• Title/Summary/Keyword: Coating Time

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A Study on Monitoring of Mitigation of Rail Corrosion using Sacrificial Anode Cathodic Protection Method (희생양극법을 적용한 철도 레일의 방식효과 모니터링 연구)

  • Choi, Jung-Youl;Park, Jong-Yoon;Lee, Kyu-Yong;Chung, Jee-Seung
    • The Journal of the Convergence on Culture Technology
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    • v.5 no.4
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    • pp.367-371
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    • 2019
  • In this study, we proposed the sacrificial anode cathodic protection method as a countermeasure to reduce the corrosion of railway rails under oceanic climatic conditions and proved the anticorrosive effect experimentally. In addition, the proposed sacrificial anode cathodic protection method were tested on site to examine long-term rail corrosion monitoring and field applicability for more than 26 months and to prove the effectiveness of rail corrosion. As a result of monitoring the corrosion state using the cellophane tape method, the appearance of the applied sections with sacrificial anode cathodic protection method was good at the present time about 26 months after the field test laying, and no abnormalities and other abnormalities of the rail welded section and the rail web were found. Hence, in places where no sacrificial anodes were installed, rust progressed rapidly. In addition, the proper spacing of sacrificial anodes was found to form the most stable corrosion coating at 1.0 ~ 1.5m. After about 26 months of monitoring, the installation of sacrificial anodes could help stabilize the overall rail corrosion level, even if the spacing was somewhat wider.

HIGH HEAT FLUX TEST WITH HIP BONDED 35X35X3 BE/CU MOCKUPS FOR THE ITER BLANKET FIRST WALL

  • Lee, Dong-Won;Bae, Young-Dug;Kim, Suk-Kwon;Jung, Hyun-Kyu;Park, Jeong-Yong;Jeong, Yong-Hwan;Choi, Byung-Kwon;Kim, Byoung-Yoon
    • Nuclear Engineering and Technology
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    • v.42 no.6
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    • pp.662-669
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    • 2010
  • To develop the manufacturing methods for the blanket first wall (FW) of the International Thermonuclear Experimental Reactor (ITER) and to verify the integrity of the joint, Be/Cu mockups were fabricated and tested at the KoHLT-1 (Korea Heat Load Test facility), a graphite heater facility located at the Korea Atomic Energy Research Institute (KAERI). Since Be and Cu joining is the focus of the present study, the fabricated mockups had a CuCrZr heat sink joined with three Be tiles as an armor material, unlike the original ITER blanket FW, which has a stainless steel structure and coolant tubes. Hot isostatic pressing (HIP) was carried out at $580^{\circ}C$ and 100 MPa for 2 hours as the method for Be/Cu joining. Three interlayers, namely, $1{\mu}mCr/10{\mu}mCu$, $1{\mu}mTi/0.5{\mu}mCr/10{\mu}mCu$, and $5{\mu}mTi/10{\mu}mCu$ were applied as a coating to the Be tiles by a physical vapor deposition (PVD) method. A shear test was performed with the specimens, which were fabricated by the same methods as those used to fabricate the mockups. The average values were 125 MPa to 180 MPa, and the samples with the $1{\mu}mCr/10{\mu}mCu$ interlayer showed the lowest value. No defect or delamination was found in the joints of the mockups by the developed ultrasonic test using a flat-type probe with a 10 MHz frequency and a 0.25 inch diameter. High heat flux (HHF) tests were performed at $1.0\;MW/m^2$ heat flux for each mockup using the given conditions, and the results were analyzed by ANSYS-CFX code. For the test criteria, an expected fatigue lifetime about 1,000 cycles was obtained by analysis with ANSYS-mechanical code. Mockups using the interlayers of $1{\mu}mTi/0.5{\mu}mCr/10{\mu}mCu$ and $5{\mu}mTi/10{\mu}mCu$ survived up to 1,100 cycles over the required number of cycles. However, one of the Be tiles in the other two mockups using the $1{\mu}mCr/10{\mu}mCu$ interlayer was detached during the screening test, and others were detached by discharge after 862 cycles. The integrity of the joints using the proposed interlayers was proven by the HHF test, but the other interlayer requires more study before it can be used for the joining of Be to Cu. Moreover, it was confirmed that the measured temperatures agreed well with the analysis temperatures, which were used to estimate the lifetime and that the developed facility showed its capability of the long time operation.

Evaluation of Titanium-nitride Coated Crown: Surface Hardness, Corrosion Resistance and Color Sustainability (타이타늄-질소 코팅된 금속관에 대한 평가: 표면 경도, 부식 저항성, 색조 안정성)

  • Kim, Hyojin;Lim, Sumin;Kim, JinYoung
    • Journal of the korean academy of Pediatric Dentistry
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    • v.48 no.3
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    • pp.344-351
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    • 2021
  • The purpose of this study was to compare surface hardness between titanium-nitride coated crowns (TiNCs) and stainless steel crowns (SSCs), and to evaluate the corrosion resistance and color sustainability of TiNCs. Ten TiNCs and 10 SSCs were used for the hardness test. Measurement was performed 30 times for each type of crowns, and the mean values were compared. Metallic raw material plates (before being processed into crowns) of TiNCs and SSCs were prepared for the corrosion resistance test. The total amounts of metal ion releases in the test solution were detected by inductively coupled plasma-optical emission spectrometry. Five TiNCs were subjected to the color sustainability test by applying repetitive brushing forces. The mean hardness values of TiNC group and SSC group were 395.53 ± 105.90 Hv and 278.70 ± 31.45 Hv respectively. Hardness of TiNCs were significantly higher than that of SSCs. The total amounts of metal ion releases from the materials of TiNCs and SSCs satisfied the criterion in International Organization for Standardization 22674. The results mean that TiNCs and SSCs were not harmful in an acidic environment. The golden coating was stable against the repetitive physical stimulations for a given period time.

A Study on the Preparation and Purification Characteristics of Graphene Oxide by Graphite Type (흑연 종류에 따른 산화 그래핀의 제조 및 정제를 통한 특성연구)

  • Jeong, Kyeom;Kim, Young-Ho
    • Clean Technology
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    • v.27 no.2
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    • pp.132-138
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    • 2021
  • Research is being conducted on graphene to provide graphene having both excellent physical as well as electrical properties in addition to unique physical properties. In this study, Hummer's method, which is a representative method for chemical exfoliation, was applied in order to investigate the possibility of the mass production of high-quality graphene oxide. Three types of graphite (graphite, crystalline graphite, and expanded graphite) were used in the preparation of graphene oxide with variations in the amount of potassium permanganate added, reaction temperature, and reaction time. Then a Fourier transform infrared spectroscopy (FT-IR), a Raman spectrometer, and a transmission electron microscope (TEM) were used to measure the quality of the prepared graphene oxide. Of the three types of graphite used in this experiment, crystalline graphite showed the highest quality. The prepared graphene oxide was then purified with an organic solvent, and an analysis conducted using energy dispersive X-ray spectroscopy (EDS). From the results of the residual values, we were able to confirm that both acid wastewater and wastewater were best purified using cyclohexane. The method for manufacturing graphene oxide as well as the method of purification using organic solvents that are presented in this study are expected to have less of an environmental impact, making them environmentally friendly. This makes them suitable for use in various industrial fields such as the film industry and for heat dissipation and as coating agents.

Basic Performance Evaluation of a Tack Coat Material for Use with a Spray Paver (동시포설 공법을 위한 택코트 재료의 기초 성능 평가 연구)

  • Jo, Shinheang;Kim, Kyungnam;Cui, Wenhui;Kim, Nakseok
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.41 no.6
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    • pp.737-744
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    • 2021
  • Spray paving minimizes material lost during the construction or repair of a road surface, and it can be done in conjunction with tack coating. This approach involves applying the asphalt mixture at the same time as spraying the tack coat by attaching a spraying device to the asphalt paver. When applying an asphalt overlay to an aged concrete surface, it is important to ensure the adhesion performance between different material properties. Accordingly, there is a need for a tack coat that can be applied by spray paving and that exhibits good adhesive performance on different materials. In this study, bonding strength tests under various conditions were performed to evaluate the basic performance of a tack coat developed for use with a spray paver. The bonding performance of the tack coat was observed to be affected by curing conditions and material lost during construction. The test results also showed that the tensile and shear bonding strengths of the developed tack coat were 1.21 and 1.99 times higher than those of a conventional one, respectively. As a result, the developed tack coat is considered suitable for application to spray paving.

A Study on the Effect of Fire Heat on the Durability of Concrete Structures Repaired and Reinforced with Epoxy Resin (화열(火熱)이 에폭시수지로 보수·보강된 콘크리트 구조체의 내구성에 미치는 영향에 관한 연구)

  • Tai Kwan Cho
    • Journal of the Society of Disaster Information
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    • v.19 no.1
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    • pp.138-145
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    • 2023
  • Purpose: In accordance with the increase in the number of buildings repaired and reinforced following deterioration from when a fire occurs in a previously reinforced building, the impact on the structure after the fire is analyzed to establish standards for repair and reinforcement measures. Method: After curing for 28 days, the process was to measure the compressive strength and induce destruction through a compressor, repair and reinforce it with epoxy, and conduct a re-compressive strength test on some specimens after curing for 3 days to understand the degree of strength restoration. The rest of the repaired and reinforced specimens as well as the unrepaired and unreinforced specimens were then put into an oven and heated according to the temporal and temperate conditions listed below, and then the compressive strength was tested to estimate the impact of fire. Result: After reinforcing the yielded specimen with epoxy, the process was to then put it in an oven and heat it at different temperatures over time. It was found that there was a decrease in the strength of the reinforcement more than that of the actual specimen. Conclusion: Based on this, it was found that a building repaired and reinforced with epoxy resin is actually more dangerous than a general unrepaired building when it is damaged by fire, and thus, that it must be prepared for fire vulnerabilities.

Electrical Conductivity, Optical Transmittance, and Oxidation Stability of Transparent Conductive Polymer Film Coated With Layered Pristine Single-walled Carbon Nanotube and Silver Nanowire (무정제 단일벽 탄소나노튜브와 은나노와이어가 적층으로 코팅된 투명전도성 고분자 필름의 전기 전도성, 광학 투과도 및 산화안정성)

  • Young Sil Lee
    • Korean Chemical Engineering Research
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    • v.61 no.3
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    • pp.456-462
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    • 2023
  • An electrically conductive and transparent electrode was created by applying a dispersion of pristine single-walled carbon nanotubes (SWCNTs) and silver nanowires to a polyethylene terephthalate (PET) film using a bar coating method. The SWCNTs were added to increase the electrical conductivity and transmittance of the silver nanowires while also preventing the haze from increasing due to the stacking of multiple layers containing SWCNTs and silver nanowires on the PET substrate. The silver nanowires in the electrode were also found to be stable against oxidation. The transparent electrode displayed excellent electrical and optical properties, with a sheet resistance of 47 Ω/□, transmittance of 96.72%, and haze of 1.93%. Additionally, the sheet resistance of the electrode remained stable over time, with a change of only 6.4% after a constant temperature and humidity test, making it suitable for long-term use. A hybrid transparent electrode that is economically feasible and environmentally sustainable has been developed through the utilization of pristine SWCNT and silver nanowire.

Development of Bi0.5(Na0.78K0.22)0.5TiO3 Lead-free Piezoelectric Ceramic Material with Core-shell Structure for Biomedical (바이오 메디컬용 코어-쉘 구조의 Bi0.5(Na0.78K0.22)0.5TiO3계 무연압전세라믹 소재의 개발)

  • Seong-jun Yun;Joonsoo Bae
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.46 no.3
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    • pp.15-22
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    • 2023
  • BNKT Ceramics, one of the representative Pb free based piezoelectric ceramics, constitutes a perovskite(ABO3) structure. At this time, the perovskite structure (ABO3) is in the form where the corners of the octahedrons are connected, and in the unit cell, two ions, A and B, are cations, A ion is located at the body center, B ion is located at each corner, and an anion O is located at the center of each side. Since Bi, Na, and K sources constituting the A site are highly volatile at a sintering temperature of 1100℃ or higher, it is difficult to maintain uniformity of the composition. In order to solve this problem, there should be suppression of volatilization of the A site material or additional compensation of the volatilized. In this study, the basic composition of BNKT Ceramics was set to Bi0.5(Na0.78K0.22)0.5TiO3 (= BNKT), and volatile site (Bi, Na, and K sources) were coated in the form of a shell to compensate additionally for the A site ions. In addition, the physical and electrical properties of BNKT and its coated with shell additives(= @BNK) were compared and analyzed, respectively. As a result of analyzing the crystal structure through XRD, both BNKT(Core) and @BNK(Shell) had perovskite phases, and the crystallinity was almost similar. Although the Curie temperature of the two sintered bodies was almost the same (TC = 290 ~ 300 ℃), it was confirmed that the d33 (piezoelectric coefficient) and Pr (residual polarization) values were different. The experimental results indicated that the additional compensation for a shell additive causes the coarsening, resulting in a decrease in sintering density and Pr(remanent polarization). However, coating shell additives to compensate for A site ion is an effective way to suppress volatilization. Based on these experimental results, it would be the biggest advantage to develop an eco-friendly material (Lead-free) that replaced lead (Pb), which is harmful to the human body. This lead-free piezoelectric material can be applied to a biomedical device or products(ex. earphones (hearing aids), heart rate monitors, ultrasonic vibrators, etc.) and skin beauty improvement products (mask packs for whitening and wrinkle improvement).

Structural and Electrical Properties of (La0.7Sr0.3)(Mn1-xFex)O3 Thin Films Prepared by Sol-Gel Method for Thermistor Devices (서미스터 소자로의 응용을 위한 솔-젤법으로 제작한 (La0.7Sr0.3)(Mn1-xFex)O3 박막의 구조적, 전기적 특성)

  • Ji-Su Yuk;Sam-Haeng Yi;Myung-Gyu Lee; Joo-Seok Park;Young-Gon Kim;Sung-Gap Lee
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.37 no.2
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    • pp.164-168
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    • 2024
  • (La0.7Sr0.3)(Mn1-xFex)O3 (LSMFO) (x = 0.03, 0.06, 0.09, 0.12) precursor solution are prepared by sol-gel method. LSMFO thin films are fabricated by the spin-coating method on Pt/Ti/SiO2/Si substrate, and the sintering temperature and time are 800℃ and 1 hr, respectively. The average thickness of the 6-times coated LSMFO films is about 181 to 190 nm and average grain size is about 18 to 20 nm. As the amount of Fe added in the LSMFO thin film increased, the resistivity decreased, and the TCR and B25/65-value increased. Electrical resistivity, TCR and B25/65-value of the (La0.7Sr0.3)(Mn0.88Fe0.12)O3 thin film are 0.0136 mΩ-cm, 0.358%/℃, and 328 K at room temperature, respectively. The resistivity properties of LSMFO thin films matched well with Mott's VRH model.

Improving Curing Rate and Physical Properties of Korean Dendropanax Lacquer with Thermal and Photo Initiator by Dual Curing (이중경화법을 이용한 열개시제 및 광개시제가 배합된 황칠도료의 경화속도 촉진 및 물성향상 연구)

  • Hwang, Hyeon-Deuk;Moon, Je-Ik;Park, Cho-Hee;Kim, Hyun-Joong;Hwang, Baik
    • Journal of the Korean Wood Science and Technology
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    • v.38 no.4
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    • pp.333-340
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    • 2010
  • The Korean Dendropanax lacquer, made from a natural resinous sap from Dendropanax orbifera Lev., was used as a golden and transparent varnish for the traditional artifacts (armor uits, helmets, arrowheads, etc.) to make them be brilliant golden color. The cured film of the acquer has excellent protective properties such as weatherability, water resistance, and nticorrosive. But, one of disadvantages is that takes a long time and much energy to fulfill curing the lacquer. The chemical constituents of the lacquer contained conjugated diene compounds s the photopolymerizable monomers. These monomers easily polymerized in sunlight to form olden-colored, hard-coating films in a short time. Photooxidation may be one of the most mportant reactions in the chemistry of the lacquer. Although the Korean Dendropanax Lacquer hould be dried to a thoroughly dry stage to achieve optimal film properties, curing with elevated emperatures may be required for the protracted curing time at atmospheric temperature. So we ntended to accelerate the curing rate of the lacquer by dual curing of thermal and radiation uring. The effect of thermal initiator on the thermal curing reaction was evaluated by monitoring he changes in double bond peak with FT-IR. Then the curing rate of the lacquer blended with hermal initiator and photoinitiator together was measured during dual curing using a RPT with V spot curing machine. Thermal initiator not only accelerated the curing rate but also improved he physical property. And the curing rate of the Korean Dendropanax lacquer was improved by ual curing method of thermal and UV curing. According to these results, the application area of he Korean Dendropanax lacquer could be expanded to surface coatings for electronic devices uch as mobile phones or electronics.