• Title/Summary/Keyword: Constituent analysis

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Anti-diabetic Constituent from the Node of Lotus Rhizome (Nelumbo nucifera Gaertn)

  • Lee, Min-Won;Kim, Jun-Sik;Cho, Su-Min;Kim, Ji-Hun;Lee, Jae-Seung
    • Natural Product Sciences
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    • v.7 no.4
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    • pp.107-109
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    • 2001
  • To investigate anti-diabetic component from the node of lotus rhizome (Nelumbo nucifera; Nymphaeaceae), activity guided isolation was conducted. One amino acid was isolated from active fraction of the aqueous methanolic extract. The structure of this compound was identified as tryptophan (1) by the analysis of spectroscopic evidences and comparisons with the data of authentic samples. Tryptophan reduced the blood glucose level significantly in glucose-fed hyperglycemic mice compared with glucose-treated group and exhibited 44.3% of activity compared with tolbutamide,.

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Analysis of Cytotoxic Constituent of Berberis koreana Palibin (매자나무 세포독성성분 분석)

  • Kim, Young-Kyoon;Kwak, Byung-Man
    • Journal of the Korean Wood Science and Technology
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    • v.26 no.3
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    • pp.100-107
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    • 1998
  • Methanol extracts of five Berberidaceae species were examined against tissue factor inhibitory and tumour cell growth inhibitory activity. Methanol extracts of Berberis koreana Palibin showed a strong cytotoxicity activity against SK-MEL-2 (Melanoma) tumour cell lines with more than 90% in $25{\mu}g/m\ell$ and against A549 (Lung carcinoma), SK-OV-3 (Ovarian cancer), XF498 (CNS cancer) and HCTl5 (Colon cancer), other Berberidaceae species except B. koreana species have no effect on the tumour cells. Biologically active compound, therefore, was isolated through the activity guided fractionation and purification. The structure was confirmed by NMR. FT-IR and MS to 2-(3,4-dihydroxybenzyl)-ethyl alcohol. It showed cytotoxicity activity against SNU-C4 tumour cell lines with 50.7% in $50{\mu}g/m\ell$. Methanol extracts of 5 Berberidacae species have no effect on the tissue factor inhibitory activity.

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Effect of Heat Treatment Characteristic on the Gas Nitriding of Stainless Steels (스테인리스강의 가스질화에 미치는 열처리 조건의 영향에 관한 연구)

  • Kim, H.G.;Hwang, G.S.;Sun, C.G.
    • Journal of the Korean Society for Heat Treatment
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    • v.16 no.2
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    • pp.78-82
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    • 2003
  • Nitrided compound layer and diffusion layer structure were observed by SEM. The compound layer and the constituent of nitrided surface of STS 304, STS 316, STS 410 and SACM 645 steel were analysed using EMPA and XRD respectively. The depth of nitriding layer that is obtained from similar nitriding condition decrease in the order of SACM 645 > STS 410 > STS 316 > STS 304. Result of phase transformation of the nitrided at $550^{\circ}C$ by XRD analysis were as follows; The austenitic stainless steel was mainly consist of $Cr_2N$ accompanying with $Fe_4N$ and $Fe_{2-3}N$ phase and martensitic stainless steel was mainly consist of present $Fe_{2-3}N+Cr_2N$ phase, but SACM 645 steel was $Fe_{2-3}N$ phase present only.

Study on The Non-polar Optical Phonon Scattering According to The Mixture of Atoms in a $A_{1-x}B_{x}$ Alloy semiconductor ($A_{1-x}B_{x}$ 혼합물반도체에서 원자들의 혼합형태에 따른 비극성 Optical 포논산란에 대한 연구)

  • 박일수;전상국
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.14 no.8
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    • pp.611-617
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    • 2001
  • The non-polar optical phonon scattering in the valence band depends on the masses, ratios, and types of mixtures of constituent atoms. Therefore, the random distribution of atoms in alloy semiconductors should be considered in the analysis of scattering mechanisms. For this purpose, the force equations of n atoms in a unit cell are expressed in a n x n matrix form to obtain the angular frequencies due to the acoustic and non-polar optical phonons. And, n is then assumed to be infinity. When this work is compared with other results published elsewhere, it is concluded that the independence of atomic displacement or amplitude of oscillation as ell as the infinite number of atoms in a unit cell must be taken into account for the random distribution of atoms in alloy semiconductors.

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Development of a Simplified Fuel-Cladding Gap Conductance Model for Nuclear Feedback Calculation in 16$\times$16 FA

  • Yoo, Jong-Sung;Park, Chan-Oh;Park, Yong-Soo
    • Proceedings of the Korean Nuclear Society Conference
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    • 1995.05a
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    • pp.636-643
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    • 1995
  • The accurate determination of the fuel-cladding gap conductance as functions of rod burnup and power level may be a key to the design and safety analysis of a reactor. The incorporation of a sophisticated gap conductance model into nuclear design code for computing thermal hydraulic feedback effect has not been implemented mainly because of computational inefficiency due to complicated behavior of gap conductance. To avoid the time-consuming iteration scheme, simplification of the gap conductance model is done for the current design model. The simplified model considers only the heat conductance contribution to the gap conductance. The simplification is made possible by direct consideration of the gas conductivity depending on the composition of constituent gases in the gap and the fuel-cladding gap size from computer simulation of representative power histories. The simplified gap conductance model is applied to the various fuel power histories and the predicted gap conductances are found to agree well with the results of the design model.

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Studies on Alumina Cement from Alunite (I) (Synthesis of monocalcium aluminate) (명반석을 이용한 알루미나 시멘트의 제조(I) (Monocalcium Aluminate의 합성))

  • 한기성
    • Journal of the Korean Ceramic Society
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    • v.15 no.4
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    • pp.199-204
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    • 1978
  • In the present investigation, refined alumina obtained from alunite locally available was used as a aluminous source to synthesize monocalcium aluminate $(CA)_3$ the major mineral constituent of alumina cement. The influence of $SiO_2$ and $Fe_2O_3$ contents on the formation of monocalcium aluminate was studied by X-ray diffraction analysis mainly. About 0.8-1.0 of $Al_2O_3/C_3O$ mol ratio and less than 4 percent of $SiO_2$ were desirable for the effective formation of CA. The small amount of alkali and sulphur contents contained in refined alumina from alunite as the impurities were affected to form $C_4A_3S$ and $C_3S_2$, disadvantageous compounds for the alumina cement, therefore the impurities should be restricted in minimum content as possible.

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Development of Textile Metal Matrix Composites for Electronic Packaging (전자 패키징용 직조형 금속복합재료 개발)

  • 이상관;김진봉;홍순형
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2000.11a
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    • pp.183-186
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    • 2000
  • A new textile metal matrix composite fur electronic packaging was developed and characterized. The thermal management materials consist of a plain woven carbon fabric as reinforcement and pure aluminum as matrix. The finite element method has been utilized in the analysis of thermal stress between the constituent components of packaging. The prototype part was manufactured by the liquid pressurizing method. The composite has CTE values of 4 to $5{\times}10^{-6}\;^{\circ}C^{-1}$10 in the range of $25^{\circ}C$ ~ 175$^{\circ}C$, resulting in good agreement with electronic materials such as Si and GaAs.

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Homogenized thermal properties of 3D composites with full uncertainty in the microstructure

  • Ma, Juan;Wriggers, Peter;Li, Liangjie
    • Structural Engineering and Mechanics
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    • v.57 no.2
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    • pp.369-387
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    • 2016
  • In this work, random homogenization analysis for the effective thermal properties of a three-dimensional composite material with unidirectional fibers is presented by combining the equivalent inclusion method with Random Factor Method (RFM). The randomness of the micro-structural morphology and constituent material properties as well as the correlation among these random parameters are completely accounted for, and stochastic effective thermal properties as thermal expansion coefficients as well as their correlation are then sought. Results from the RFM and the Monte-Carlo Method (MCM) are compared. The impact of randomness and correlation of the micro-structural parameters on the random homogenized results is revealed by two methods simultaneously, and some important conclusions are obtained.

Nonlinear stability of smart nonlocal magneto-electro-thermo-elastic beams with geometric imperfection and piezoelectric phase effects

  • Faleh, Nadhim M.;Abboud, Izz Kadhum;Nori, Amer Fadhel
    • Smart Structures and Systems
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    • v.25 no.6
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    • pp.707-717
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    • 2020
  • In this paper, analysis of thermal post-buckling behaviors of sandwich nanobeams with two layers of multi-phase magneto-electro-thermo-elastic (METE) composites have been presented considering geometric imperfection effects. Multi-phase METE material is composed form piezoelectric and piezo-magnetic constituents for which the material properties can be controlled based on the percentages of the constituents. Nonlinear governing equations of sandwich nanobeam are derived based on nonlocal elasticity theory together with classic thin beam model and an analytical solution is provided. It will be shown that post-buckling behaviors of sandwich nanobeam in thermo-electro-magnetic field depend on the constituent's percentages. Buckling temperature of sandwich nanobeam is also affected by nonlocal scale factor, magnetic field intensity and electrical voltage.