• Title/Summary/Keyword: Constituent analysis

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FTIR characterization and antioxidant activity of water soluble crude polysaccharides of Sri Lankan marine algae

  • Fernando, I.P. Shanura;Sanjeewa, K.K. Asanka;Samarakoon, Kalpa W.;Lee, Won Woo;Kim, Hyun-Soo;Kim, Eun-A;Gunasekara, U.K.D.S.S.;Abeytunga, D.T.U.;Nanayakkara, Chandrika;de Silva, E.D.;Lee, Hyi-Seung;Jeon, You-Jin
    • ALGAE
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    • v.32 no.1
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    • pp.75-86
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    • 2017
  • Polysaccharides of marine algae exhibit different structural characteristics and interesting biological functions. In this study, crude polysaccharides (CP) of eleven Sri Lankan marine algae obtained through hot water extraction and ethanol precipitation were investigated for DPPH, alkyl, and hydroxyl radical scavenging activities using electron spin resonance spectrometry and for intracellular reactive oxygen species scavenging activity in the Chang liver cell line. Characterization of CPs was done by Fourier transform infrared (FTIR) spectroscopy and by analysis of the monosaccharide composition. Time-dependent density functional theory quantum-chemical calculations at the RB3LYP/6-31G(d,p) level for constructed dimeric units of the corresponding polysaccharides were used to resolve the FTIR spectra. CPs from Chnoospora minima showed the highest DPPH and alkyl radical scavenging activities and higher intracellular reactive oxygen species scavenging effects for both AAPH and $H_2O_2$ induced ROS production in "Chang" cells. The major polysaccharide constituent in C. minima CP was identified as fucoidan and it displayed a higher sulfate content. The degree of sulfation of these polysaccharides suggests a positive correlation with the observed antioxidant properties.

Analysis of High Temperature Deformation Stability and Properties of Duplex Stainless Steels According to Annealing Temperature (듀플렉스 스테인레스 소재의 고온 변형 안정성 및 어닐링 온도에 따른 특성 분석)

  • Kwon, Gi Hyoun;Na, Young-Sang;Yoo, Wee-Do;Lee, Jong-Hoon;Park, Yong-Ho
    • Korean Journal of Metals and Materials
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    • v.50 no.7
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    • pp.495-502
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    • 2012
  • The aim of this study was to analyze high temperature deformation stability and properties of duplex stainless steels(DSS) according to annealing temperature. In order to analyze high temperature deformation stability, a number of compression tests were carried out with a stain rate of $10^{-2}s^{-1}{\sim}10s^{-1}$ up to a compression ratio of 50% in a temperature range of $950^{\circ}C-1300^{\circ}C$. The analysis of high temperature deformation stability of DSS was performed based on the Ziegler model. In order to analyze the high temperature properties of DSS, annealing treatments were conducted by isothermal holding for 1 hr at $950^{\circ}C$ to $1300^{\circ}C$ with $50^{\circ}C$ intervals followed by water cooling. The hardness and tensile tests were performed on specimens with different volume fractions of constituent phases, such as austenite, ferrite and sigma. The hardness and tensile strength of 2507 according to the annealing temperature are better than those of 2205. The strain rate sensitivity and Ziegler parameter are higher in 2205 than in 2507 as a whole, which implies that 2205 is better than 2507 in terms of forgeability at high temperature.

Qualitative Analysis and Plasma Characteristics of Soil from a Desert Area using LIBS Technique

  • Farooq, W. Aslam;Tawfik, Walid;Al-Mutairi, Fahad N.;Alahmed, Zeyad A.
    • Journal of the Optical Society of Korea
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    • v.17 no.6
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    • pp.548-558
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    • 2013
  • In this work, laser induced breakdown spectroscopy (LIBS) is used to investigate soil samples collected from different desert areas of Riyadh city in Saudi Arabia. Both qualitative analysis and plasma parameters are studied via the observed LIBS spectra. These experiments have been done using a Spectrolaser-7000 system with 50 mJ fundamental wavelength of Nd:YAG laser and detection delay time of 1 microsecond. Many spectral lines are highly resolved for many elements like Al, Fe, Mg, Si, Mn, Na, Ca and K. The electron temperatures Te and electron densities Ne, for the constituent of generated LIBS plasma, are determined for all the collected samples. It is found that both Te and Ne vary from one desert area to other. This variation is due to the change of the elemental concentration in different desert areas that affects the sample's matrices. Time dependent measurements have also been performed on the soil samples. While the signal-to-base ratio (SBR) reached its optimal value at 1 microsecond, the plasma parameters Ne and Te reach values of $4{\times}10^{17}cm^{-3}$ and 9235 K, respectively, at 2.5 microsecond. The later indicate that the plasma cooling processes are slow in comparison to the previously observed results for metallic samples. The observed results show also that in the future it is possible to enhance the exploitation of LIBS in the remote on-line environmental monitoring application, by following up only the values of Ne and Te for one element of the soil desert sample using an optical fiber probe.

Hair Protection Effect by Adding Mask Pack Active Ingredients to the End Paper During Permanent Wave Treatment (퍼머넌트 웨이브 시술시 엔드 페이퍼에 마스크팩 유효성분 첨가에 따른 모발 보호효과)

  • Lee, Bo-Lim;Ko, Kyoung-Sook
    • Journal of Convergence for Information Technology
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    • v.11 no.11
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    • pp.288-295
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    • 2021
  • This study was conducted to investigate the effect of end paper adsorbed with mask pack active ingredients on hair during permanent wave treatment. Permanent wave was performed with purchasing mask packs containing green tangerine, collagen, and Houttuynia cordate active ingredients among commercially available mask packs and adsorbing them to the end paper. As experimental methods, hair thickness, hair moisturizing power, tensile strength, hair epidermis observation using SEM, and hair constituent element analysis using EDS were performed. As a result of the experiment, it was confirmed that the experimental group treated with Houttuynia cordate active ingredient on the end paper had a hair protection effect as a result of hair thickness, tensile strength, hair epidermis observation, and hair component analysis. In addition, it was confirmed that the experimental group treated with green tangerine active ingredient on the end paper contained a relatively large amount of moisture in the hair moisturizing power test result. It is hoped that the development and research of various materials and tools will proceed so that basic cosmetic products containing active ingredients can be developed and used as hair cosmetics, and applied during chemical treatment in the industrial field.

Numerical Verification for Plane Failure of Rock Slopes Using Implicit Joint-Continuum Model (내재적 절리-연속체 모델을 이용한 암반사면 평면파괴의 수치해석적 검증)

  • Shin, Hosung
    • Journal of the Korean Geotechnical Society
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    • v.36 no.12
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    • pp.125-132
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    • 2020
  • Embedded joints in the rock mass are a major constituent influencing its mechanical behavior. Numerical analysis requires a rigorous modeling methodology for the rock mass with detailed information regarding joint properties, orientation, spacing, and persistence. This paper provides a mechanical model for a jointed rock mass based on the implicit joint-continuum approach. Stiffness tensors for rock mass are evaluated for an assemblage of intact rock separated by sets of joint planes. It is a linear summation of compliance of each joint sets and intact rock in the serial stiffness system. In the application example, kinematic analysis for a planar failure of rock slope is comparable with empirical daylight envelope and its lateral limits. Since the developed implicit joint-continuity model is formulated on a continuum basis, it will be a major tool for the numerical simulations adopting published plenteous thermal-hydro-chemical experimental results.

Classification of Torso Shape According to Abdominal Protrusion of Middle-Aged Women (중년 여성 복부 돌출 정도에 따른 토르소 형태 분류)

  • Do, Wolhee;Lee, Jeongeun
    • Fashion & Textile Research Journal
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    • v.23 no.2
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    • pp.226-236
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    • 2021
  • The purpose of this study was to classify the torso shape based on abdominal protrusion caused by changes in the physical characteristics of middle-aged women. This study analyzed 3D shape data of 401 females ranging in age from 40 to 59 years who participated in the 6th Size Korea project. Based on the Size Korea 3D measurement standard, 27 additional items such as height, protrusion, and angle were measured in the 3D scan data. Nine factors were extracted from the analysis of constituent factors of the torso: "vertical size of torso," "flatness and protrusion of abdomen," "torso front extrusion," "upper body height," "bust size and flatness," "size of belly and angle of lower abdomen," "hip length," "hip flatness," and "horizontal size of bust." As a result of the cluster analysis using these nine factors, the torsos of middle-aged women were classified into three types. Type 1 has upper abdominal deposition with a small and long upper body and an advanced abdomen; type 2 has lower abdominal deposition with a small and short torso and a small belly and hip flexion; and type 3 has central abdominal deposition with a big and long torso, large breasts, and protruding abdo¬men front. The middle-aged women were mostly distributed in Type 2. The above results will be useful as basic data for the development of clothing with improved fit to accommodate the changed physical characteristics of middle-aged women.

Increasing Effects of Apoptosis When Co-treated Scutellaria barbata D. Don. with Anti-cancer Drugs (반지련(半枝蓮)과 항암제 병용 투여에 의한 암세포 성장 저해에 관한 연구)

  • Nam, Ju-Young;Sung, Jung-Suk;Jun, Hyun-Ik;Lee, Jeong-Won;Kwon, Su-Kyung;Kim, Dong-Il
    • The Journal of Korean Obstetrics and Gynecology
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    • v.22 no.1
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    • pp.125-139
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    • 2009
  • Purpose: This experiment was designed to find out increasing effects of S. barbata. co-treatment with anti-cancer drugs at cancer cell's growth inhibition effect. Methods: Divergent observational study of the S. barbata. co-treatment with Cisplatin treatment on HeLa cell. Cell viability using MTT assay, Cell Culture and Cytotoxicity Studies, Cell Cycle Analysis, Annexin V-FITC/PI assay, Cell morphological assessment, PARP cleavage using Western blotting analysis when HeLa cell were co-treated with Cisplatin and Scutellaria Barbata extracts. Results: When HeLa cell were co-treated with Cisplatin and Scutellaria Barbata extracts, we found out viability of HeLa cell, changing in the distribution of cell cycle, Annexin V-FITC staining, DAPI staining, PARP clavage protein assay by Western-blot. So Scutellaria Barbata extracts have increased apoptosis Conclusion: When co-treated Scutellaria Barbata extracts with anti-cancer drugs, the anti-cancer effects were increased. We still not sure which constituent apoptosis at cancer cells and activates anti-cancer effects suppressing, but we believe that it'll be revealed here after with following experiments.

Analysis of the current status of quantitative literature evidence for the prescription of 56 herbal medicines covered by health insurance (건강보험 급여 한약제제 56종 처방의 계량적 문헌 근거 현황 분석)

  • Chul Kim;Hyeun-kyoo Shin
    • The Journal of Korean Medicine
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    • v.44 no.3
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    • pp.189-200
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    • 2023
  • Objectives: The purpose of this study is to analyze the current state of quantitative literature evidence for the prescription of 56 herbal medicines covered by health insurance that have been studied in Korea for the past 30 years, to evaluate the reliability of the evidence, and to find out the research direction of herbal medicine prescription in the future. Methods: 56 kinds of herbal medicine prescriptions were searched in domestic literature search databases OASIS, DBpia, and overseas PubMed, classified into chemistry, toxicity, cells, animals, clinical cases, and clinical trial studies, and built into an EBM pyramid structure. Results: When classified according to research contents, there were 61 cases (7.5%) of physicochemical analysis to identify constituent substances, 80 cases (9.8%) of toxicity evaluation, and 672 cases (82.7%) of efficacy evaluation. The efficacy evidence was classified according to the evidence-based medical pyramid structure: 196 cell trials (29.1%), 372 animal trials (55.4%), 89 case and case reporting series (13.3%), 7 comparative case studies (1.1%), and 8 randomized control clinical trials (1.2%). In the pyramid composition, the basis for the validity of 56 kinds of herbal medicines prescribed was 568 cases (84.5%) in cell and animal units, which could not be said to be highly reliable. There was no relationship between the ranking of quantitative literature evidence for herbal medicine prescriptions and the ranking of salary administration. Conclusions: In an era that continues to require scientific evidence for herbal medicine, traditional herbal medicine should secure the basis for safety validity even for the 10th most frequent prescription among 56 herbal medicine prescriptions for consumers. In particular, traditional herbal medicine should increase the quantitative and qualitative level of case reports on related herbal medicine prescriptions, focusing on each clinical society, and move toward comparative case studies and randomized clinical trial so that traditional herbal medicine is positioned as Evidence-based medicine.

An Analysis of Cognizance about and Participation Factors of the Social Welfare labor Union : Centering around Social Welfare Workers (사회복지노동조합에 대한 인식 및 참여요인 분석 : 사회복지종사자를 중심으로)

  • Chai, Goo-Mook
    • Korean Journal of Social Welfare
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    • v.54
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    • pp.65-97
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    • 2003
  • This study seeks the countermeasures for the successful organization of the social welfare labor union after examining social welfare workers' cognizance about a labor union and analyzing the major factors affecting their participation in a labor union. An analysis of social welfare workers' cognizance about the social welfare labor union. demonstrates that (1) most social welfare workers have positive opinions about a labor union organization and the participation in a labor union, (2) a great part of workers prefer forming a labor union and a professional organization together in relation to the organization of social welfare workers, and (3) the effective strategies for the organization of a labor union are in the order of the uplift of social welfare workers' consciousness, the constitution of the basic organizations which propel the formation of a labor union, and the preparation of policy countermeasures which attain the supports of clients and citizens. An analysis of factors affecting the participation in a labor union shows that the attitude toward the participation behavior (positive results), subjective norm (specific individuals), subjective norm (social constituent members), and perceived behavior control in the analysis model, male, lower position in officers, and lower educational attainment in democratic characteristics, and lower democratic and professional managements in officers and longer working hours in labor environmental conditions affect positively the participation in a labor union. These results suggest several assignments for the successful organization of the social welfare labor union. First the activities that make social welfare workers recognize the beneficial results bringing about by the participation in a labor union need to be carried out, second strategies that persuade the influential individuals to supports the participation in a labor union need to be developed, third activities that make the social constituent members understand the ethical, professional, and non-productive characteristics of social service works not to be confronted with the organization of a labor union should be pursued, fourth the organizational environments in which social welfare workers can freely participate in a labor union according to their intentions need to be made up, fifth the policy countermeasures which attain the support of social welfare workers, clients and citizens should be developed and carried out, and finally the basic organizations that effectively propel the formation of a labor union need to be constituted.

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An Improved Method of FTA and Associated Risk Analysis Reflecting Automotive Functional Safety Standard (자동차 기능안전 표준을 반영하는 개선된 FTA 및 위험원 분석 기법)

  • Jung, Ho-Jeon;Lee, Jae-Chon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.9
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    • pp.9-17
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    • 2017
  • Ensuring the safety of automobiles and trains during system operation is regarded as indispensable due to the progress in unmanned operation. The automotive functional safety standard, ISO 26262, has been proposed to ensure the safe design of vehicles. This standard describes in detail the required risk analysis and evaluation procedure and safety measures, while appropriately reflecting the system design information. Therefore, much research has been done on the risk analysis procedure, wherein the design information is mostly extracted from physical components of similar systems already in operation, the information traced back to obtain constituent functions, and then methods of identifying risk sources are studied. This method allows the sources of risk to be identified quickly and easily, however if the design requirements are changed or systems are newly developed, others may be introduced which are not accounted for, thereby yielding mismatched design information. To resolve this problem, we propose a top-down analysis in order to utilize the system design information appropriately. Specifically, a conceptual system is designed to obtain the functions, which are then analyzed. Then, a function-based fault tree analysis is conducted, followed by a risk source analysis. In this paper, a case study of automotive safety is presented, revealing that the proposed method can analyze the risk sources with reduced possibility of omission by systematically reflecting the system design information.