• Korean Journal of Materials Research
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• v.29 no.4
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• pp.221-227
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• 2019

This study examines the role of the nano- and micro-particle ratio in dispersion stability and mechanical properties of composite resins for SLA(stereolithography) 3D printing technology. VTES(vinyltriethoxysilane)-coated $ZrO_2$ ceramic particles with different nano- and micro-particle ratios are prepared by a hydrolysis and condensation reaction and then dispersed in commercial photopolymer (High-temp) based on interpenetrating networks(IPNs). The coating characteristics of VTES-coated $ZrO_2$ particles are observed by FE-TEM and FT-IR. The rheological properties of VTES-coated $ZrO_2/High-temp$ composite solution with different particle ratios are investigated by rheometer, and the dispersion properties of the composite solution are confirmed by relaxation NMR and Turbiscan. The mechanical properties of 3D-printed objects are measured by a tensile test and nanoindenter. To investigate the aggregation and dispersion properties of VTES-coated $ZrO_2$ ceramic particles with different particle ratios, we observe the cross-sectional images of 3D printed objects using FE-SEM. The 3D printed objects of the composite solution with nano-particles of 80 % demonstrate improved mechanical characteristics.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.41 no.8
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• pp.665-672
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• 2013

One of the major causes of stiffness and strength degradations in laminated composite structures is the delamination between composite layers. In most engineering applications, laminated composite structures have certain curvatures. If the curved composite structure is subjected to bending that tends to flatten the composite structures, through the thickness stresses can be generated in the thickness direction of the composites. Under normal operation open mode delamination could occur at the sites of peak interlaminar stress. This paper describes a technique to determine radial direction stress of a laminated composite structure using a curved beam. Stacking sequence effects of interlaminar stress were studied. The radial location and intensity of the open mode delamination stress were calculated and compared with the results obtained from the analytical solution and finite element method.

• International Journal of Highway Engineering
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• v.19 no.1
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• pp.45-52
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• 2017

PURPOSES : The main purpose of this study is to develop a high elastic modulus and low-shrinkage roller-compacted concrete base (RCCB) in order to prevent fatigue cracking and reflective cracking in the asphalt surface layer of composite pavement. Using a rigid base material with low shrinkage can be a solution to this problem. Moreover, a strong rigid base with high elastic modulus is able to shift the location of critical tensile strain from the bottom of the asphalt layer to the bottom of the rigid base layer, which can prevent fatigue cracking in the asphalt layer. METHODS : Sensitivity analysis of composite pavement via numerical methods is implemented to determine an appropriate range of elastic modulus of the rigid base that would eliminate fatigue cracking. Various asphalt thicknesses and elastic moduli of the rigid base are used in the analysis to study their respective influences on fatigue cracking. Low-shrinkage RCC mixture, as determined via laboratory testing with various amounts of a CSA expansion agent (0%, 7%, and 10%), is found to achieve an appropriate low-shrinkage level. Shrinkage of RCC is measured according to KS F 2424. RESULTS : This study shows that composite pavements comprising asphalt thicknesses of (h1) 2 in. with E2 > 19 GPa, 4 in. with E2 > 15 GPa, and 6 in. with E2 > 11 GPa are able to eliminate tensile strain in the asphalt layer, which is the cause of fatigue cracking in this layer. Shrinkage test results demonstrate that a 10% CSA RCC mixture can reduce shrinkage by 84% and 93% as compared to conventional RCC and PCC, respectively. CONCLUSIONS : According to the results of numerical analyses using various design inputs, composite pavements are shown to be able to eliminate fatigue cracking in composite pavement. Additionally, an RCC mixture with 10% CSA admixture is able to reduce or eliminate reflective cracking in asphalt surfaces as a result of the significant shrinkage reduction in the RCC base. Thus, this low-shrinkage base material can be used as an alternative solution to distresses in composite pavement.

• Restorative Dentistry and Endodontics
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• v.25 no.3
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• pp.482-486
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• 2000

The purpose of the present study was first, to evaluate the relationship between composite surface conversion and surface discoloration, second, to know if there was difference in surface discoloration between celluloid-strip-finished composite surface and polished surface. In addition, the discoloration of composite surface was also evaluated with visual inspection or digital camera with high resolution monitor, Z100, Tetric Ceram, Spectrum, and Aelitfil were used. The composite surfaces were celluloid-strip finished (group 1), polished (group 2), celluloid-strip finished under nitrogen gas purging (group 3) or only light cured without finishing or polishing under nitrogen gas purging (group 4). The microhardness of each samples were also measured in each group. The samples of each group were also divided into 4 subgroup whether they were immediately placed in disclosing solution (0.2% Elythrosin, pH 7.0) (subgroup1), 1 day after light curing(subgroup 2), 3day after light curing(subgroup 3) or 7 day after light curing(subgroup 4). The computer controlled spectrophotometer was used to determine CIELAB coordinates ($L^*$, $a^*$, $b^*$). The amounts of color difference were compared. The results were as follows; 1. There was no difference in discoloration between celluloid strip finished composite surface and polished surface. 2. The samples discolored more when they were placed in disclosing solution immediately after polymerization than other groups. 3. When the samples were light cured under nitrogen gas purging and without polishing process, they discolored more than other groups even though they showed higher micro hardness. 4. With visual inspection or digital camera, only a limited information was available in detecting composite surface discoloration.

• Structural Engineering and Mechanics
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• v.12 no.2
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• pp.135-156
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• 2001

Analytical solutions and finite element results of laminated composite plates with smart material layers embedded in them are presented in this study. The third-order plate theory of Reddy is used to study vibration suppression characteristics. The analytical solution for simply supported boundary conditions is based on the Navier solution procedure. The velocity feedback control is used. Parametric effects of the position of the smart material layers, material properties, and control parameters on the suppression time are investigated. It has been found that (a) the minimum vibration suppression time is achieved by placing the smart material layers farthest from the neutral axis, (b) using thinner smart material layers have better vibration attenuation characteristics, and, (c) the vibration suppression time is larger for a lower value of the feedback control coefficient.

• Transactions on Electrical and Electronic Materials
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• v.15 no.4
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• pp.193-197
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• 2014

Si-carbon composites as anode materials for lithium rechargeable batteries were prepared simply by mixing Si nanoparticles with carbon black and/or graphite through a solution process. Si nanoparticles were well dispersed and deposited on the surface of the carbon in a tetrahydrofuran solution. Si-carbon composites showed more than 700 mAh/g of initial capacity under less than 20% loading of Si nanoparticle in the composites. While the electrode with only Si nanoparticles showed fast capacity fading during continuous cycling, Si-carbon composite electrodes showed higher capacities. The cycle performances of Si nanoparticles in composites containing graphite were improved due to the role of the graphite as a matrix.

• Textile Coloration and Finishing
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• v.9 no.1
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• pp.23-32
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• 1997

Composite membranes having different mixing ratio of Wool(SCMK) and poly(ethylene terephthalate) (PET) were prepared by dissolving wool/PET in hexafluoro-2-propanol(HFIP), casting the obtained solution on a glass plate and evaporation the solvent in the presence and absence of an electric field. The internal structure of the prepared membrane was investigated using polarise microscope dyeing and dye permeation method. In the composite membrane prepared under electric field, both components were micro mixing, while in the membranes prepared under nonelectric field, the two components formed a random sea/island structure according to different mixing ratio. Such characteristic membrane structure was influenced the permeation behavior of C.I. Acid Red 118 through the membranes from an aqueous solution.

• Steel and Composite Structures
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• v.14 no.3
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• pp.283-293
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• 2013

This paper deals with the applicability of a new extended layerwise optimization method for thermal buckling load optimization of laminated composite plates. The design objective is the maximization of the critical thermal buckling of the laminated plates. The fibre orientations in the layers are considered as design variables. The first order shear deformation theory (FSDT) is used for the finite element solution of the laminates. Finally, the numerical analysis is carried out to show the applicability of extended layerwise optimization algorithm of laminated plates for different parameters such as plate aspect ratios and boundary conditions.

• Journal of Integrative Natural Science
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• v.6 no.3
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• pp.183-186
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• 2013

Well defined 1-dimentional (1-D) photonic crystals of polystyrene replicas have been successfully obtained by removing the porous silicon from the free-standing rugate porous silicon/phenylmethylpolysiloxane composite film. Rugate porous silicon was prepared by an electrochemical etching of silicon wafer in HF/ethanol mixture solution. Exfoliated rugate porous silicon was obtained by an electropolishing condition. A composite of rugate porous silicon/phenylmethylpolysiloxane composite film was prepared by casting a toluene solution of phenylmethylpolysiloxane onto the top of rugate porous silicon film. After the removal of the template by chemical dissolution, the phenylmethylpolysiloxane castings replicate the photonic features and the nanostructure of the master. The photonic phenylmethylpolysiloxane replicas are robust and flexible in ambient condition and exhibit an excellent reflectivity in their reflective spectra. The photonic band gaps of replicas are narrower than that of typical semiconductor quantum dots.

• Steel and Composite Structures
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• v.21 no.4
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• pp.883-919
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• 2016

In this research, buckling analysis of an embedded laminated composite plate is investigated. The elastic medium is simulated with spring constant of Winkler medium and shear layer. With considering higher order shear deformation theory (Reddy), the total potential energy of structure is calculated. Using Principle of Virtual Work, the constitutive equations are obtained. The analytical solution is performed in order to obtain the buckling loads. A detailed parametric study is conducted to elucidate the influences of the layer numbers, orientation angle of layers, geometrical parameters, elastic medium and type of load on the buckling load of the system. Results depict that the highest buckling load is related to the structure with angle-ply orientation type and with increasing the angle up to 45 degrees, the buckling load increases.