• 한국재료학회지
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• 제8권11호
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• pp.993-998
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• 1998

본 연구는 형상기억합금을 이용하여 제조한 신소재 중의 하나인 형상기억복합재료를 소개하고자 한다. 이 복합재료는 TiNi 섬유의 형상기억효과로 금속복합재료의 취약점이라 할 수 있는 기지와 섬유간의 열팽창차이로 인한 인장잔류응력을 제거하고 기지내에 압축잔류응력을 발생시켜 높은 인장강도를 갖는다. 따라서 본 연구에서는 용탕단조법으로 복합재료를 제조한 후 미세조직을 관찰하고 TiNi 섬유의 역변태온도 이상에서 피로실험을 수행하여 복합재료의 피로특성을 검토하였다. 이 결과 363K에서의 피로균열전파제어효과는 섬유체적률과 예변형에 의하여 증가된다.

• Composites Research
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• 제33권5호
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• pp.241-246
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• 2020

본 연구에서는 교반주조 공정을 통해 B₄C 입자가 균일하게 분산된 알루미늄 금속복합재료를 제조하고 후 공정으로 열간압연을 수행하였다. 제조된 복합재료의 미세조직, 기계적 특성 및 내마모 특성에 대해 분석하였다. 40 ㎛ 크기의 B₄C 입자가 균일하게 분산된 복합재료는 강화재의 체적율이 증가함에 따라 인장강도는 증가하였으며, 마모 성능도 개선되었다. 20 vol.% 복합재료의 경우 인장강도 값은 292 MPa로 기지재인 Al6061 대비 155% 증가하였다. 내마모시험 결과 20 vol.% 복합재료의 경우 마모 너비와 깊이가 각각 856 ㎛, 36 ㎛이며, 마찰계수는 0.382로 Al6061 대비 상당히 우수한 내마모 특성을 나타내었다.

• 한국주조공학회지
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• 제20권6호
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• pp.377-385
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• 2000

Al matrix composites as the most promising MMCs can be expected to be excellent engineering materials in the nearest future. So as to improve material properties of composite, many manufacturing processes have been developed. Among them, squeeze casting process which offers fine microstructure and near-net-shape is one of the most successful MMCs manufacturing processes. But, in case of with subsieve size particles (under 44 ${\mu}m$), it is very difficult to homogeneously distribute particles in matrix of Al matrix composite by various casting processes, including squeeze casting used so far. Duplex process which was developed in previous study was used to distribute the particle of subsieve size more homogeneously in matrix of Al matrix composite. Microstructures, wear and heat resistance characterization of Al-Si-Cu-Mg-(Ni)/SiCp manufactured by duplex process were examined to clarify the effect of manufacturing conditions, particle size of reinforcement and alloying elements. Al matrix composites reinforced with SiCp(10 ${\mu}m$) have the lowest wear amount among composites reinforced with 3 ${\mu}m$, 5 ${\mu}m$ and 10 ${\mu}m$ SiCp. The wear amount of Al matrix composites with 10 wt.% SiCp(3, 5, 10 ${\mu}m$) was decreased according to the increase of the sliding speed because abrasive wear takes place at high sliding speed of 4m/s and worn debris with block type occurs at low sliding speed of 1m/s. As for heat resistance, it is made clear that remarkable heat resistance property can be obtained by addition of Ni element in Al matrix composites.

• 한국주조공학회지
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• 제19권6호
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• pp.493-500
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• 1999

Squeeze casting was used for fabricating a light metal base composite having high strength and wearresistance. Reactive sintering was used to prepare the preform of Squeeze casting. To utilize Fe-Al intermetallic compounds and SiC particle as a reinforcement, there needs to prepare Fe-Al mixed powder at 50, 60, 70at.%Al, and add SiC powder to the above mixture at 4, 7, 16, 24wt.%. The prepared mixture with SiC was reactive sintered in a tube furnace at $660^{\circ}C$ to get a porous hybrid preform of intermetallic compound and SiC. The preform prepared above was placed in a metal mold, preheated at $660^{\circ}C$ AC4C matrix was injected into the mold with the temperature of the melt at $610^{\circ}C$ After these processes, 66MPa was applied to the mold for 5 minute to finish the whole procedure. The maximum reaction temperature was increased with the increased Al amount, but decreased with the increased SiC amount. The density of the preform was decreased with SiC amount increase in the compacts due to swelling of the preform. An optical microscope was applied to observe the micro structure and the dispersion of the reinforcements. To analyze phases, We utilized XRD, EDS. Hardness test were chosen to get the information of mechanical properties. There were no significant changes in micro structure between the composite and preform. However, it was shown that uniform dispersion of the reinforcers and complete infiltration of the melt into the preform were achieved through the procedure of the squeeze casting. It was observed that the hardness of the composite is decreased with increased SiC amount, resulting from the volumetric expansion of the preform.

• 한국추진공학회지
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• 제4권1호
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• pp.65-73
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• 2000

금속기지 복합재료의 주조는 폭넓은 재료의 선택과 공정조건들을 제공하는 좋은 공정이다. 용탕교반기술은 압착주조 또는 분말야금과 비교하면 매우 간단하고 값이 싸기 때문에 주조방법중에서 산업응용에 가장 널리 쓰이는 좋은 방법이다. 최근에는 $\alpha$ -$Al_2O_{3(p)}$/Lo-Ex alloy 복합재료의 입자크기, 입자의 부피 분율, 기계적 성질에 있어서 Mg첨가 그리고 열팽창계수 등이 연구되어 왔다. $\alpha$ -$Al_2O_3$는 입자계면과 기지에 형성되어 기계적 성질에 중요한 역할을 하였다 대부분 복합재료의 인장강도는 증가하지 않지만 16$\mu\textrm{m}$ $\alpha$ -$Al_2O_3$ 입자를 5vol%로 첨가한 경우, 3wt.% Mg를 첨가한 복합재료의 인장강도는 증가한다. 강화재의 부피분율과 mg은 복합재료의 열팽창계수를 감소시켰다.

• 한국세라믹학회지
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• 제52권5호
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• pp.320-324
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• 2015

Optimization of the fabrication process of NiO-yttrium doped barium zirconate (BZY) composite anode substrates using tape-casting for high performance thin-film protonic ceramic fuel cells (PCFCs) is investigated. The anode substrate is composed of a tens of microns-thick anode functional layer laminated over a porous anode substrate. The macro-pore structure of the anode support is induced by micron-scale polymethyl methacrylate (PMMA) pore formers. Thermal gravity analysis (TGA) and a dilatometer are used to determine the polymeric additive burn-out and sintering temperatures. Crystallinity and microstructure of the tape-cast NiO-BZY anode are analyzed after the sintering.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2000년도 춘계학술발표대회 논문집
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• pp.31-37
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• 2000

Metal matrix composites(MMCs) are rapidly becoming one of the strongest candidates for structural materials for many high temperature application. Among the high temperature environment, thermal shock is known to cause significant degradation in most MMC system. Therefore, the nondestructive evaluation on thermal shock damage behavior of SiC/A16061 composite has been carried out using ultrasonic surface and SH-waves. For this study, Sic fiber reinforced metal matrix composite specimens fabricated by a squeeze casting technique were thermally cycled in the temperature range 25~$400^{\circ}C$ up to 1000 cycles. Three point bend test was conducted to investigate the effect of thermal shock damage on mechanical properties. The relationship between thermal shock damage behavior and the change of ultrasonic velocity and attenuation were discussed by considering SEM observation of fracture surface.

• Design & Manufacturing
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• 제6권1호
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• pp.95-100
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• 2012

In this study, a novel Cu composite sheet with embedded high electric conduction path was developed as another alternative for the interconnect materials possessing high electrical conductivity as well as high strength. The Cu composite sheet was fabricated by forming Ag conduction paths not within the interior but on the surface of a high strength Cu substrate by damascene electroplating process. As a result, the electrical conductivity increased by 40% thanks to mesh type Ag conduction paths, while the ultimate tensile strength decreased by 20%. The interfacial fracture resistance of Cu composite sheet prepared by damascene electroplating increased by above 50 times compared to Cu composite sheet by conventional electroplating. For feasibility test for practical application, a leadframe for LED module was manufactured by a progressive blanking and piercing processes, and the blanked surface profile was evaluated as a function of the volume fraction of Ag conduction paths. As Ag conduction path became finer, pressing formability improved.

• 한국세라믹학회지
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• 제36권10호
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• pp.1123-1131
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• 1999

Alumina-glass composites which are considered as the material of the choice for all dental crown was prepared by aqeous-based tape casting and sintering for 2h at 1120$^{\circ}C$ followed by glass infiltration for 2h at 1100$^{\circ}C$ Biaxial strength and fracture toughness of the composites were evaluated to determine the optimum composition of the tape as a function of the amount of constituent such as alumina binder and plasticizer. The strength and the fracture toughness of the alumina tape increased with increasing the contents of alumina and binder. These observations are consistent with in fluence of the constituents on mean alumuna particle distance in tapes suggesting that high strength of the glass infiltrated alumina composites is related to toughening by crack bowing. The biaxial strength and the fracture toughness of the composite containing the optimum constituent composition were 523 MPa and 3.3 MPa$.$1/2 respectively.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.327-328
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• 2006

We have demonstrated that textured $Al_2O_3-mullite-SiC$ nanocomposites can be fabricated by slip casting followed by partial oxidation - reaction sintering of mixed suspensions of $Al_2O_3$ and SiC powders in a high magnetic field. The sintered density was changed by the degree of oxidation at 1200C and 1300C. The degree of orientation of alumina in the nanocomposite was examined on the basis of the X-ray diffraction patterns and scanning electron micrographs. It is confirmed that alumina-oriented nanocomposites were fabricated. The three-point bending strength at room temperature was observed for the nanocomposites.