• 제목/요약/키워드: Chemical Composition test

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Preparation and Characteristics of Ice Cream from Mix Added with Nutmeats (견과육 첨가 아이스크림의 제조 및 특성)

  • Kim, Jong Woo
    • Korean Journal of Agricultural Science
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    • v.25 no.2
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    • pp.176-180
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    • 1998
  • Ice cream were made with chestnut meat and walnut meat which are special agricultural products in Chungnam area. The nut meat powders were added in the concentration of 1~5% in the ice cream mix. The over run characteristic, chemical composition and sensory test were examined. The results obtained were as follows. 1. The score of over run was lower for chestnut ice cream(35.75~38.81%) and walnut ice cream (36.31~40.38%) than for control ice cream (41.28%). 2. The concentration of solid-non-fat and crude protein were higher for chestnut ice cream 31.05~31.73% and 4.48~4.78% than for control ice cream. The walnut ice cream contained more fat and protein (12.21~16.29% and 4.63~5.27%) than for control ice cream did. 3. The scores of tastes and odor were higher for chestnut ice cream than for control ice cream, and the scores of odor were higher significantly (P<0.05%) for walnut ice cream.

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The Laccase Activity of Trametes versicolor during Cultivation on Acetylated Wood and 13C-CP/MAS NMR Study (아세틸화 처리 목재에 배양시킨 Trametes versicolor의 Laccase활성과 13C-CP/MAS NMR 분석)

  • Son, Dong-Won;Lee, Dong-Heub
    • Journal of the Korean Wood Science and Technology
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    • v.29 no.4
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    • pp.60-66
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    • 2001
  • For examine anti-degradation factors of acetylated wood, acetylated wood was incubated on Trametes versicolor. The laccase activity was examined in broth culture and solid fermentation that contain acetylated chips. The change of acetyl groups and chemical composition in the acetylated wood having massloss analysed by $^{13}C$-CP/MAS NMR. The laccase activity was detected in broth culture. When the T. versicolor contact to acetylated wood directly, the laccase activity was very low and couldn't maintain during test periods. Through the analysing of $^{13}C$-CP/MAS NMR, the acetylation took place carbohydrates as well as lignin and hydroxyl group of amorphous region was more easily substituted that of crystalline region The spectral analyses of $^{13}C$-CP/MAS NMR were shown that introduced acetyl bond was stable against fungal attack.

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Influence of Essential Oil in 'Shiranuhi' Immature Fruit on Antioxidant and Antimicrobial Activities (부지화 미숙과 에센셜 오일의 항산화 및 항균 활성 효과)

  • Kim, Sang Suk;Hyun, Ju Mi;Kim, Kwang Sik;Park, Kyung Jin;Park, Suk Man;Choi, Young Hun
    • Korean Journal of Medicinal Crop Science
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    • v.21 no.6
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    • pp.493-497
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    • 2013
  • This study was designed to analyze the chemical composition of essential oil in 'Shiranuhi' immature fruit and to test their biological activities. 'Shiranuhi' immature essential oils (SIEO) were obtained by steam distillation from fruits collected from Jeju Island and were analyzed using gas chromatograph (GC)-flame ionization detectors (FID) and GC-MS. Fourteen components were identified in the essential oil. Limonene (75.21%) and terpineol (8.68%) were the major components in SIEO. Since acne vulgaris is the combined result of a bacterial infection and the inflammatory response to that infection, we examined whether SIEO possessed antibacterial against skin pathogens. As a result, SIEO showed excellent antibacterial activities against drug-susceptible and -resistant Propionibacterium acnes and Staphylococcus epidermidis, which are acne-causing bacteria. In this study, SIEO was examined on DPPH radical scavenging activities, which showed moderate antioxidant activity ($SC_{50}$, $15.36{\mu}L/mL$). In order to determined whether SIEO can be safely applied to human skin, the cytotoxicity effects of SIEO were determined by colorimetric MTT assays in normal human fibroblasts and keratinocyte HaCaT cells. They exhibited low cytotoxicity at $0.5{\mu}L/mL$ in both celllines. Based on these results, we suggest the possibility that essential oil of 'Shiranuhi' maybe considered as an antibacterial and antioxidant agent.

Microstructural Evaluation and High Temperature Mechanical Properties of Ni-22Cr-18Fe-9Mo ODS Alloy (Ni-22Cr-18Fe-9Mo계 ODS 합금의 미세조직 및 고온인장 특성 평가)

  • Jeong, Seok-Hoan;Kang, Suk-Hoon;Han, Chang-Hee;Kim, Tae-Kyu;Kim, Do-Hyang;Jang, Jin-Sung
    • Journal of Powder Materials
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    • v.18 no.5
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    • pp.456-462
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    • 2011
  • Yttrium oxide is one of the most thermo-dynamically stable materials, so that it is generally used as a dispersoid in many kinds of dispersion strengthed alloys. In this study, a nickel-base superalloy is strengthened by dispersion of yttrium oxide particles. Elemental powders with the composition of Ni-22Cr-18Fe-9Mo were mechanically alloyed(M.A.) with 0.6 wt% $Y_2O_3$. The MA powders were then HIP(hot isotactic press)ed and hot rolled. Most oxide particles in Ni-22Cr-18Fe-9Mo base ODS alloy were found to be Y-Ti-O type. The oxide particles were uniformly dispersed in the matrix and also on the grain boundaries. Tensile test results show that the yield strength and ultimate tensile strength of ODS alloy specimens were 1.2~1.7 times higher than those of the conventional $Hastelloy^{TM}$ X(R), which has the same chemical compositions with ODS alloy specimens except the oxide particles.

Corrosion Behavior of Ti-6Al-4V Alloy after Plasma Electrolytic Oxidation in Solutions Containing Ca, P and Zn

  • Hwang, In-Jo;Choe, Han-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2016.11a
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    • pp.120-120
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    • 2016
  • Ti-6Al-4V alloy have been used for dental implant because of its excellent biocompatibility, corrosion resistance, and mechanical properties. However, the integration of such implant in bone was not in good condition to achieve improved osseointergraiton. For solving this problem, calcium phosphate (CaP) has been applied as coating materials on Ti alloy implants for hard tissue applications because its chemical similarity to the inorganic component of human bone, capability of conducting bone formation and strong affinity to the surrounding bone tissue. Various metallic elements, such as strontium (Sr), magnesium (Mg), zinc (Zn), sodium (Na), silicon (Si), silver (Ag), and yttrium (Y) are known to play an important role in the bone formation and also affect bone mineral characteristics, such as crystallinity, degradation behavior, and mechanical properties. Especially, Zn is essential for the growth of the human and Zn coating has a major impact on the improvement of corrosion resistance. Plasma electrolytic oxidation (PEO) is a promising technology to produce porous and firmly adherent inorganic Zn containing $TiO_2(Zn-TiO_2)$coatings on Ti surface, and the a mount of Zn introduced in to the coatings can be optimized by altering the electrolyte composition. In this study, corrosion behavior of Ti-6Al-4V alloy after plasma electrolytic oxidation in solutions containing Ca, P and Zn were studied by scanning electron microscopy (SEM), AC impedance, and potentiodynamic polarization test. A series of $Zn-TiO_2$ coatings are produced on Ti dental implant using PEO, with the substitution degree, respectively, at 0, 5, 10 and 20%. The potentiodynamic polarization and AC impedance tests for corrosion behaviors were carried out in 0.9% NaCl solution at similar body temperature using a potentiostat with a scan rate of 1.67mV/s and potential range from -1500mV to +2000mV. Also, AC impedance was performed at frequencies ranging from 10MHz to 100kHz for corrosion resistance.

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Corrosion Resistance Characteristics of Cold Rolled Steel by Cr-free Green Organic/Inorganic Hybrid Coating Solution (크롬 프리 친환경 유/무기 하이브리드 코팅액에 의한 냉연강판의 내식특성)

  • Nam, Ki Woo;Kim, Jung Ryang;Choi, Chang Min
    • Journal of Ocean Engineering and Technology
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    • v.27 no.2
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    • pp.33-38
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    • 2013
  • In the past, a very popular method for reducing the corrosion on zinc involved the use of chemical conversion layer coatings based on $Cr^{+6}$. However, there is an important problem with using chromium salts as a result of restrictive environmental protection legislation. This study investigated the optimum condition for galvanized steel using an organic/inorganic solution with a Ti composition. In the case of a fixed heat treatment time, the corrosion resistance values of LR-0727(1) and LR-0727(2) were improved as the heat treatment temperature increased, and the optimum minimum temperature decreased with the heat treatment time. At the optimum heat treatment condition of two coating solutions, the heat treatment time of the LR-0727(1) solution was shorter than LR-0727(2) for the same heat treatment temperature. LR-0727(1) coated specimens did not show desquamation, and all of the specimens showed a good adhesive property. In contrast, in the case of the LR-0727(2) coated specimens, desquamation arose. Therefore, the adhesive property of LR-0727(1) was superior to that of LR-0727(2). The pencil hardness had a 3H average for all of the coating solutions and heat treatment conditions. In the case of a corrosion resistance test with boiling water, the coated specimens of LR-0727(1) were discolored, but LR-0727(2) was not. Finally, LR-0727(1) was more moisture proof than LR-0727(2).

Study on the corrosion resistance of coating mixture to acid for the desulfurization system (탈황설비용 탄소강 코팅조성물의 내산성에 관한 연구)

  • Kim, In-Ki;Ryu, Jeong-Koon
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.16 no.6
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    • pp.278-285
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    • 2006
  • Coating mixtures of the resin B-H for the application to the desulfurization system of power plant were coated on carbon steels and cured at the temperature of $65^{\circ}C{\sim}80^{\circ}C$. After being contacted with 70wt% $H_2SO_4$ solution of $100^{\circ}C\;and\;120^{\circ}C$ for several hours, their composition, Vicker's hardness and microstructures by SEM were examined. Corrosion resistance of the coating mixtures to $H_2SO_4$ solution was related to the content of $SO_3$ in the coated specimens after corrosion test. The lower curing temperature and the shorter curing time the coated specimens went through, the higher corrosion resistance to acid they showed, but the more cracks were developed at higher temperature. It was realized that the corrosion resistance to sulfaric acid solution was increased on the condition of curing temperature above $65^{\circ}C$ and curing time above 12 hours at least.

A Study on the Characteristics and Utilization of Ash from Sewage Sludge Incinerator (하수(下水)슬러지 소각재의 특성(特性) 평가(評價) 및 재활용(再活用)을 위한 기초연구(基礎硏究))

  • Lee, Hwa-Young
    • Resources Recycling
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    • v.17 no.3
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    • pp.3-9
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    • 2008
  • The measurement of physicochemical properties and chemical composition of SSA(sewage sludge ash) has been carried out and the preparation of lightweight material has also been performed using SSA for reuse as building or construction materials. For this aim, lightweight material has been prepared by forming the mixture of SSA, lightweight filler and inorganic binder followed by calcination at elevated temperature and characterized in terms of density and compressive strength. The pH of fly ash was found to be slightly alkaline, pH 8.69, due to the addition of caustic soda in order to neutralize the acidic gas while the pH of bottom ash was 6.48 Heavy metal leachability based on the standard leach test was also found to be below the detection limit for Cd, Cu, Pb, As and Cr of SSA. As far as the compressive strength of lightweight material was concerned, the compressive strength of lightweight material using fly ash was higher than that of lightweight material using bottom ash.

Effects of Surface Machining by a Lathe on Microstructure of Near Surface Layer and Corrosion Behavior of SA182 Grade 304 Stainless Steel in Simulated Primary Water

  • Zhang, Zhiming;Wang, Jianqiu;Han, En-hou;Ke, Wei
    • Corrosion Science and Technology
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    • v.18 no.1
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    • pp.1-7
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    • 2019
  • To find proper lathe machining parameters for SA182 Grade 304 stainless steel (SS), six kinds of samples with different machining surface states were prepared using a lathe. Surface morphologies and microstructures of near surface deformed layers on different samples were analysed. Surface morphologies and chemical composition of oxide films formed on different samples in simulated primary water with $100{\mu}g/L\;O_2$ at $310^{\circ}C$ were characterized. Results showed that surface roughness was mainly affected by lathe feed. Surface machining caused grain refinement at the top layer. A severely deformed layer with different thicknesses formed on all samples. In addition to high defect density caused by surface deformation, phase transformation, residual stress, and strain also affected the oxidation behaviour of SA182 Grade 304 SS in the test solution. Machining parameters used for # 4 (feed, 0.15 mm/r; back engagement, 2 mm; cutting speed, 114.86 m/min) and # 6 (feed,0.20 mm/r; back engagement, 1 mm; cutting speed, 73.01 m/min) samples were found to be proper for lathe machining of SA182 Grade 304 SS.

Microstructure Analysis of Cement Composite containing PMHS Emulsion to Improve Hydrophobic (소수성 증진을 위한 PMHS 유액 혼입 시멘트 복합체의 미세구조 분석)

  • Kim, Younghwan;Oh, Hongseob
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.25 no.1
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    • pp.25-32
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    • 2021
  • For developing the durable eco-concrete, water-repellent and hydrophobic emulsion were prepared by stirring and mixing polymethyl hydrosiloxane and polyvinyl alcohol. After adding the PMHS emulsion cement paste, the hydration reaction characteristics and the change in chemical composition were analyzed through BSE and EDS analysis, and the micropores were evaluated by MIP test. Cement mixed with PMHS emulsion was analyzed to increase the hydration reactivity and to decrease the capillary porosity, but it was found that the capillary porosity varies depending on the degree of dispersion of the emulsion in the cement paste. In the case of the emulsion containing metakaolin, there was little difference in hydration degree and porosity from the case of using only the PMHS emulsion. However, when the cement surface was coated with PMHS emulsion, the contact angle was found to increase significantly compared to OPC, and it was analyzed that especially when PVA fiber was used together, it changed to a hypohydrophobic surface.