• Journal of the Korean institute of surface engineering
• /
• v.26 no.6
• /
• pp.316-326
• /
• 1993

Adhesion and hardeness are the most important properties of a hard coated layer which is applied to wear-resistant devices. Zr/ZrN layer was deposited on tool steel(SKH9) and stainless steel(SUS304) by a re-active D.C. magnetron sputtering technique and their microhardness and adhesion strength were measured for the films processed by changing the partial pressures of $N_2$ gas (4~10$\times$$10^{-4}$mbar) and the substrate bias voltage(0~250V). The adhesion strength was evaluated by acoustic signals through the scratch-test with the incremental applied load. As the partial pressure of $N_2$ gas and the substrate bias voltage were increased, the adhesion strength of tool steel was observed to be stronger than that of the stainless steel. The adhesion strength was generally, observed to decrease with the same tendency regardless of the kinds of substrates. The adhesion strength of tool steel was increased more and more strongly than that of stainless steel as heat-treated temperature was increased. The strength of tool steel was appeared to be high adhesion strength at $400^{\circ}C$. From the failure mode of the film during the scratch adhesion test, the cohesive failure was observed to be obvious and the adhesive failure in a minor portion in the Zr/ZrN doublelayer regardless of the kinds of substrates.

• Structural Engineering and Mechanics
• /
• v.73 no.5
• /
• pp.501-513
• /
• 2020

In the present work, the optimization of machining parameters to achieve the desired technological parameters such as surface roughness, tool radial vibration and material removal rate have been carried out using response surface methodology (RSM). The hard turning of EN19 alloy steel with coated carbide (GC3015) cutting tools was studied. The main problem faced in manufacturer of hard and high precision components is the selection of optimum combination of cutting parameters for achieving required quality of surface finish with maximum production rate. This problem can be solved by development of mathematical model and execution of experiments by RSM. A face centred central composite design (FCCD), which comes under the RSM approach, with cutting parameters (cutting speed, feed rate and depth of cut) was used for statistical analysis. A second-order regression model were developed to correlate the cutting parameters with surface roughness, tool vibration and material removal rate. Consequently, numerical and graphical optimization were performed to obtain the most appropriate cutting parameters to produce the lowest surface roughness with minimal tool vibration and maximum material removal rate using desirability function approach. Finally, confirmation experiments were performed to verify the pertinence of the developed mathematical models.

• Journal of the Korean Ceramic Society
• /
• v.49 no.5
• /
• pp.417-422
• /
• 2012

Copper nano particles have been considered as the materials for conductive ink due to its good thermal, electrical conductivity and low cost. However, copper nanoparticles oxidize easily, decreasing dispersion stability and electrical conductivity. Therefore, it is important to develop a method to minimize oxidation of copper nano particles to improve its dispersion stability property in copper nano ink. In this study, copper nano particles were coated with 1-Octanethiol VSAM(Vaporized Self Assembled Multilayers) to prevent oxidation and coated copper powders were dispersed in conductive ink successfully by studying its relationship of different chain length of solvents to 1-Octanethiol coating layer to fabricate nano ink. Various alcohol solvents, such as 1-Hexanol, 1-Octanol, and 1-Decanol were used. The coating layer was observed using FESEM and TEM. Furthermore, dispersion of copper nano particles in nano inks, was characterized using Turbiscan analyzer, viscometer, and contact angle measurement tool.

• International Journal of Advanced Culture Technology
• /
• v.3 no.1
• /
• pp.161-168
• /
• 2015

This article aims to apply a friction stir spot welding for producing a lap joint of AA1100 aluminum alloy and SGACD zinc coated steel. The experiment was designed by MINITAB and then investigated the relation among the friction spot joint parameters. The experimental results are as follows. The friction spot joining could successively produce the lap joint of AA1100 aluminum alloy and SGACD zinc coated steel. Interaction between the rotate speed, the hold time and the tool insert speed affected to vary the tensile shear strength of the lap joint. The prediction of the optimized welding parameters that indicated the tensile shear strength of 1966 N was the rotated speed of 4000 rpm, the pin hold time of 6 sec, the pin insert rate of 6 mm/min with the S/N ratio of 66.56 that was higher than that of the total mean S/N ratio. The practical experiment of the predicted welding parameters indicated the tensile shear strength of 2165 N and had the S/N ratio of 66.70 that was higher than the predicted tensile shear strength.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
• /
• 2002.10b
• /
• pp.141-142
• /
• 2002

In this paper, we propose a slurry jet (water containing $1\;{\mu}m$ alumina particles) impact test in order to quickly evaluate the wear properties of physical vapor deposited (PVD) coatings on commercial cutting tools. Linear wear was obtained for bothe coating and substrate material, and the penetration through the coating into the substrate was signified by a sharp increase in slope of the wear versus time curve. The PVD coatings deposited on the tools showed the same wear rates as those on reference plate specimens produced by the same coating methods. We conclude that our proposed evaluation technique for coatings is considerably useful as a screening test when evaluating coated tools like twist drills, taps, end mills, gear hobs, etc.

• Transactions of the Korean Society of Machine Tool Engineers
• /
• v.15 no.1
• /
• pp.49-55
• /
• 2006

The effect of coating temperature with regard to surface properties of TiN-coated layer on hard metal(WC-Co) are experimentally investigated. Hardness, surface roughness, TiN coating thickness and adsorption force were measured in order to evaluate the effect of coating temperature. The two-way ANOVA method is used in order to evaluate the experimental data. In AIP processing, It is concluded that the furnace temperature in the range of $400^{\circ}C\~500^{\circ}C$ affected to a little increasing the number of production with the coating temperature.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
• /
• 1997.10a
• /
• pp.310-315
• /
• 1997

An extensive corrosion study was initiated by galvalume steel sheet manufacturing company to clarify the corrosion behavior of zinc and zinc and zinc-alloy coated automotive sheet steel in out panel and electrical application. Since the early 1980's the use of zinc and aluminum alloy coated steel for vehicular corrosion protection has increased drastically. This paper describes the evaluation of formability, weldability and painted corrosion performance of galvalume steel sheet. This paper presents an overview of the program and some initial test results on the weldability, lifetime of the electrode tip shape of the spot welding and corrosion protection. Galvalume steel sheet improved corrosion performance and spot weldability of galvalume steel has no problem for the variation of welding current. And tip lifetime was changed according to the influence of shape.

• Transactions of the Korean Society of Machine Tool Engineers
• /
• v.11 no.4
• /
• pp.1-5
• /
• 2002

A 110 m diameter aspheric metal secondary mirror for a test model of an earth observation satellite camera was fsbricated by ultra-precision single point diamond turning (SPDT). Aluminum alloy for mirror substrates is known to be easily machinable, but not polishable due to its ductility. A harder material, Ni, is usually electrolessly coated on an A1 substrate to increase the surface hardness for optical polishing. Aspheric metal secondary mirror without a conventional polishing process, the surface roughness of Ra=10nm, and the form error of Ra=λ/12(λ=632.8nm) has been required. The purpose of this research is to find the optimum machining conditions for reflector cutting of electroless-Ni coated A1 alloy and apply the SPDT technique to the manufacturing of ultra precision optical components of metal aspheric reflector.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 1995.10a
• /
• pp.139-142
• /
• 1995

Inconel 718 is one of the most difficut workpiece for machining, So it is necessary to evaluate the machining characteristics of Inconel 718 In this study, High speed machining of this material was carried out with Tin coated WC ball endmill and TiN coated HSS ball endmill. The cutting force and shape of machined surface and cip type were investigated according to variation of cutting speed,feed rate and depth of cut

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
• /
• 1988.06a
• /
• pp.43-48
• /
• 1988

보호피막을 입히는 방법으로는 화학증착법과 물리증착법이 주로 사용되고 있다. 고온 분위기에서 기체 상태인 반응물의 화학반응을 통하여 원하는 물질을 증착시키는 화학증착법은 물리증착법에 비해 점착성(adhesion)이 우수하고, 보호피막층의 성분조절이 용이하며, 반응물이 기체상태이므로 대량생산이 용이하여 보호피막 증착법으로 많이 사용되고 있다. $Si_3N_4$-TiC ceramic 표면에 TiC, TiN 및 Ti(C, N) coating을 함으로써 얻을 수 잇는 장점들은 표면층의 경도를 증가시키며, steel과의 마찰계수의 감소 및 coating 층 자체가 고온에서 고체 윤활제로 작용하여 마찰열의 상당한 감소를 얻을 수 있으며, 또한 coating층 자체가 비교적 안정한 화합물로 피삭재내의 성분원소들에 대한 diffusion barrier로 작용되며, 내식성을 증가시킬 수 있다. 본 연구에서는 각 증착층의 미소경도, 열충격저항, steel과의 마찰계수를 측정하였으며, 최종적으로 절삭시험을 통하여 증착층들의 내마모성을 조사, 규명하였다.