• Title/Summary/Keyword: Ceramic microstructure

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Influence of the Metallization During the Manufacturing of the Ceramic Capacitor on the Dielectric Properties (콘덴사 제어에 있어서 금속화과정이 유도특성에 미치는 영향)

  • Ho-Gi Kim
    • The Transactions of the Korean Institute of Electrical Engineers
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    • v.33 no.2
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    • pp.83-87
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    • 1984
  • Influence of the metallization during the manufacturing of the ceramic multilayer capacitor on the dielectric properties was studied as a change of the capacity and the dissipation factor. Due to the change of the relative dielectric constant as a function of the measuring temperature the influence of the metallization could be obtained and the change of the dissipation factor as a function of the measuring frequency was anaysed. In order to investigate the boundary effect between the metallization and the dielectric a kind of microstructure model at the internal Grain and Grain Boundary was constructed and tried to analyse the change of the dielectric properties.

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Synthesis and Conductivity Properties of LaNiO$_3$ Ceramic Conductors (LaNiO$_3$전도성 세라믹의 합성과 도전특성)

  • 조정호;조주현;김강언;정수태
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11a
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    • pp.406-409
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    • 2001
  • The conductivity properties and synthesis of LaNiO$_3$ ceramics from La$\sub$1+$\delta$/NiO$_3$($\delta$=--0.06, 0, 0.06) were investigated. A single perovskite phase was realized at 800$^{\circ}C$. La$_2$NiO$_4$ and other unexpected oxide were observed at 1000$^{\circ}C$. The Microstructure was showed clearly that it is a low density porous material. LaNiO$_3$ ceramic showed a metallic conductivity. The conductivity of La rich samples had a higher value than the La poor samples.

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Characterizations of Cr-P-PTFE composite coatings electroplated from trivalent chromium-based bath

  • Park, Jong-Kyu;Byoun, Young-Min;Seo, Sun-Kyo;Park, Su-Young;Choi, Sun-Woo
    • Journal of Ceramic Processing Research
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    • v.19 no.6
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    • pp.455-460
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    • 2018
  • Chromium plating is a common surface treatment technique extensively applied in industry due its excellent properties which include substantial hardness, abrasion resistance, corrosion resistance, surface color, and luster. In this study, the effect of PTFE on corrosion behavior of Cr-P plating, low carbon steel substrates are electroplated in Cr(III) baths without and with PTFE. Trivalent chromium carbon plating was electroplated from trivalent chromium sulfate-based baths with different PTFE dispersion contents. The study focused on the microstructure, PTFE content, roughness, and corrosion resistance of the Cr-P-PTFE composite plating. Scanning electron microscopy and atomic force microscopy images showed a smoother plating and a decrease in the surface roughness of the electrodeposited. The results demonstrate that PTFE eliminates the cracks within plating by reducing internal stress. Therefore, the corrosion resistance of Cr-P-PTFE composite platings were better than that of Cr-P alloy platings.

Study on properties of geopolymer-polyurethane sponge composite

  • Chen, Zhilei;Lee, Sang-Jin
    • Journal of Ceramic Processing Research
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    • v.19 no.5
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    • pp.419-423
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    • 2018
  • A newly conceived geopolymer composite was fabricated by a combination of the geopolymer and polyurethane sponge. The density and porosity of hardened geopolymer composite, corresponded to different pore sizes of polyurethane sponge, exhibited no significant differences from each other. However, the mechanical behavior, the compressive strength and flexural strength, showed slight differences accordingly. Fracture of the geopolymer composite exposed to high compressive load was not observed from all specimens containing polyurethane sponge. The toughness enhancement of the geopolymer composite, due to spontaneous elasticity of polyurethane sponge, crack spread, and crack diffraction, was identified through the stress-strain curve and microstructure of fracture surface. The newly designed geopolymer composite having a 3-dimensional sponge skeleton showed relatively higher flexural strength of 8.0 MPa than other conventional geopolymer composites.

Texture Characteristics of TiN Film by Electron Backscatter Diffraction

  • Jeong, Bong-Yong
    • Korean Journal of Metals and Materials
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    • v.50 no.12
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    • pp.867-871
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    • 2012
  • The microstructure and texture of TiN coatings on a Ni-based super-alloy were characterized by the automated version of electron backscatter diffraction (EBSD), EBSD techniques were used to investigate the very fine TiN grain shape and crystal orientation. This study confirmed that EBSD techniques provide a very useful tool for characterization of coating materials. The TiN grains had a special texture, a {001}-fiber texture in the coating layer. It was also found that, in severe environments, the coating performance of equiaxial and randomly oriented TiN is superior to that with columnar structures.

Color manipulation of silica aerogel by copper incorporation during sol-gel process

  • Lee, Sang-Seok;Park, Il-Kyu
    • Journal of Ceramic Processing Research
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    • v.20 no.1
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    • pp.30-34
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    • 2019
  • Copper (Cu)-incorporated silica aerogel was synthesized by a sol-gel process with two-step drying process for color modification. The microstructure of the silica aerogel was not affected significantly by the Cu concentration and an amorphous structure was maintained without any crystalline impurity phases. The textural properties of the silica aerogels investigated by using N2 adsorption-desorption isotherms exhibited the typical features of mesoporous materials. The pore size and porosity were not changed significantly even with the incorporation of Cu up to 1.5 M, which indicates negligible variation of thermal insulating properties. However, the color of the aerogel changed from white and light greenish to dark greenish with increasing Cu content. The color change of the silica aerogel was due to the modification of the electron energy band structure of silica by the Cu atomic levels. Therefore, the color of the silica aerogel powders could be manipulated by incorporating Cu without degrading the thermal insulating properties.

Microstructure analysis of DLC thin film fabricated by filtered arc ion plating method

  • Park, Y.P.;Kim, T.G.;Cheon, M.W.
    • Journal of Ceramic Processing Research
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    • v.13 no.spc2
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    • pp.363-367
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    • 2012
  • DLC (diamond liked carbon) coating of the tungsten carbide (WC) alloy core surface for molding a glass aspheric lens improves the quality of glass lens and the molding core and is characterized by high hardness, high elasticity, abrasion resistance and chemical stability. In this study, the effect of DLC coating of a thin film by means of the filtered AIP (arc ion plating) technique was examined on Ra and shape of the coated surface. Roughness before and after DLC coating was measured and the result showed that the roughness was improved after coating as compared to before coating. It was observed that DLC coating of the WC alloy core surface for molding had an effect on improving the roughness and shape of the core surface. It is considered that this will have an effect on improving abrasion resistance and the service life of the core surface.

Enhanced salt coating on FeS2 surface with the addition of Li2O

  • Cheong, Hae-Won;Kang, Seung-Ho;Kim, Jong-Myong;Cho, Sung-Baek
    • Journal of Ceramic Processing Research
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    • v.13 no.spc2
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    • pp.198-201
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    • 2012
  • The electrolytes in thermal batteries are nonconductive solids at ambient temperature, which prevent the self-discharge and corrosion. To meet severe environmental requirements and guarantee acceptable handling yields, all the pellets in cells should have adequate strength, especially for the cathodes due to their poor binding properties among FeS2 particles. By modifying the surface microstructure of FeS2 through molten-salt heat treatment, the inter-particle binding strength is greatly increased, resulting in the enhanced pellet strength and yield. The addition of Li2O also promoted the soft salt coating coverage of hard FeS2 particles, which can be explained by the enhanced wettability of the molten salt.

Fabrication of Ceramic Oxides for Neutron Irradiation (중성자조사를 위한 세라믹 합성)

  • Lee, Sang-Heon
    • Proceedings of the KIEE Conference
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    • 2008.05a
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    • pp.201-202
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    • 2008
  • Formation of pores in melt processed ceramics oxides and its effect on the microstructure were studied. Spherical Pores with a size of a few tens of microns were formed due to the evolution of oxygen gas during melting of a oxide. The liquid pockets were converted into sperical oxide regions with a lower oxide density through the peritectic reaction during subsequent fabrication.

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