• 대한기계학회:학술대회논문집
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• 대한기계학회 2000년도 춘계학술대회논문집A
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• pp.103-108
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• 2000

Since the ceramic/metal joint material is made at a high temperature, the residual stress development when it is cooled from bonding temperature to room temperature due to remarkable difference of thermal expansion coefficient between ceramic and metal. As residual stress at ceramic/metal joints influences the strength of joints, it is important to estimate residual stress quantitatively. In this study, it is attempted to estimate joint residual stress of $Si_3N_4/STS304$ joints quantitatively and to compare the strength of Joints. The difference of residual stress is measured when repeated thermal cycle is loaded under the conditions of the practical use of the ceramic/metal joint. And 4-point bending test is performed to examine the influence of residual stress on fracture strength. As a residual it is known that the stress of joint decreases as the number of thermal cycle increases.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 추계학술대회 논문집 Vol.15
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• pp.79-82
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• 2002

In this paper, a single phase driven piezoelectric motor design was presented for linear motion. Two metal/ceramic composite actuators, a piezoelectric ring which was bonded to a metal endcap from one side, were used as the active elements of this motor. The motor was composed of a piezoelectric ceramic, a metal ring which has 4 arms, and a guider. Motors with 30.0[mm] and 35.0[mm] diameter were studied by finite element analysis and experiments. As results, the maximum speed of motor was obtained at resonant frequency. When the applied voltage of the motor increased, the speed was increased. Also, bidirectional motion of the motor was achieved by combining two motors which have different resonant frequency.

• 대한치과기공학회지
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• 제2권1호
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• pp.69-75
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• 1980

• 대한치과보철학회지
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• 제43권6호
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• pp.707-716
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• 2005

Statement of problem. Collarless metal ceramic fixed partial dentures(FPDs) had an esthetic problem such as opaque reflection in cervical region. To overcome this, modified coping which removed its facial cervical metal could be used. The marginal quality could be worsen according to the amount of its facial metal reduction. Purpose. The purpose of this study was to evaluate marginal fits of collarless metal ceramic FPDs with retainers of modified copings. Material and method. Dentoform maxillary left central incisor and right lateral incisor were prepared for 3-unit collarless metal ceramic FPD and fixed in yellow stone. This model was duplicated to PBT resin dies via CAD/CAM and injection molding. Four different facial margin design groups were investigated. Group A was a coping with a thin facial metal collar, group B was a collarless coping with its facial metal to the shoulder, group C was a collarless coping with its facial metal 1 mm short of the shoulder, and group D was a collarless coping with its facial metal 2 mm short of the shoulder. Seven collarless metal ceramic FPDs per group were fabricated. They were cemented to PBT resin dies with resin cement. After removal of pontics, each retainers were separated and observed under Accura 2000 optical microscope. Then, retainers were embeded in orthodontic resin and cross sectioned faciopalatally. Internal marginal fits of midfacial porcelain margins were observed under FE-SEM. Result and conclusion. Within the limitations of this in vitro study. The following conclusions were drawn. 1. Mean marginal gaps of collarless FPDs were in the $50-60{\mu}m$ range. 2. In midfacial margin, marginal discrepancies were greater in group A than in the experimental groups(p<0.05). 3. In midpalatal margin, marginal gaps were greater in group C and D than in group A and B(p<0.05). 4. Marginal fits of porcelain margins were better than those of metal margins in collarless metal ceramic FPDs. 5. In both teeth, internal marginal gaps of group C and D were greater than those of group A and B(p<0.05).

• Journal of Welding and Joining
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• 제30권3호
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• pp.38-43
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• 2012

In this study, active metal brazing methods for $ZrO_2$ and Ti alloy were discussed. To get a successful metal-ceramic bonding, various factors (melting temperature, corrosion, sag resistance, thermal expansion coefficient etc. of base materilas and filler metal) should be considered. Moreover, in order to clarify bonding between the metal and ceramic, the mechanism of the interfacial structure of the joints should be identified. The driving force for the formation of metal and ceramic interfaces is the reduction of the free energy which occurs when their contact becomes complete. Interfacial bonding depends on the material combinations and the bonding processes. This study describes the bonding between ceramic and metal in an active metal brazing.

• 대한치과교정학회지
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• 제22권2호
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• pp.327-343
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• 1992

Metal brackets and ceramic brackets were bonded to natural teeth, porcelain crowns and gold crowns After stored in artificial saliva solution for 72 hours at $37^{\circ}C$, the shear bond strengths were measured by Instron and compared with them, the bonding sites and bracket bases were examined by scanning electron microscope and light optical stereomicroscope. The results were as follows: 1. The shear bond strengths of the group which metal brackets were bonded to natural teeth and the groups which ceramic brackets were bonded to natural teeth and porcelain crowns were comparable to each other, the shear bond strength of the group which metal brackets were bonded to gold crowns was significantly low. 2. The bond failed predominantly at the bracket base/adhesive interface with the bulk of adhesive remaining on enamel in the group which metal brackets were bonded to natural teeth. 3. The bond failed consistently at the crown/adhesive interface with all of adhesive remaining on the bracket babes in the group which metal brackets were bonded to gold crowns. 4. The bond failed at the enamel or crown/adhesive interface with the bulk of adhesive remaining on the bracket bases in the groups which cramic brackets were bonded to natural teeth and porcelain crowns. 5. The shear bond strengths of the groups which ceramic brackets were bonded to porcelain crowns were not affected by etching time.

• 대한치과기공학회지
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• 제23권2호
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• pp.161-170
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• 2002

The Purpose of this study was to investigate the chemically improvement of metal-ceramics bond strength in the course of recasting Ni-Cr metal composite system with 10wt.%, 20wt.% and 30wt.% aluminum respectively. We have tested the bond strength, micro-structure, chemical composition of each metal composites and metal- ceramic bond interfaces by 3-point bending strength tester, SEM and EDS. We have made the conclusions through this study as follow: 1. The most suitable amount of aluminum to the Ni-Cr metal composite recasting is 20wt. % for improving metal-ceramics bond strength with debonding strength value of 49.54 kgf/mm2. 2. The aluminum must be changed to small spread alumina like phases and second aluminum-metal composites phases in the morphology of Ni-Cr metal composite system by adding during it's casting. These second phases have inclined functional oxide phases mixed with metal elements and they must take roll to improvement of metal-ceramics bond strength. 3. In the case of 30wt.% aluminum appended to Ni-Cr metal composite system, an excess of second inclined functional oxide phases produce cracks and spalling of them apart from it's base material. It must be a important factor of reduction of metal-ceramics bond strength.

• 한국산학기술학회논문지
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• 제21권12호
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• pp.434-439
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• 2020

최근, 치과 산업에서 레이저를 열원으로 합금을 제조하는 선택적 레이저 용융법(Selective laser melting, SLM)이 소개되고 있다. 하지만 SLM으로 제작된 금속-세라믹 수복물에 대한 연구가 부족한 실정이다. 따라서 본 연구의 목적은 SLM 그리고 CAST(casting)에 의해 제조된 Co-Cr 합금의 금속-세라믹(metal-ceramic) 결합 강도(bond strength)를 평가하는 것이다. SLM 그리고 CAST 방법을 사용하여 Co-Cr 시편을 제조하고 세라믹을 소결하여 시료를 제작하였다. 연구의 실험은 표본 준비 및 분석을 통해 2020년 1월부터 6월까지 수행되었다. 금속-세라믹 결합 강도는 만능 시험기에 의해 측정되었다. 부착 세라믹의 면적분(The area fraction of adherence ceramic, AFAC)은 SEM/EDS로 시편의 Si 함량을 측정하였다. 금속-세라믹 결합 강도 및 AFAC 결과는 t-test를 사용하여 분석하였다(α = .05). SLM 그리고 CAST Co-Cr 합금 사이의 결합 강도에 대해서는 유의한 차이가 발견되지 않았다(P>.05). SLM은 CAST 그룹보다 많은 세라믹 부착성(ceramic adherence)을 나타냈다(P<.001). 세라믹과 합금의 결합 강도는 제조 방법엥 영향을 받지 않았다. 그러나 SLM은 더 우수한 세라믹 부착성을 보였다. 이는 향후 임플란트 상부 보철물 제작에도 SLM으로 제작한 합금이 사용 가능한 것을 시사한다. CAST 방식의 단점을 극복하고 시간과 비용을 절약할 수 있을 것으로 기대된다.

• The Journal of Advanced Prosthodontics
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• 제6권4호
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• pp.266-271
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• 2014

PURPOSE. The purpose of this study was to compare the fracture strength of the metal and the bond strength in metal-ceramic restorations produced by selective laser sintering (SLS) and by conventional casting (CAST). MATERIALS AND METHODS. Non-precious alloy (StarLoy C, DeguDent, Hanau, Germany) was used in CAST group and metal powder (SP2, EOS GmbH, Munich, Germany) in SLS group. Metal specimens in the form of sheets ($25.0{\times}3.0{\times}0.5mm$) were produced in accordance with ISO 9693:1999 standards (n=30). To measure the bond strength, ceramic was fired on a metal specimen and then three-point bending test was performed. In addition, the metal fracture strength was measured by continuing the application of the load. The values were statistically analyzed by performing independent t-tests (${\alpha}=.05$). RESULTS. The mean bond strength of the SLS group (50.60 MPa) was higher than that of the CAST group (46.29 MPa), but there was no statistically significant difference. The metal fracture strength of the SLS group (1087.2 MPa) was lower than that of the CAST group (2399.1 MPa), and this difference was statistically significant. CONCLUSION. In conclusion the balling phenomenon and the gap formation of the SLS process may increase the metal-ceramic bond strength.

• 대한치과보철학회지
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• 제52권2호
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• pp.90-96
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• 2014

연구 목적: 이 연구의 목적은 열가압성형기법이 금속도재관의 치경부 변연적합도에 미치는 영향을 확인하는 것이다. 연구 재료 및 방법: 실험에 앞서, 4개의 금속 주모형을 형성하였다. 각 모형은 각각chamfer, heavy chamfer, shoulder with bevel, shoulder (collarless)변연을 형성하였다. 각 변연당 10개씩의 금관을 제작하여, 총 40개를 제작하였다. Coping 단계에서, 그리고 금속도재관 완성 단계에서 주모형과 금관 사이의 변연간극은 100배율의 광학현미경 관찰을 통하여 측정되었다. Data분석은 paired t-test along with one-way ANOVA와 Duncan multiple comparison test를 이용하여 이루어졌다. 결과: 변연간극의 평균과 표준편차를 분석한 결과, 금속 코핑과 그 후 완성된 금속도재관, 모든 경우에서 변연부 간격은 임상적 허용범위 안에 있었다. Chamfer 변연 실험군의 경우 Heavy chamfer 변연 실험군에 비하여 금속도재관 완성 후 변연부 간격의 유의한 증가가 있었다. 그리고Shoulder 변연 실험군에서 도재로 처리된 변연이 Chamfer와 Shoulder변연 실험군의 금속변연에 비하여 변연부 간격이 유의하게 작게 나타났다. 결론: 열가압성형기법을 통하여 제작한 금속도재수복물의 변연적합도는 전통적인 방법으로 제작한 금속도재수복물의 변연적합도와 유의한 차이점이 없었다. 제작과정의 효율성으로, 열가압성형기법은 임상에서의 효과적인 사용법으로 고려될 수 있다.