• 에너지공학
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• 제20권2호
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• pp.90-95
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• 2011

이 연구는 압축천연가스자동차용 Type III 용기 복합재에 발생한 스크래치, 컷, 가우지 등의 손상을 평가하여 계속 사용여부를 판정하기 위해 수행하였다. 결함내구성 시험결과, 복합재의 손상등급에 따라 ISO 19078에서 정한 최소요구 반복회수(11,250회)는 모두 만족하였고 용기의 반복성능은 손상등급 1, 2에서는 20,000회를 상회하다가 손상등급 3에서는 18,000~21,000회의 범위를 나타내었다. 실험용기 12개 중 8개가 Type III 용기복합재 결함의 영향을 받아 파괴되었고 나머지는 결함과 관계없이 파괴된 것으로 판단된다. 전산모사에 의한 구조해석결과는 $1.25\;mm{\times}200\;mm$의 결함모델에 사용압이 가해졌을 때 발생한 응력은 79.5 MPa이고 무결함 용기의 라이너 평탄부에 발생한 응력은 66.6 MPa로서 약 19.37%의 차이가 발생하였다. 이것은 라이너의 피로수명에 영향을 미칠 수 있는 차이로 볼 수 있고 이 결함은 용기의 반복성능에 영향을 미치는 임계값으로 판단할 수 있었다.

• Structural Engineering and Mechanics
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• 제32권3호
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• pp.429-445
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• 2009

Thermal stability of quasi-isotropic composite and polymeric structures is considered one of the most important criteria in predicting life span of building structures. The outdoor applications of these structures have raised some legitimate concerns about their durability including moisture resistance and thermal stability. Exposure of such quasi-isotropic composite/polymeric structures to various and severe climatic conditions such as heat flux and frigid climate would change the material behavior and thermal viability and may lead to the degradation of material properties and building durability. This paper presents an analytical model for the generalized problem. This model accommodates the non-linearity and the non-homogeneity of the internal heat generated within the structure and the changes, modification to the material constants, and the structural size. The paper also investigates the effect of the incorporation of the temperature and/or material constant sensitive internal heat generation with four encountered climatic conditions on thermal stability of infinite cylindrical quasi-isotropic composite/polymeric structures. This can eventually result in the failure of such structures. Detailed critical analyses for four case studies which consider the population of the internal heat generation, cylindrical size, material constants, and four different climatic conditions are carried out. For each case of the proposed boundary conditions, the critical thermal stability parameter is determined. The results of this paper indicate that the thermal stability parameter is critically dependent on the cylinder size, material constants/selection, the convective heat transfer coefficient, subjected heat flux and other constants accrued from the structure environment.

• 한국해양공학회지
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• 제21권3호
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• pp.52-57
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• 2007

Composite material is one of the strongest candidates for deep see pressure hulls. Research regarding composite cylinders, subjected to hydrostatic pressure, has been ongoing for a couple of decades, abroad, but domestic research is very new. Experimental investigations seem necessary, in order to understand their structural behavior not only up to the ultimate limit state, but in the post-ultimate regime. That experimental information will be very helpful in the development of any theoretical methods or to substantiate any commercial numerical packages for structural analyses. In this study, ultimate strength tests on seven composite cylinders subjected to hydrostatic pressure are reported, which includes the fabrication method of models, mechanical properties of the material, initial shape imperfection measurements, test procedure, and strain and axial shortening measurements during the tests. The ultimate strengths of the models were compared with predictions of numerical analyses. The numerical predictions are higher than the test results. It seems necessary to improve the accuracy of the numerical predictions by considering the initial shape and material imperfections.

• 한국항공우주학회지
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• 제35권3호
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• pp.196-203
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• 2007

외부 수압을 받는 복합재 원통의 좌굴 후 거동과 파손을 유한요소법과 시험으로 연구하였다. 좌굴 후 점진적 파손해석을 위해서는 비선형 유한요소해석 프로그램인 ACOS를 사용하였다. 유한요소해석의 타당성 검증을 위해 5개의 복합재 원통 모델을 제작하여 수압 시험을 수행하였다. 또한 상용 유한요소해석 프로그램인 MSC/NASTRAN과 MSC/MARC를 이용한 해석을 병행하여 ACOS에 의한 결과와 비교하였다. 세 개의 프로그램 중 ACOS가 실험과 가장 가까운 좌굴압력을 예측하였고, 한 경우를 제외하면, 실험값과는 약 12～26% 정도의 차이를 보였다. 해석에서는 원주방향으로 네 개의 웨이브를 가지는 전체 좌굴이 나타나지만, 실제 시험에서는 원통의 기하학적 초기결함으로 인해 국부좌굴이 발생하여 최종파손으로 연결되었다.

• Restorative Dentistry and Endodontics
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• 제38권4호
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• pp.241-247
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• 2013

Objectives: The aim of this study was to determine the effect of epigallocatechin gallate (EGCG) on the shear bond strength of composite resin to bleached enamel. Materials and Methods: Ninety enamel surfaces of maxillary incisors were randomly divided into 9 groups as follows: G1: control (no bleaching); G2: bleaching; G3: bleaching and storage for seven days; G4 - 6: bleaching and application of 600, 800 and 1,000 ${\mu}mol$ of EGCG-containing solution for 10 minutes, respectively; G7 - 9: bleaching and application of 600, 800 and 1,000 ${\mu}mol$ of EGCG-containing solution for 20 minutes, respectively. The specimens were bleached with 30% hydrogen peroxide gel and a composite resin cylinder was bonded on each specimen using a bonding agent. Shear bond strength of the samples were measured in MPa. Data was analyzed using the two-way ANOVA and Tukey HSD tests (${\alpha}$ = 0.05). Results: The maximum and minimum mean shear bond strength values were observed in G1 and G2, respectively. Time and concentration of EGCG showed no significant effects on bond strength of the groups (p > 0.05). Multiple comparison of groups did not reveal any significant differences between the groups except for G2 and all the other groups (p < 0.05). Conclusions: There is a significant decrease in bond strength of composite resin to enamel immediately after bleaching. A delay of one week before bonding and the use of EGCG increased bond strength of composite resin to bleached enamel.

• The Journal of Advanced Prosthodontics
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• 제4권4호
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• pp.187-191
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• 2012

PURPOSE. The aim of the present study was to assess the effect of ascorbic acid, ethanol and acetone on microtensile bond strength between fiber posts pre-treated with hydrogen peroxide and composite resin cores. MATERIALS AND METHODS. Twenty four fiber posts were pre-treated with 24% hydrogen peroxide and divided into 4 groups as follows: G1: no treatment, as control group; G2: treatment with10% ascorbic acid solution for 5 minutes; G3: treatment with 70% ethanol solution for 5 minutes; and G4: treatment with 70% acetone solution for 5 minutes. Each fiber post was surrounded by a cylinder-shaped polyglass matrix which was subsequently filled with composite resin. Two sections from each sample were selected for microtensile test at a crosshead with speed of 0.5 mm/min. Statistical analyses were performed using one-way ANOVA and a post hoc Tukey HSD test. Fractured surfaces were observed under a stereomicroscope at ${\times}20$ magnification. The fractured surfaces of the specimens were observed and evaluated under a SEM. RESULTS. Means of microtensile bond strength values (MPa) and standard deviations in the groups were as follows: G1: $9.70{\pm}0.81$; G2: $12.62{\pm}1.80$; G3: $16.60{\pm}1.93$; and G4: $21.24{\pm}1.95$. G4 and G1 had the highest and the lowest bond strength values, respectively. A greater bond strength value was seen in G3 compared to G2. There were significant differences between all the groups (P<.001). All the failures were of the adhesive mode. CONCLUSION. Application of antioxidant agents may increase microtensile bond strength between fiber posts treated with hydrogen peroxide and composite cores. Acetone increased bond strength more than ascorbic acid and ethanol.

• Restorative Dentistry and Endodontics
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• 제45권2호
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• pp.13.1-13.10
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• 2020

Objective: The aim of this study was to evaluate the influence of different modeling agents on the surface microhardness (Vickers hardness number; VHN), roughness (Ra), and color change (ΔE) of a nano-hybrid composite with or without exposure to discoloration by coffee. Materials and Methods: Sixty-four cylinder-shaped nano-hybrid composite specimens were prepared using a Teflon mold. The specimens' surfaces were prepared according to the following groups: group 1, no modeling agent; group 2, Modeling Liquid; group 3, a universal adhesive (G-Premio Bond); and group 4, the first step of a 2-step self-adhesive system (OptiBond XTR). Specimens were randomly allocated into 2 groups (n = 8) according to the storage medium (distilled water or coffee). VHN, Ra, and ΔE were measured at 24 hours, 1 week, and 6 weeks. The Kruskal-Wallis test followed by the Bonferroni correction for pairwise comparisons was used for statistical analysis (α = 0.05). Results: Storage time did not influence the VHN of the nano-hybrid composite in any group (p > 0.05). OptiBond XTR Primer application affected the VHN negatively in all investigated storage medium and time conditions (p < 0.05). Modeling Liquid application yielded improved Ra values for the specimens stored in coffee at each time point (p < 0.05). Modeling Liquid application was associated with the lowest ΔE values in all investigated storage medium and time conditions (p < 0.05). Conclusion: Different types of modeling agents could affect the surface properties and discoloration of nano-hybrid composites.

• Restorative Dentistry and Endodontics
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• 제26권4호
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• pp.332-340
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• 2001

Flowable composite resin has lower filler content, increased flow, and lower modules of elasticity. It is suggested that flowable composite resin can be bonded to the tooth structure intimately and absorb or dissipate the stress. Therefore, it may be advantageous to use flowable composite resin for the base material of class II restoration and for the class V restoraton. The purpose of this study was to evaluate the microleakage and shear bond strength of four flowable composite resins (Aeliteflo, Flow-It, Revolution, Ultraseal XT Plus) compared to Z100 using Scotchbond Multi Purpose dentin bonding system. To evaluate the microleakage, notch-shaped class V cavities were prepared on buccal and lingual surfaces of 80 extracted human premolars and molars on cementum margin. The teeth were randomly divided into non-thermocycling group (group 1) and thermocycling group (group 2) of 40 teeth each. The experimental teeth of each group were randomly divided onto five subgroups of eight samples (sixteen surfaces). The Scotchbond Multi-Purpose and composite resin were applied for each group following the manufacturer's instructions. the teeth of group 2 were thermocycled five hundred times between 5$^{\circ}C$ and 55$^{\circ}C$. The teeth of group 2 were placed in 2% methylene blue dye for 24 hours, then rinsed with tab water. The specimens were embedded in clear resin, and sectioned longitudinally with a diamond saw. The dye penetration on each of the specimen were observed with a stereomicioscope at $\times$20 magnification. To evaluate the shear bond strength, 60 teeth were divided into five groups of twelve teeth each. The experimental teeth were ground horizontally below the dentinoenamel junction, so that no enamel remained. After applying Scotchbond Multi-Purpose on the dentin surface, composite resin was applied in the shape of cylinder. The cylinder was 4mm in diameter and 2mm in thickness. Shear bond strength was measured using Instron with a cross-head speed of 0.5mm/min. After shear bond strength measurement, mode of failure was evaluated with a stereomicroscope at $\times$30 magnification. All data were statistically analyzed by One Way ANOVA and Student-Newman-Keuls method. The correlation between microleakage and shear bond strength was analyzed by linear regression. The results of this study were as follows ; 1. In non-thermocycling group, the leakage value of Z100 was significantly lower than those of flowable composite resins at the enamel and dentin margin, margin, except that Revolution showed the lower leakage value than that of Z100 at the dentin margin (p<0.05). 2. In thermocycling group, the leakage values of Z100 and Ultraseal XT Plus were lower than those of other subgroup at the enamel and dentin margin, except that Flow-It showed the lower leakage value than that of Ultraseal XT Plus at the dentin margin (p<0.05). 3. The leakage value of Z100 and Ultraseal XT Plus in thermocycling group were not higher than that in non-thermocycling group at the enamel margin. The leakage value of Z100 in thermocycling group was not higher than that in non-thermocycling group at the dentin margin (p<0.05). 4. As for the shear bond strength measurement, there were no statistically significant differences among groups (p<0.05). The shear bond strengths given in descending order were as follows: Z100(16.81$\pm$2.98 MPa), Flow-It(14.8$\pm$4.43 MPa), Aeliteflo(14.34$\pm$3.69 MPa), Revolution(13.46$\pm$4.23 MPa), Ultraseal XT Plus(12.83$\pm$3.16 MPa). 5. Failure modes of all specimens were adhesive failures. 6. There was no correlation between microleakage and shear bond strength.

• 한국유체기계학회 논문집
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• 제19권3호
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• pp.53-56
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• 2016

In this study, experiments and finite element method analysis were used to determine the autofrettage pressure that is optimal and then maximizes the cycling life of Type3 composite cylinders used in self-contained breathing apparatus. For both approaches, the cylinders were pressurized at 100, 110, ${\ldots}$, 290 % of the test pressure, respectively. The stresses were computed by the FEM analysis; while the strains of cylinders were recorded and the failure modes were monitored during the cycling test. As a result, from the good agreements between the simulations and experiments, it was concluded that at least 70 % of the test pressure should be applied as the autofrettage pressure in order to takes visible effect on the cycling life, and 160 % of the test pressure induces the maximum cycling life and the desired failure mode.

• 항공우주기술
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• 제9권1호
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• pp.72-77
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• 2010

필라멘트 와인딩으로 제작된 고체 모터 연소관의 구조강성저하 평가 및 파열특성을 확인하기 위한 수압시험을 수행하였다. 본 연소관의 파손 요구조건으로서 운용 중 최대 예상압력(MEOP)의 1.5배 이상의 압력에서 실린더 파손이 일어나야함을 제시하였다. 해석 결과 연소관의 내부압력이 2088psig 일 때 실린더층의 섬유가 끊어지는 것으로 나타났으며 수압시험을 수행하여 2200psig 수준에서 실린더 부위가 파손됨을 검증하였다. 또한 제작 후 1년 정도 경과 후에도 강성저하가 없음을 알 수 있었다.