the number of induced internal stress and randomly distributed to 4 experimental groups (n = 10, Stress 0 [control], Stress 1, Stress 2 and Stress 3). For measuring the cyclic fatigue failure, the K3 files were worked against a sloped glass block and time for file separation was recorded. Data was statistically analyzed Statistical analyses were performed using two-way ANOVA and Duncan post-hoc test at p < 0.05 level. Results: Except .04 taper size 30 in Stress 1 group, there were statistically significant differences in time for file separation between control and all experimental groups. K3 with .04 taper showed higher cyclic fatigue resistance than those of .06 taper. Conclusion: In the limitation of this study, the cyclic fatigue of the K3 file was influenced by the accumulated internal stress from use until the auto-stop function was activated by the torque-controlled motor. Therefore, clinicians should avoid the reuse of the K3 file that has undergone auto-stops.

HPLC Separation of Isoquinoline Alkaloids for Quality Control of Corydalis species

  • Kim, Eun-Kyung;Jeong, Eun-Kyung;Han, Sang-Beom;Jung, Jee-H.;Hong, Jong-Ki
    • Bulletin of the Korean Chemical Society
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    • v.32 no.10
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    • pp.3597-3602
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    • 2011
  • A simple and rapid analytical method was developed for the determination of eight isoquinoline alkaloids in Corydalis species. Eight isoquinoline alkaloids, including 2 aporphine alkaloids (isocorydine and glaucine) and 6 protoberberine alkaloids (coptisine, palmatine, berberine, canadine, corydaline, and tetrahydrocoptisine) were used as chemical markers which have a various biological activity and determined for quality control of Corydalis (C.) species (C. ternata, C. yanhusuo, and C. decumbens). To evaluate the quality of these herbal medicines, LC chromatographic separation of alkaloids were preferentially investigated on reversed-phase C18 column with pH variation and composition of mobile phase. In addition, the separation of these alkaloids in herbal extracts was found to be significantly affected on mobile phase composition using gradient elution. Especially for C. yanhusuo extract, berberine was seriously interfered with other alkaloid extracted from sample matrix when mobile phase composition was not optimized. As results, these compounds were successfully separated within 28 min using 10 mM ammonium acetate containing 0.2% triethylamine (adjusted at pH 5.0) as a mobile phase with gradient elution. On the basis of optimized HPLC conditions, 23 different Corydalis species samples were analyzed for the determination of alkaloid levels. In addition, principal component analysis (PCA) combined with the chromatographic data could be successfully classified the different geographic origin samples.