• Title/Summary/Keyword: Chemical compositions

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Quality Evaluation to Determine the Grading of Commercial Salt-Fermented Fish Sauce in Korea (국내산 시판 액젓의 등급판정을 위한 품질 평가)

  • Cho, Young-Je;Lee, Hong-Hee;Kim, Bo-Kyoung;Gye, Hyeon-Jin;Jung, Woo-Young;Shim, Kil-Bo
    • Journal of Fisheries and Marine Sciences Education
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    • v.26 no.4
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    • pp.823-830
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    • 2014
  • This study conducted to investigate the quality of commercial fish sauce and determine the grade of them by measuring the chemical compositions and biogenic amines. The commercial salt-fermented anchovy sauce contained 65.84-70.94% (mean : 68.39%) of moisture, 22.19-25.43% (24.22%) of salinity, 5.4-6.1 (5.8) of pH, 0.76-1.61%(1.18%) of total nitrogen, 478.52-924.66 mg/100 g (702.05 mg/100 g) of amino nitrogen and 584.59-1593.52 mg/kg of histamine. Whereas commercial salted-fermented sand lance sauces contained 66.63-71.99% (68.73%) of moisture, 23.9-25.5% (24.57%) of salinity, 5.5-6.4(6.16) of pH, 0.64-1.46% (1.07%) of total nitrogen, 433.51-1006.67 mg/100 g (665.36 mg/100 g) of amino nitrogen and 194.01-1839.68 mg/kg of histamine. Correlation of TN, AN and VBN containing nitrogen was high, but there was no significant correlation between these results and histamine. In total nitrogen content, 6 of the 20 fish sauces were less than Korea Food Standard. The eight samples were less than the amino nitrogen regulation of Korean Industrial Standard (KS). And 14 fish sauce were exceeded by 68% for moisture content standard of Korean Industrial Standard.

Petrology of the Cretaceous volcanic rocks in Pusan ares, Korea (부산일원에 분포하는 백악기 화산암류의 암석학적 연구(I))

  • 김진섭;윤성효
    • The Journal of the Petrological Society of Korea
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    • v.2 no.2
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    • pp.156-166
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    • 1993
  • The volcanic stratigraphy and geochemistry of the Cretaceous volcanic rocks in the southern part of the Pusan showed that the volcanic rocks of the study area consist of alternating pyroclastic rocks and andesitic lavas, apparently constituting a thick volcanic sequence of a stratovolcano. The andesitic rocks contain augite, plagioclase, and hornblende as phenocrysts. Matrix minerals are augite, magnetite, hornblende, apatite. Mafic minerals, such as chlorite, epidote, sericite, and iron oxides occur as alteration products. Dacitic volcanic breccia and rhyolitic welded ash-flow tuff locally overlie the andesitic rocks. The rocks reported in the previous studies as andesitic breccia and andesite plot in the field of basalt, basaltic andesite, andesite, dacite and rhyolite, based on their chemical compositions. The volcanic rocks of the study area belong to the calc-alkaline series, and the andesitic rocks which are predominant in the area plot to the field of orogenic andesite.

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Effects of Storage Gas Concentrations on the Qualities of Garlic(Allium sativum L.) Bulb during CA Storage (통마늘의 CA저장 중 저장기체 농도에 따른 품질변화)

  • 강준수;홍경훈
    • Food Science and Preservation
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    • v.8 no.3
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    • pp.258-263
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    • 2001
  • This experiment was conducted to measure the physiological qualities and the chemical compositions of garlic bulb (Allium sativum L) stored in air and controlled atmosphere at 0$\^{C}$ for 4months. There were no significant differences in physiological qualities such as soluble solid, dry weight and firmness by O$_2$ and CO$_2$ concentrations during 4 months of storage. The surface color of garlic cloves changed toward more dark direction in Hunter color surface with storage. CA storage inhibited the sprout growth by 50% and had no significant difference in root growth. Garlic stored in CA showed lower level of pungency, especially CA of low oxygen concentration (1%) showed the lowest level of pyruvate. Garlic stored in high CO$_2$ concentration(20%) showed the lowest level of fructan concentrations and the highest free sugar concentrations.

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Variation of Mechanical Properties according to Microstructure of High Strength Steel Weld Metal (고강도강 용접금속의 미세조직에 따른 기계적 특성 변화 연구)

  • Lee, Jae-Hee;Kim, Sang-Hoon;Yoon, Byung-Hyun;Jung, Hong-Chul;Lee, Chang-Hee
    • Proceedings of the KWS Conference
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    • 2010.05a
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    • pp.70-70
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    • 2010
  • In the present study, to estimate the mechanical properties of 800 MPa grade weld metal, welding was carried out using 800 and 600 MPa grade flux cored arc welding (FCAW) consumable and characteristics of the weld metals were investigated. The chemical composition of weld metals was investigated by an optical emission spectroscopy (OES) method. The microstructure of weld metals was analyzed by optical microscopy (OM) and secondary electron microscopy (SEM). The compositions and sizes of inclusions which are the dominant factors for the nuclei of acicular ferrite were analyzed by an transmission electron microscopy (TEM). In addition, mechanical properties of the weld metals were evaluated through tensile tests and charpy impact tests. Mostly the acicular ferrite phase which has high strength and toughness was observed. The 600 MPa grade weld metal was consisted of 75% acicular ferrite and 25% ferrite which was formed at high temperature (grain boundary ferrite, widmanstatten ferrite, polygonal ferrite). However, the 800 MPa grade weld metal was composed of about 73% acicular ferrite and 27% low temperature phase (bainite, martensite). Toughness was considerably decreased due to the increase of tensile strength (from 600 MPa to 800 MPa). The sizes of inclusions which were observed in both weld metal were $0.4{\sim}0.8\;{\mu}m$, it is effective size to form acicular ferrite.

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Investigation and Assessment of the Deterioration on Aging Large Water Mains (대형 상수관로 노후상태 조사 및 평가에 관한 연구)

  • Kim, Ju-Hwan;Bae, Chul-Ho;Kim, Jung-Hyun;Hong, Sung-Ho;Lee, Kyung-Jae
    • Journal of Korean Society of Water and Wastewater
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    • v.20 no.4
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    • pp.545-558
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    • 2006
  • The current conditions of large water mains are evaluated by deteriorations and the causes of deterioration are investigated through visual assessments in the field, mechanical tests and analysis of chemical compositions in laboratory for each pipe material, unlined cast iron pipes (CIPs), ductile iron pipes (DCIPs) and steel pipes (SPs) Tubercles and scales from internal and external corrosion of unlined cast iron pipes were identified as the causes of functional performance limitations in large water mains. It is investigated that main causes of internal and external corrosion of water pipes are from lots of depositions of organic and inorganic substances on pipe surface, concentrated pitting, and uniform corrosion by local or global exfoliation or detachment of lining and coatings of DCIPs and SPs. Internal and external corrosion depths of CIPs were higher than those of DCIPs and SPs. Consequently, total corrosion rate summed internal and external corrosion rates of CIPs also were shown to be higher than those of DCIPs and SPs. The failure time from hole generation of CIPs by total corrosion rate was predicted to be taken sixteen years, and DCIPs and SPs were twenty-six years and one hundred and fifty three years. And longitudinal deflection of investigated water mains were not happened and mechanical strengths such as tensile strength, elongation, and hardness also were mostly suited to Korea Standards. It was thought that the weakness of tensile strength of one sample(S-11) was, however, due to higher carbon contents(%) in CIPs. Pipe deterioration score of S-46 was 55.2 and was preferentially assessed to be rehabilitated.

Distribution of Hemicelluloses in Warts and the Warty Layer in Normal and Compression Wood Tracheids of Cryptomeria Japonica

  • Kim, Jong-Sik;Awano, Tatsuya;Yoshinaga, Arata;Takabe, Keiji
    • Journal of the Korean Wood Science and Technology
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    • v.39 no.5
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    • pp.420-428
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    • 2011
  • The distribution of arabino-4-O-methylglucuronoxylans (AGXs) and O-acetyl-galactoglucomannans (GGMs) in warts and the warty layer of tracheids in normal wood (NW) and compression wood (CW) of Cryptomeria japonica was investigated. Under field emission scanning electron microscope (FE-SEM) observation, warts and the warty layer of delignified NW and CW tracheids were degraded by xylanase treatment, indicating that warts and the warty layer contain high amounts of AGXs. However, the effect of xylanase was not observed in NW and CW tracheids before delignification, suggesting that AGXs in warts and the warty layer may be encrusted with lignin. After ${\beta}$-mannanase treatment, no noticeable changes were observed in warts and the warty layer of NW tracheids, indicating that warts and the warty layer contain either no or very few GGMs. Similar results to FE-SEM observations were also observed with immunogold labeling. AGX labeling was observed in warts and the warty layer of NW and CW tracheids, while GGM labeling was not detected. NW tracheids showed a much stronger density of AGX labeling than did CW tracheids in warts and the warty layer, indicating differences in the chemical compositions of warts and the warty layer between NW and CW tracheids.

The Influence of Spices on the Volatile Compounds of Cooked Beef Patty

  • Jung, Samooel;Jo, Cheorun;Kim, Il Suk;Nam, Ki Chang;Ahn, Dong Uk;Lee, Kyung Heang
    • Food Science of Animal Resources
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    • v.34 no.2
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    • pp.166-171
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    • 2014
  • The aim of this study is to examine the influences of spices on the amounts and compositions of volatile compounds released from cooked beef patty. Beef patty with 0.5% of spice (nutmeg, onion, garlic, or ginger powder, w/w) was cooked by electronic pan until they reached an internal temperature of $75^{\circ}C$. A total of 46 volatile compounds (6 alcohols, 6 aldehydes, 5 hydrocarbons, 6 ketones, 9 sulfur compounds, and 14 terpenes) from cooked beef patties were detected by using purge-and-trap GC/MS. The addition of nutmeg, onion, or ginger powder significantly reduced the production of the volatile compounds via lipid oxidation in cooked beef patty when compared to those from the control. Also, the addition of nutmeg and garlic powder to beef patty generated a lot of trepans or sulfur volatile compounds, respectively. From these results, the major proportion by chemical classes such as alcohols, aldehydes, hydrocarbons, ketones, sulfur compounds, and terpenes was different depending on the spice variations. The results indicate that addition of spices to the beef patty meaningfully changes the volatile compounds released from within. Therefore, it can be concluded that spices can interact with meat aroma significantly, and thus, the character of each spice should be considered before adding to the beef patty.

Litholohical and Mechanical Characteristics of Crushed Limestone Aggregates (쇄석 골재용 석회암의 암석학적 및 역학적 특성)

  • 진호일;민경원;백환조;연규석
    • Magazine of the Korea Concrete Institute
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    • v.9 no.3
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    • pp.119-126
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    • 1997
  • Recently, duc to highly increased consumption of' ngg~.egatc>s f o ~ . construction. studies have focused on the effective utilization of rock wastes abandoned so far. This study was designed, firstly, to determine t,hc petrological, g'ochemical and mechanical cha~,acte~istics of' crushed limestone aggregates in thc Samhwa district for suitable construction aggregates and, secondly, to offer basic data for cff'ective utilization of low grade limestones. Results of' the petrographic st,udy indicates that the crushed limestone aggregates in the Samhwa district can bo separate4 into two groups, namely f'inc-grained and cowlxcgrained limestones. Dominantly distributed fine-grained limestone containing some dolomite has higher Mgo and $SiO_2$ contents compared to the coarse-graincd limestonr. It, can be classified as medium strength rock by the physical and mcxhanical pi.opertics. I3ased on the size of' mineral grains and chemical compositions, it is suggested that the crushed limestone aggregates in t,his study area would bctkr be u s ~ i for asphalt concr.ctt., road pavement, or railroad ballast materials than for cement concrete.

Characterizations and Quantitative Estimation of Alkali-Activated Binder Paste from Microstructures

  • Kar, Arkamitra;Ray, Indrajit;Halabe, Udaya B.;Unnikrishnan, Avinash;Dawson-Andoh, Ben
    • International Journal of Concrete Structures and Materials
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    • v.8 no.3
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    • pp.213-228
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    • 2014
  • Alkali-activated binder (AAB) is recently being considered as a sustainable alternative to portland cement (PC) due to its low carbon dioxide emission and diversion of industrial wastes and by-products such as fly ash and slag from landfills. In order to comprehend the behavior of AAB, detailed knowledge on relations between microstructure and mechanical properties are important. To address the issue, a new approach to characterize hardened pastes of AAB containing fly ash as well as those containing fly ash and slag was adopted using scanning electron microscopy (SEM) and energy dispersive X-ray spectra microanalyses. The volume stoichiometries of the alkali activation reactions were used to estimate the quantities of the sodium aluminosilicate (N-A-S-H) and calcium silicate hydrate (CSH) produced by these reactions. The 3D plots of Si/Al, Na/Al and Ca/Si atom ratios given by the microanalyses were compared with the estimated quantities of CSH(S) to successfully determine the unique chemical compositions of the N-A-S-H and CSH(S) for ten different AAB at three different curing temperatures using a constrained nonlinear least squares optimization formulation by general algebraic modeling system. The results show that the theoretical and experimental quantities of N-A-S-H and CSH(S) were in close agreement with each other. The $R^2$ values were 0.99 for both alkali-activated fly ash and alkali-activated slag binders.

Studies on the Manufacturing of Carbon Bond Graphite Crucible (카아본 본드형 흑연 도가니 제조에 관한 연구)

  • 김충일;김문수
    • Journal of the Korean Ceramic Society
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    • v.13 no.1
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    • pp.11-19
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    • 1976
  • This study was focused on the improvement of production techniques of small crucibles in relation with the appropriate selection of raw materials, various batch compositions and physical and chemical characteristics of the crucibles. Various tests gave the optimum batch composition for the carbon bond graphite cructble as follows: Pyontaek graphite flake (refractory aggregate) : 40Part Silicon carbide: 15Part Tar pitch (binder) : 11Part Inorganic additives (to improve the oxidation resistance) : 15 Part Cryolite : 3 Part Ferro manganese : 2 Part Ferrosilicon : 25 Part Crucibles pressed with 400kg/$\textrm{cm}^2$ at 12$0^{\circ}C$. and fired in reducing atmosphere at 120$0^{\circ}C$ brought the most favorable results as follows: Bulk density : 2.31 Apparent density : 2.58 Porosity : 15.2% Oxidation loss at 1, 50$0^{\circ}C$. for 3 hrs : below 3.77% Water absorption : 6.01% Compressive strength : 438kg/$\textrm{cm}^2$ Tensile strength : 256kg/$\textrm{cm}^2$.

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