• 제목/요약/키워드: Compounds

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Volatile Compounds Collected by Simultaneous Steam Distillation-Solvent Extraction from Hong Kong Salt-Dried Croakers

  • Kim, Joo-Shin;Chung, Hau Yin
    • Fisheries and Aquatic Sciences
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    • 제11권3호
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    • pp.140-148
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    • 2008
  • We compared the quality and quantity of volatile components in salt-dried croakers prepared by different methods and obtained from different locations. In total, 110 compounds were found among regular- and delay-type salt-dried croakers purchased from two locations in Hong Kong. The major chemical classes included miscellaneous compounds(17), pyrazines(16), alcohols(15), and sulfur-containing compounds(13). Fish obtained in different locations but prepared by the same method differed only slightly in the number of identified compounds. In general, fish prepared by the delay method had a larger number of compounds compared to fish prepared by the regular method. Further, a greater number and higher levels of compounds were found in the fish obtained from one of the two locations. Overall, the delay preparation method resulted in a greater number of compounds with stronger intensity compared to the regular method.

Aminopyrine 분자화합물의 흡수에 관한 연구 (Studies on the absorption of molecular compounds of aminopyrine)

  • 한세호
    • 약학회지
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    • 제13권4호
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    • pp.125-138
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    • 1969
  • The absorptions of aminopyrine, molecular compounds of aminopyrine and mixed compounds of aminopyrine were studies in the small intestine of rats (in situ). The molecular compounds of aminopyrine were more absorbed than aminopyrine and mixed compounds of aminopyrine were less absorbed than aminopyrine in small intestine of rats. The appearent permeability coefficients and the absorption velocity constants of the molecular compound of aminopyrine-barbital were highest and the orders of decreasing in values of permeability coefficients and the absorption velocity constants of the other molecular compounds are as follows: Aminopyrine-secobarbital, Aminopyrine-phenobarbital Aminopyrine-amobarbital, Aminopyrine-cyclobarbital Aminopyrine-allobarbital. The orders of decreasing in values of the appearent permeability coefficients and the absorption velocity constants of the mixed compounds of aminopyrine are as follows: Aminopyrine secobarbital, Aminopyrine allobarbital Aminopyrine cyclobarbital, Aminopyrine amobarbital Aminopyrine phenobarbital, Aminopyrine barbital. The relative absorption rates of aminopyrine, molecular compounds of aminopyrine and the mixed compounds of aminopyrine by the goldfish method and the partition coefficients were correlative to the values of circulation method.

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곤달비 및 곰취의 휘발성 향기성분 비교 (Comparison on Volatile Flavor Compounds in Ligularia stenocephala and Ligularia fischeri Leaves)

  • 최남순
    • 한국식품영양학회지
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    • 제34권4호
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    • pp.340-346
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    • 2021
  • The purpose of this study was to investigate the volatile flavor compounds of Ligularia stenocephala and Ligularia fischeri, edible wild plants. The volatile flavor compounds were isolated by the simultaneous distillation extraction method and analyzed by GC-MSD (gas chromatography-mass selective detector). Forty-eight volatile flavor compounds were identified in the extracts from L. stenocephala and the major compounds were sabinene, cis-ocimene, trans-caryophyllene, and β-elemene. Fifty-one volatile flavor compounds were identified in the extracts from L. fischeri and the major compounds were α-pinene, germacrene-D, transcaryophyllene, endo-1-bourbonanol and 1-limonene. The common volatile flavor compounds between two plants were transcaryophyllene, sabinene, β-elemene and β-cubebene etc. However, α-phellendrene and myrcene were identified in L. stenocephala, but were not identified in L. fischeri. However α-pinene, germacrene-D and limonene were identified in L. fischeri but were not identified in L. stenocephala.

NF막을 이용한 EDCs, PhACs, PCPs 물질의 제거 특성 평가 (Removal Characteristics of Endocrine Disrupting Compounds (EDCs), Pharmaceutically Active Compounds (PhACs) and Personal Care Products (PCPs) by NF Membrane)

  • 장혜원;박찬혁;홍승관;윤여민;정진영;정윤철
    • 상하수도학회지
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    • 제21권3호
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    • pp.349-357
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    • 2007
  • Reports of endocrine disrupting compounds (EDCs), pharmaceutically active compounds (PhACs), and personal care products (PCPs) have raised substantial concern in important potable drinking water quality issues. Our study investigates the removal of EDCs, PhACs, and PCPs of 10 compounds having different physico-chemical properties (e.g., molecular weight, and octanol-water partition coefficient ($K_{OW}$)) by nanofiltration (NF) membranes. The rejection of micropollutants by NF membranes ranged from 93.9% to 99.9% depending on solute characteristics. A batch adsorption experiments indicated that adsorption is an important mechanism for transport/removal of relatively hydrophobic compounds, and is related to the octanol-water partition coefficient values. The transport phenomenon associated with adsorption may also depend on solution water chemistry such as pH and ionic strength influencing the pKa value of compounds. In addition, it was visually seen that the retention was somewhat higher for the larger compounds based on their molecular weight. These results suggest that the NF membrane retains many organic compounds due to both hydrophobic adsorption and size exclusion mechanisms.

V-SDE와 SPME법에 의한 꽃게(Portunus trituberculatus)육의 휘발성 향기성분 비교 (Comparison of Volatile Flavor Compounds in Meat of the Blue Crab Using V-SDE and SPME Methods)

  • 차용준;조우진;정은정
    • 한국수산과학회지
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    • 제39권6호
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    • pp.441-446
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    • 2006
  • Volatile flavor compounds in meat of the blue crab Portunus trituberculatus were compared using vacuum simultaneous steam distillation-solvent extraction (V-SDE) and solid phase microextraction (SPME)/ gas chromatography (GC)/ mass selective detection (MSD) methods. A total of 100 volatile flavor compounds were identified by both methods: 77 by V-SDE and 59 by SPME. These compounds were composed of 17 aldehydes, 12 ketones, 19 alcohols, 5 esters, 4 sulfur-containing compounds, 6 nitrogen-containing compounds, 23 aromatic compounds, 6 hydrocarbons, 2 terpenes, and 6 miscellaneous compounds. Although more compounds were detected using V-SDE than using SPME, the levels of all groups detected, except esters, were higher using SPME than using V-SDE. In addition to trimethylamine, aldehydes, and aromatic compounds, the S- and N-containing compounds with low thresholds are thought to have positive roles for flavors in the meat of the blue crab.

6년생 적변내성 인삼계통의 Phenolic Compounds 함량 특성 (Phenolic Compounds Contents of Rusty-Root Tolerance Ginseng Lines in 6-Year Old Root)

  • 이성식
    • Journal of Ginseng Research
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    • 제26권3호
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    • pp.165-169
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    • 2002
  • 고려인삼의 적변내성 지표성분을 선발하기 위하여 적변지수가 낮아 적변에 강한 건전계통(LRL) 7계통과 적변지수가 높아 적변에 약한 적변계통(HRL) 7계통을 선발하여 시료로 사용하였다. 4년생과 6년생의 적변지수 상관관계는 고도의 유의성을 나타내었다. phenolic compounds 함량이 중심주 및 지세근 조직에서는 차이가 없었다. 피층조직에서는 적변인삼은 건전인삼보다 phenolic compounds 성분 함량이 높았으나, 적변의 정도를 동일하게 한적변계통군와 건전계통군간에는 phenolic compounds 함량의차이가 없어서 지표성분으로 활용 가능성이 없었다. 표피조직에서 적변삼은 건전삼에 비해 phenolic compounds 함량이 높았고, 적변삼이나 건전삼을 시료로 사용 했을 때 모두 적변계통군(HRL)은 건전계통군(LRL)보다 phenolic compounds 함량이 높아서, 적변삼 선발 지표성분으로 활용 가능성이 제시되었다.

Quality Properties of Seasoned-Dried Pacific Saury Treated with Liquid Smoke -1. Volatile Flavor Compounds in Commercial Liquid Smokes-

  • Park Sung-Young;Kim Hun;Cho Woo-Jin;Lee Young-Mi;Lee Jung-Suck;Cha Yong-Jun
    • Fisheries and Aquatic Sciences
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    • 제4권4호
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    • pp.229-237
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    • 2001
  • In order to identify of volatile flavor compounds and polycyclic aromatic hydrocarbons (PAHs) in commercial liquid smokes, this study was conducted to analyze volatile flavor compounds by solvent extraction and/or Purge & Trap method/GC/MSD. A total of 156 volatile flavor compounds were detected in 6 commercial liquid smokes, and these compounds were composed mainly of 12 aldehydes, 60 ketones, 7 alcohols, 14 acids, 20 esters, 24 aromatic compounds, 7 furans and 12 miscellaneous compounds. Ketones $(806.6-7,573.9\mu g/mL)$ and aromatic compounds $(282.6-7,896.3 \mu g/mL)$ were more abundant than others. The PAHs known as carcinogen have not been detected in this study. The acids $(422.9-4,903.1\mu g/mL)$ was identified in relatively high concentration compared to other groups. Phenol and its derivatives among aromatic compounds were in relatively high concentration. Especially, the phenol and its derivatives including o-cresol, guaiacol, 4-ethylguaiacol and syringol were in higher concentration.

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방사선 조사 돼지고기에서 휘발성 조사물질의 구명 (Identification of Irradiation-induced Volatile Flavor Compounds in Irradiated Pork Meats)

  • 차용준;김훈;조우진;정연정;변명우;유영재
    • 생명과학회지
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    • 제11권1호
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    • pp.35-42
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    • 2001
  • Irradiation-induced volatile flavor compounds in irradiated (0, 1, 3, 5, 10 kGy) pork meats were analyzed by liquid liquid continuous extraction (LLCE) and gas chromatography/mass spectrometry (GC/MS) methods. One hundred nine volatile compounds were detected in irradiated pork meats. These compounds were mainly composed of hydrocarbons (42 compounds), aromatic compounds (39), aldehydes(9), ketones(5) and miscellaneous compounds (14). Among these, three volatile compounds, such as decene, 1,2,3,4,-tetrahydro-6-methylnaphthalene and 1,2,3,4-tetrahydro-dimethylnaphthalene were selected as irradiation-induced compounds comparing with irradiation dosages in irradiated pork meats. By the high correlation coefficient with the increment of irradiation dose, however, decene (r=0.93) was considered as marker compound for detecting irradiation dosage in fresh pork meats.

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한국어 복합어와 구의 음향 음성학적 특성 (Acoustic Characteristics of Korean Compounds and Phrases)

  • 이서배
    • 말소리와 음성과학
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    • 제4권1호
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    • pp.49-54
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    • 2012
  • Recent studies on acoustic correlates of stress in English compounds and English phrases have revealed the difference of changes in acoustic manifestation between English compounds and English phrases with different intonation patterns. However, little effort has been made to compare Korean compounds and Korean phrases in different intonational environments. Therefore, this study focuses on the analysis of acoustic characteristics of Korean compounds and Korean phrases produced in different intonational sentence patterns (Subject, Question, Clause-Final, and Statement-Final). Measurements of vowel duration, intensity (dB) and pitch (in semitones) were compared. The results of the experiment in which 30 native speakers of Korean pronounced Korean compounds and Korean phrases (obtained from $8{\times}30$ sentences) in controlled prosodic and intonational environments reveal clear patterns that distinguish Korean compounds from Korean phrases and support the evidence of acoustic salience for phrases. Duration differences turned out to be a significant cue to distinguish Korean compounds and Korean phrases in all but the Clause Final position. According to the size effect, duration ratio is the most reliable cue to distinguish Korean compounds and Korean phrases followed by the pitch differences between the first syllable and the second syllable and the intensity ratio. Implications for Korean and English intonation training were also discussed.

ACGIH TLV가 전면 개정된 알루미늄 화합물의 노출기준 관리 (Management of OELs for Aluminum Compounds with Completely Revised ACGIH TLVs)

  • 박승현;김세동
    • 한국산업보건학회지
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    • 제30권3호
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    • pp.249-255
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    • 2020
  • Objective: The purpose of this study was to provide technical information about the management of occupational exposure limits(OELs) for substances with completely revised ACGIH TLVs. Methods: The history of ACGIH TLVs for aluminum compounds, the reason for the complete revision of the related ACGIH TLV in 2008, and OELs for them in respective countries were reviewed. In addition, the results of a 2019 work environment assessment for aluminum compounds in Korea were reviewed. Results: In 1979, the ACGIH set up the TLVs for aluminum compounds considering types of compounds such as metal dust, pyro powders, welding fumes, soluble salts, alkyls, and aluminum oxide. However, in 2008 the ACGIH withdrew the TLVs for all types of aluminum and its compounds and adopted new TLVs for aluminum metal and insoluble compounds. This can cause confusion in many countries in the management of exposure to aluminum compounds because they adopt or refer to the ACGIH TLVs. Conclusion: Although Korea is setting occupational exposure limits by referring to the ACGIH's TLVs, it is necessary to sufficiently review whether it is necessary to accept the TLVs as they are if a TLV is completely changed, like took place with the revision of aluminum compounds in 2008.