• 제목/요약/키워드: Consistency Checks

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UHPLC 시스템 종료 및 재가동 시 가이드 (UHPLC System Shutdown and Reactivation Advice)

  • Mark Fever;Gemma Lo
    • FOCUS: LIFE SCIENCE
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    • 제1호
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    • pp.8.1-8.3
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    • 2024
  • Ultra-high performance liquid chromatography (UHPLC) systems are integral to modern analytical laboratories, necessitating careful maintenance and operation protocols to ensure optimal performance. This document provides comprehensive guidelines for the proper shutdown and reactivation of UHPLC systems to prevent damage and maintain operational efficiency. • Shutdown: Remove the column and replace it with a union to avoid blockages. Flush the system with a compatible solvent mix, clean mobile phase reservoirs to prevent microbial growth, flush the pump with storage solvent, and clean the autosampler, including the needle and injection port. • Reactivation: Inspect the system for wear or damage, gradually reintroduce mobile phases starting with a weak solvent, reinstall the column securely, and perform system checks on baseline stability, pressure consistency, and detector performance. By adhering to these guidelines, laboratories can ensure the longevity and reliability of their UHPLC systems, maintaining high analytical performance and minimizing downtime. These procedures help prevent common issues such as blockages, contamination, and component wear, thereby supporting efficient and accurate analytical operations.

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맵리듀스 프레임워크를 이용한 대용량 공간 추론기의 설계 및 구현 (Design and Implementation of a Large-Scale Spatial Reasoner Using MapReduce Framework)

  • 남상하;김인철
    • 정보처리학회논문지:소프트웨어 및 데이터공학
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    • 제3권10호
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    • pp.397-406
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    • 2014
  • 미국의 Jeopardy! 퀴즈쇼와 같은 DeepQA 환경에서 인간을 대신해 컴퓨터가 효과적으로 답하기 위해서는, 광범위한 지식베이스와 빠른 시공간 추론 능력이 요구된다. 본 논문에서는 대표적인 병렬 분산 컴퓨팅 환경인 맵리듀스 프레임워크를 이용해, 새로운 방향 및 위상 관계를 효율적으로 추론할 수 있는 대용량 공간 추론 알고리즘을 제시한다. 이 추론 알고리즘은 CSD-9 방향 관계들과 RCC-8 위상 관계들을 포함한 대용량 공간 지식베이스를 입력으로 가정하며, 이로부터 새로운 방향 관계와 위상 관계들을 추론해내기 위해 지식베이스에 대한 경로 일관성 검사와 교차 일관성 검사를 수행한다. 맵리듀스 프레임워크의 원리에 따라 추론 계산의 병렬성을 극대화하기 위해, 맵 단계에서는 대용량의 지식베이스를 다수의 노드들에 효과적으로 분할하여 분산시키고, 리듀스 단계에서는 분산된 지식베이스들로부터 새로운 공간 지식을 유도하도록 공간 추론 알고리즘을 설계하였다. 본 연구에서는 맵리듀스 프레임워크로 구현한 대용량 공간 추론기와 샘플 공간 지식 베이스를 이용한 실험들을 수행하고, 이를 통해 본 논문에서 제안한 대용량 공간 추론기의 높은 성능을 확인할 수 있었다.

직장인들의 건강수준 평가를 위한 측정도구의 신뢰도와 타당도 분석 (Reliability and Validity on Measurement Instrument for Health Status Assessment in Occupational Workers)

  • 고상백;장세진;강명근;차봉석;박종구
    • Journal of Preventive Medicine and Public Health
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    • 제30권2호
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    • pp.251-266
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    • 1997
  • In order to test scaling assumption, and to assess the validity, reliability, and acceptability of the Short form 36(SF-36) health survey questionnaire, we conducted a survey. Samples were 296 workers who had been employed in small sized companies. All scale passed for item internal consistency(100% sucess rate) and item discriminant validity(100% success .ate). Reliability coefficients were ranged from the lowest 0.51 to the highest of 0.85. For 87.5% of the total workers, inconsistent responses were not observed. Only 3.0% of the total workers failed two or more checks. Factor analysis was performed using principal axis factor method and quartimax rotation. In this survey, the SF-36 retained available psychometric properties even when used in a generally healthy worker group. But further study with some consideration to develope health status measurement is expected : first, the definition of health status should be rationalized. Second, the measurement of outcome is an important consideration in evaluations of quality of care. But ambiguities hinder understanding of this important topic. Third, internal consistency should be interpreted with caution as an indication reliability because it ignores potentially important sources of variation that can occur over time.

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연속간행물 종합목록의 중복레코드 최소화 방안 연구 (A Study on the Duplicate Records Detection in the Serials Union Catalog)

  • 이혜진;김순영;김완종;최호남
    • 한국콘텐츠학회:학술대회논문집
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    • 한국콘텐츠학회 2007년도 추계 종합학술대회 논문집
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    • pp.445-448
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    • 2007
  • 연속간행물 종합목록은 국내 여러 기관에 산재한 연속간행물의 정보를 통합하여 공유하고, 정보자원화하기 위한 필수 도구로서 최적화된 목록 및 소장 정보를 생성하여 이용자에게 학술지에 대한 신뢰성 있는 정보를 제공하는 것이 목적이다. 이를 위해서는 데이터의 일관성이 무엇보다 중요하며 레코드의 중복성은 종합목록 품질평가에 있어 중요한 척도 중에 하나가 된다. 본 연구는 연속간행물 기반의 종합목록 데이터의 품질을 개선하기 위하여 오류 데이터로 인한 중복레코드를 최소화하기위한 방안을 마련하는데 있다. 이를 위하여 연속간행물의 중복레코드 검증 요소를 분석하고 검증 프로세스를 제안하였다.

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QUALITY ASSURANCE IMPLEMENTATION IN THE NATIONAL CANCER CENTRE

  • Jui, Wong-Toh
    • 한국의학물리학회:학술대회논문집
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    • 한국의학물리학회 2002년도 Proceedings
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    • pp.19-22
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    • 2002
  • The importance of accurate dose delivery in radiotherapy is well documented. Studies have shown that a mere 5% deviation of the prescribed dose can produce an undesirable treatment outcome. Uncertainties in the dose delivery can arise at different stages of the radiotherapy process. Therefore, a good quality assurance programme will ensure the best possible results and consistency of the radiotherapeutic treatment. Quality assurance in any radiotherapy department involves the responsibility of a multi-disciplinary team of radiation oncologists, medical physicists and radiation technologists. This paper will focus on the physical and technical aspects of QA. The organizational structure and responsibility of the physics QA team is outlined and also included the types and frequencies of QA checks. For a QA program to be effective, action levels should be clearly defined and understood by all staff concerned. Data of the Singapore National Cancer Centre's participation over the last ten years with the IAEA / WHO Postal TLD Dose Inter-comparison programme is presented. The data obtained were within the international criteria. For a QA program to be successfully implemented, there must be a commitment by management to provide adequate staff, test equipment, machine time as well as continual training and education. This is in addition to the positive attitudes of all the staff. A quality audit is also necessary to serve as a check and balance to ensure that the QA is in order.

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Classifying Rules by In-out Traffic Direction to Avoid Security Policy Anomaly

  • Kim, Sung-Hyun;Lee, Hee-Jo
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • 제4권4호
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    • pp.671-690
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    • 2010
  • The continuous growth of attacks in the Internet causes to generate a number of rules in security devices such as Intrusion Prevention Systems, firewalls, etc. Policy anomalies in security devices create security holes and prevent the system from determining quickly whether allow or deny a packet. Policy anomalies exist among the rules in multiple security devices as well as in a single security device. The solution for policy anomalies requires complex and complicated algorithms. In this paper, we propose a new method to remove policy anomalies in a single security device and avoid policy anomalies among the rules in distributed security devices. The proposed method classifies rules according to traffic direction and checks policy anomalies in each device. It is unnecessary to compare the rules for outgoing traffic with the rules for incoming traffic. Therefore, classifying rules by in-out traffic, the proposed method can reduce the number of rules to be compared up to a half. Instead of detecting policy anomalies in distributed security devices, one adopts the rules from others for avoiding anomaly. After removing policy anomalies in each device, other firewalls can keep the policy consistency without anomalies by adopting the rules of a trusted firewall. In addition, it blocks unnecessary traffic because a source side sends as much traffic as the destination side accepts. Also we explain another policy anomaly which can be found under a connection-oriented communication protocol.

해양과학기지 시계열 관측 자료 품질관리 시스템 구축: 국제 관측자료 품질관리 방안 수온 관측 자료 시범적용과 문제점 (Quality Control of Observed Temperature Time Series from the Korea Ocean Research Stations: Preliminary Application of Ocean Observation Initiative's Approach and Its Limitation)

  • 민용침;정진용;장찬주;이재익;정종민;민인기;심재설;김용선
    • Ocean and Polar Research
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    • 제42권3호
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    • pp.195-210
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    • 2020
  • The observed time series from the Korea Ocean Research Stations (KORS) in the Yellow and East China Seas (YECS) have various sources of noise, including bio-fouling on the underwater sensors, intermittent depletion of power, cable leakage, and interference between the sensors' signals. Besides these technical issues, intricate waves associated with background tidal currents tend to result in substantial oscillations in oceanic time series. Such technical and environmental issues require a regionally optimized automatic quality control (QC) procedure. Before the achievement of this ultimate goal, we examined the approach of the Ocean Observatories Initiative (OOI)'s standard QC to investigate whether this procedure is pertinent to the KORS. The OOI QC consists of three categorized tests of global/local range of data, temporal variation including spike and gradient, and sensor-related issues associated with its stuck and drift. These OOI QC algorithms have been applied to the water temperature time series from the Ieodo station, one of the KORS. Obvious outliers are flagged successfully by the global/local range checks and the spike check. Both stuck and drift checks barely detected sensor-related errors, owing to frequent sensor cleaning and maintenance. The gradient check, however, fails to flag the remained outliers that tend to stick together closely, as well as often tend to mark probably good data as wrong data, especially data characterized by considerable fluctuations near the thermocline. These results suggest that the gradient check might not be relevant to observations involving considerable natural fluctuations as well as technical issues. Our study highlights the necessity of a new algorithm such as a standard deviation-based outlier check using multiple moving windows to replace the gradient check and an additional algorithm of an inter-consistency check with a related variable to build a standard QC procedure for the KORS.

이동 컴퓨팅 환경에서 읽기-전용 트랜잭션을 지원하기 위한 비동기적 캐쉬 무효화 기법 (Asynchronous Cache Invalidation Strategy to Support Read-Only Transaction in Mobile Environments)

  • 김일도;남성헌
    • 정보처리학회논문지C
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    • 제10C권3호
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    • pp.325-334
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    • 2003
  • 이동 클라이언트/서버 데이터베이스 시스템에서 클라이언트 캐쉬의 상태 정보가 없이 비동기적 캐쉬 무효화 기법을 사용하여, 읽기-전용 트랜잭션을 지역에서 처리한다면 비동기적 무효화 리포트는 완료를 요청한 이동 트랜잭션의 대기시간에 대해 보장을 해주지 않는 문제가 발생한다. 이 문제를 해결하기 위해, 본 논문에서는 두 가지 종류의 메시지 사용을 제안한다. 트랜잭션의 처리 지연을 줄이기 위한 비동기적 무효화 메시지와 완료를 요청한 트랜잭션의 대기 시간을 보장해 주기 위한 안내 메시지이다. 비동기 무효화 리포트는 자신을 나타내기 위한 일련번호를 가지며, 안내 메시지는 가장 최근에 브로드캐스트 된 무효화 메시지의 일련번호를 가진다. 이동 클라이언트는 이 메시지들의 일련번호를 사용하여 자신의 캐쉬에 대한 유효여부를 점검함으로 이동 트랜잭션의 대기시간에 대해 보장해준다.

병렬 객체지향 시스템의 검증 (Model Checking of Concurrent Object-Oriented Systems)

  • 조승모;김영곤;배두환;변성원;김상택
    • 한국정보과학회논문지:소프트웨어및응용
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    • 제27권1호
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    • pp.1-12
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    • 2000
  • 모델체킹은 검증하려는 대상 시스템의 동작 모델이, 그 시스템이 만족해야 할 성질을 만족시키는지를, 시스템의 상태공간을 검사해 봄으로써 알아보는 정형 검증 기법의 하나이다. 이러한 모델체킹 기법을 병렬 객체지향 시스템에 적용하기 위해 기존의 모델체커인 SPIN에서 지원하는 모델링 언어인 Promela를 병렬객체지향 개념을 추가하여 확장한 언어인 APromela를 제안하였다. 이는 Promela가 프로세스를 단위로 하는 병렬성만을 지원하는데 반해, 액터 모델에 기반한 객체지향 병렬성을 지원한다. 또한 우리는 이 언어로 작성된 모델을 자동으로 Promela로 변환하는 규칙을 제안하였다. 이를 통해, 기존의 모델체커를 이용해 병렬 객체지향 시스템의 검증을 수행할 수 있다. 이 언어의 응용으로 UML 로 기술된 명세의 검증을 수행하는 과정을 제시하였다.

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Early overcounting in otoliths: a case study of age and growth for gindai (Pristipomoides zonatus) using bomb 14C dating

  • Andrews, Allen H;Scofield, Taylor R.
    • Fisheries and Aquatic Sciences
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    • 제24권1호
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    • pp.53-62
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    • 2021
  • Gindai (Pristipomoides zonatus) is one of six snappers in a management complex called the Deep 7 of the Hawaiian Islands. Little is known about its life history and a preliminary analysis of otolith thin sections indicated the species may exhibit moderate growth with a lifespan approaching 40 years. Preliminary age estimates from the previous study were reinvestigated using the same otolith sections in an attempt to validate those ages with bomb radiocarbon (14C) dating. From the misalignment of birth years for the otolith 14C measurements with regional references - the post-peak bomb 14C decline period - it was concluded that previous ages were inflated from overcounting of the earliest growth zone structure in otolith sections. The oldest gindai was re-aged to 26 years once the age reading was adjusted for early overcounting, 13 years younger than the original estimate of 39 years for this fish. In general, the earliest otolith growth of gindai was massive and complicated by numerous subannual checks. The approach of lumping the early growth structures was supported by the alignment of 14C measurements from otolith core material (first year of growth). The result was greater consistency of calculated birthdates with the 14C decline reference, along with minor offsets that may indicate age estimation was imprecise by a few years for some individuals. The revised von Bertalanffy growth function applied to the validated age-at-length estimates revealed more rapid growth (k = 0.378 cf. 0.113) and a lifespan of approximately 30 years. The findings presented here are a case study of how the bomb 14C decline period can be used as a tool in the refinement of age reading protocols.