• Korean Journal of Materials Research
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• v.8 no.11
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• pp.993-998
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• 1998

In this study TiNi/A16061 shape memory composite is introduced as one of new material using a shape memory alloy. High tensile strength of composite due to compressive residual stress in matrix by the shape memory effect of TiNi fiber can be produced. This composite can remove the tensile residual stress by the difference of coefficients of thermal expansion between fiber and matrix. one of the significant weak point of metal matrix composite. In this paper, shape memory composites are made by squeeze casting. And then, microstructure and fatigue properties of the composites by shape memory effect above inverse transformation temperature A, of TiNi alloy are discussed. The results of the fatigue crack control properties of TiNi/A16061 shape memory composite by a squeeze casting are summarized as follows the effect of fatigue crack propagation control at 363K increases according to the increase of volume fraction and prestrain in composites.

• Composites Research
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• v.33 no.5
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• pp.241-246
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• 2020

In this study, aluminum (Al) alloy matrix composites in which B₄C particles were uniformly dispersed was manufactured through stir casting followed by hot rolling process. The microstructure, mechanical properties, and wear resistance properties of the prepared composites were analyzed. The composite in which the 40 ㎛ sized B₄C particles were uniformly dispersed increased the tensile strength and improved wear performance as the volume ratio of the reinforcement increased. In the case of the 20 vol.% composite, the tensile strength was 292 MPa, which was 155% higher than that of the Al6061. As a result of the wear resistance test, the wear width and depth of the 20 vol.% B₄C/Al6061 composites were 856 ㎛, and 36 ㎛, and the friction coefficient was 0.382, which were considerably superior to Al6061.

• Journal of Korea Foundry Society
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• v.20 no.6
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• pp.377-385
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• 2000

Al matrix composites as the most promising MMCs can be expected to be excellent engineering materials in the nearest future. So as to improve material properties of composite, many manufacturing processes have been developed. Among them, squeeze casting process which offers fine microstructure and near-net-shape is one of the most successful MMCs manufacturing processes. But, in case of with subsieve size particles (under 44 ${\mu}m$), it is very difficult to homogeneously distribute particles in matrix of Al matrix composite by various casting processes, including squeeze casting used so far. Duplex process which was developed in previous study was used to distribute the particle of subsieve size more homogeneously in matrix of Al matrix composite. Microstructures, wear and heat resistance characterization of Al-Si-Cu-Mg-(Ni)/SiCp manufactured by duplex process were examined to clarify the effect of manufacturing conditions, particle size of reinforcement and alloying elements. Al matrix composites reinforced with SiCp(10 ${\mu}m$) have the lowest wear amount among composites reinforced with 3 ${\mu}m$, 5 ${\mu}m$ and 10 ${\mu}m$ SiCp. The wear amount of Al matrix composites with 10 wt.% SiCp(3, 5, 10 ${\mu}m$) was decreased according to the increase of the sliding speed because abrasive wear takes place at high sliding speed of 4m/s and worn debris with block type occurs at low sliding speed of 1m/s. As for heat resistance, it is made clear that remarkable heat resistance property can be obtained by addition of Ni element in Al matrix composites.

• Journal of Korea Foundry Society
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• v.19 no.6
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• pp.493-500
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• 1999

Squeeze casting was used for fabricating a light metal base composite having high strength and wearresistance. Reactive sintering was used to prepare the preform of Squeeze casting. To utilize Fe-Al intermetallic compounds and SiC particle as a reinforcement, there needs to prepare Fe-Al mixed powder at 50, 60, 70at.%Al, and add SiC powder to the above mixture at 4, 7, 16, 24wt.%. The prepared mixture with SiC was reactive sintered in a tube furnace at $660^{\circ}C$ to get a porous hybrid preform of intermetallic compound and SiC. The preform prepared above was placed in a metal mold, preheated at $660^{\circ}C$ AC4C matrix was injected into the mold with the temperature of the melt at $610^{\circ}C$ After these processes, 66MPa was applied to the mold for 5 minute to finish the whole procedure. The maximum reaction temperature was increased with the increased Al amount, but decreased with the increased SiC amount. The density of the preform was decreased with SiC amount increase in the compacts due to swelling of the preform. An optical microscope was applied to observe the micro structure and the dispersion of the reinforcements. To analyze phases, We utilized XRD, EDS. Hardness test were chosen to get the information of mechanical properties. There were no significant changes in micro structure between the composite and preform. However, it was shown that uniform dispersion of the reinforcers and complete infiltration of the melt into the preform were achieved through the procedure of the squeeze casting. It was observed that the hardness of the composite is decreased with increased SiC amount, resulting from the volumetric expansion of the preform.

• Journal of the Korean Society of Propulsion Engineers
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• v.4 no.1
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• pp.65-73
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• 2000

Casting of metal matrix composites is an attractive process since it offers a wide selection of materials and processing conditions. Among the casting methods, melt-stirring technology is much attractive route in industrial application because it is more simple and inexpensive compared to squeeze casting or powder metallurgy. In the present work, effects of particle size, volume fraction of particles and mg addition on mechanical properties and thermal expansion coefficients of $\alpha$ -$Al_2O_{3(p)}$/LXA composites were studied. It is shown that $\alpha$ -$Al_2O_3$ particles formed at the interface of $\alpha$ -$Al_2O_3$ particles and matrix made an important role on mechanical properties. Ultimate tensile strength of most composite materials was not increased. But in the case of 5vol% addition of 16$\mu\textrm{m}$ $\alpha$ -$Al_2O_3$ Particle, Ultimate tensile strength of composite materials with 3wt.% Mg was increased. Volume fraction of reinforcements and mg content were thermal expansion coefficients of composite materials were decreased.

• Journal of the Korean Ceramic Society
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• v.52 no.5
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• pp.320-324
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• 2015

Optimization of the fabrication process of NiO-yttrium doped barium zirconate (BZY) composite anode substrates using tape-casting for high performance thin-film protonic ceramic fuel cells (PCFCs) is investigated. The anode substrate is composed of a tens of microns-thick anode functional layer laminated over a porous anode substrate. The macro-pore structure of the anode support is induced by micron-scale polymethyl methacrylate (PMMA) pore formers. Thermal gravity analysis (TGA) and a dilatometer are used to determine the polymeric additive burn-out and sintering temperatures. Crystallinity and microstructure of the tape-cast NiO-BZY anode are analyzed after the sintering.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2000.04a
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• pp.31-37
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• 2000

Metal matrix composites(MMCs) are rapidly becoming one of the strongest candidates for structural materials for many high temperature application. Among the high temperature environment, thermal shock is known to cause significant degradation in most MMC system. Therefore, the nondestructive evaluation on thermal shock damage behavior of SiC/A16061 composite has been carried out using ultrasonic surface and SH-waves. For this study, Sic fiber reinforced metal matrix composite specimens fabricated by a squeeze casting technique were thermally cycled in the temperature range 25~$400^{\circ}C$ up to 1000 cycles. Three point bend test was conducted to investigate the effect of thermal shock damage on mechanical properties. The relationship between thermal shock damage behavior and the change of ultrasonic velocity and attenuation were discussed by considering SEM observation of fracture surface.

• Design & Manufacturing
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• v.6 no.1
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• pp.95-100
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• 2012

In this study, a novel Cu composite sheet with embedded high electric conduction path was developed as another alternative for the interconnect materials possessing high electrical conductivity as well as high strength. The Cu composite sheet was fabricated by forming Ag conduction paths not within the interior but on the surface of a high strength Cu substrate by damascene electroplating process. As a result, the electrical conductivity increased by 40% thanks to mesh type Ag conduction paths, while the ultimate tensile strength decreased by 20%. The interfacial fracture resistance of Cu composite sheet prepared by damascene electroplating increased by above 50 times compared to Cu composite sheet by conventional electroplating. For feasibility test for practical application, a leadframe for LED module was manufactured by a progressive blanking and piercing processes, and the blanked surface profile was evaluated as a function of the volume fraction of Ag conduction paths. As Ag conduction path became finer, pressing formability improved.

• Journal of the Korean Ceramic Society
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• v.36 no.10
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• pp.1123-1131
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• 1999

Alumina-glass composites which are considered as the material of the choice for all dental crown was prepared by aqeous-based tape casting and sintering for 2h at 1120$^{\circ}C$ followed by glass infiltration for 2h at 1100$^{\circ}C$ Biaxial strength and fracture toughness of the composites were evaluated to determine the optimum composition of the tape as a function of the amount of constituent such as alumina binder and plasticizer. The strength and the fracture toughness of the alumina tape increased with increasing the contents of alumina and binder. These observations are consistent with in fluence of the constituents on mean alumuna particle distance in tapes suggesting that high strength of the glass infiltrated alumina composites is related to toughening by crack bowing. The biaxial strength and the fracture toughness of the composite containing the optimum constituent composition were 523 MPa and 3.3 MPa$.$1/2 respectively.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.327-328
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• 2006

We have demonstrated that textured $Al_2O_3-mullite-SiC$ nanocomposites can be fabricated by slip casting followed by partial oxidation - reaction sintering of mixed suspensions of $Al_2O_3$ and SiC powders in a high magnetic field. The sintered density was changed by the degree of oxidation at 1200C and 1300C. The degree of orientation of alumina in the nanocomposite was examined on the basis of the X-ray diffraction patterns and scanning electron micrographs. It is confirmed that alumina-oriented nanocomposites were fabricated. The three-point bending strength at room temperature was observed for the nanocomposites.