• Journal of the Korean Society of Clothing and Textiles
• /
• v.27 no.5
• /
• pp.554-559
• /
• 2003

A newly developed contact angle measurement instrument by laser beam projection allows for rapid and direct determination of contact angles. The instrument may have a possibility to characterize newly developed nano-fibers. When the laser beam impinges on an edge of an interface of liquid and solid, projected beam were split across and made two straight lines on a tangent screen. From the result, it could measure the contact angle directly by reading the angle between two split beams. The purpose of this study was to prove reliability and reproducibility of the contact angle measurement instrument by laser beam projection compare to the conventional one by microscope through the comparative experiment and questionnaire. Test samples were selected by consideration of hydrophilic and hydrophobic, such as nylon 6 and polypropylene, respectively. The laser contact angle measurement has accurate, fast and convenient method to measure contact angle, and it can be a unique method to characterize nano-fibers.

• Resources Recycling
• /
• v.7 no.5
• /
• pp.41-45
• /
• 1998

A Hew way of contact angle measurement is derived based on simple geometrical calculation. Without using complicated contact angle measurement instrument. Just measuring the diameter and height of liquid lens made it possible to calculate the contact angle value with a reasonable reliability. To validate the contact angle value obtained by this method, contact angle of the same liquid lens is measured using conventional goniometer and it is verified that two values are nearly same within the limit of observational error.

• Journal of Adhesion and Interface
• /
• v.15 no.2
• /
• pp.57-62
• /
• 2014

Pythagolas rule was used for investigation of static contact angle in particular figures. Static contact angle measurement was important to evaluate the wettability between solid and liquid. Optimum measurement method and standardization of calculation for static contact angle were investigated for practical application. Optimum diameter of droplet for static contact angle measurement was confirmed as 1 mm. Contact angle measurement using Pythagolas rule was also used to calculate advancing, receding angle and wettability of different surface condition. At last, it was concluded that the Pythagolas rule method was more accurate than general lineation method for static contact angle measurement.

• Science of Emotion and Sensibility
• /
• v.5 no.3
• /
• pp.67-74
• /
• 2002

Testing device was newly designed and built to measure the dynamic contact angle. The measurement was made using microscope interfaced with computerized image analysis system while the dynamic condition being controled using Instron. As specimens for the experiment, two different types of fibers, i.e., hydrophilic and hydrophobic, were prepared. In case of hydrophilic fiber, the increase of twist level gave the increase of contact angle. However, in hydrophobic yarn the increase of twist level gave the decrease of contact angle. When saline was used as a telling liquid, the increase of the concentration gave the increase of contact angle. The results rationalized clearly on the basis of known concepts could be used in designing fabric structure for the improvement of comport performance.

• Proceedings of the Korean Fiber Society Conference
• /
• 2003.10a
• /
• pp.103-103
• /
• 2003

A newly developed contact angle measurement instrument by laser beam projection allows for rapid and direct determination of contact angles. From the result of comparative experiment and questionnaire, the laser contact angle.

• Journal of the Korean Society for Precision Engineering
• /
• v.30 no.4
• /
• pp.414-420
• /
• 2013

We developed inkjet based measurement system for micro-droplet behavior on a substrate. By using the inkjet dispenser, a droplet, which is as small as few pico-liter in volume, can be jetted and the amount can be controlled. After jetting, the droplet image on the substrate is acquired from side view camera. Then, droplet profile is extracted to measure droplet volume, contact angle and evaporation characteristics. Also top view image of the droplet is acquired for better understanding of droplet shape. The previous contact angle measurement method has limitations since it mainly measures the ratio of height and contact diameter of droplet on a substrate. Unlike previous measurement system, our proposed method has advantages because various behavior of droplet on substrate can be effectively analyzed by extracting the droplet profile.

• Journal of Korea Technical Association of The Pulp and Paper Industry
• /
• v.35 no.3
• /
• pp.43-52
• /
• 2003

The new principle to measure a sizing degree by a contact angle was developed using an automatic determination of the 3-end point coordinates of the water droplet on a sheet, which could diminish the operator's bias during measurement. A constant amount of water was first placed on a sample sheet by a water dispenser, and then an image of the liquid droplet was captured by a digital camera and then transmitted to a computer. The program measuring for contact angle extracted a liquid contour by Gaussian function combined with a 8-direction chain code. The Euclidean equation was applied to the binary image of the liquid contour in order to measure the diameter of the contour. Finally, the contact angle of the liquid was calculated by using the diameter and the top coordinates. In addition, a surface free energy of the sample sheet and an elapsed time taken up to the complete absorption into the sheet were simultaneously measured with the contact angle.

• Journal of the Korean Society of Clothing and Textiles
• /
• v.15 no.1
• /
• pp.70-75
• /
• 1991

Contact angle measuring device was developed in this laboratory using laser beam projec-tion. The new method allows for rapid and direct determination of stationary, advancing, and receding contact angles on both planar and nonplanar solid surfaces, including fibers with very small diameters. A narrow laser beam impinges on an edge of an interface of liquid and solid. This makes two projected laser beam lines upon and radiating from the center of a protractor scale on a tangent screen. Contact angle is measured by determining the difference in angle on the protractor scale between the two projected laser beam lines. Contact angles measured on Perspex-CQ using this instrument were in agreement with the literature. it was shown that this instrument provides a novel method for the facile and accurate measurement of contact angles.

• Korean Journal of Soil Science and Fertilizer
• /
• v.36 no.5
• /
• pp.263-271
• /
• 2003

Effects of the existence of $CO_2$ gas and pH on the silica surface characteristics at silica/Pb(II) and sodium dodecyl sulfonate (SDS, $C_{12}H_{25}SO_3Na$) solution interface were studied. The hydrophobic characteristics of silica surface was delineated by contact angle measurement and surface force measurement using atomic force microscopy (AFM). In $CO_2$ free condition provided by purging $N_2$ gas, the contact angle of fused silica surface in $10^{-4}M$ Pb(II) and SDS solution increased greatly up to $90^{\circ}$ compared with $40^{\circ}$ in atmospheric condition. It was due to the precipitation of $PbCO_3$ in atmospheric condition. In $CO_2$ free condition the change of contact angle and adhesion force ($F_{ad}$) in AFM, affected by pH change, was similar to the distribution of $PbOH^+$ ion in speciation diagram corresponding to $10^{-4}M$ total Pb(II). Therefore, it was convinced that the $PbOH^+$ ion among Pb(II) species would be the main adsorbing type on silica surface. Both of contact angle measurement and surface force measurement using AFM showed that the Pb only treatment made the silica surface hydrophobic. However, it could not be explained theoretically by current knowledge, and required further study in atomic level to solve the problem.

• Journal of the Korean Society of Clothing and Textiles
• /
• v.15 no.4 s.40
• /
• pp.437-445
• /
• 1991

The effect of diameter of rods or fibers on contact angle was studied in a vertical rod configuration. A contact angle measuring device described in the previous paper was optimized for the measurement of small-diameter fibers. It was shown that contact angles of water and hexadecane on nylon 6 monofilsments and glass rods increased with decrease of diameter below a critical diameter, which varied from one system to another. Beyond the critical value, contact angle of the liquid on the vertical glass rod reached to an equilibrium value which is equal to the unique value of the contact angle of the liquid drop on the horizontal glass plate.