• Journal of the Korean Ceramic Society
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• v.41 no.5
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• pp.406-409
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• 2004

A blue phosphor(ZnS:Cu) is manufactured by solid state reaction for ACPEL(AC powder EL). The effect of artificial defect on phosphor surface on the ZnO phase conversion and resulting luminescence have been studied. It was found that ZnS:Cu could converse to cubic phase more easily due to the formation of artificial defect on 1st fired phosphor by ball-milling process, resulting in improvement of luminescence of phosphor phosphors under the driven EL condition. We found out an optimized ball-mill condition through considering effect of each ball-mill conditions such as milling time and milling rpm on defect. Also we determined relationship between emission luminescence and phase of phosphor based on analyses of crystal structures of phosphors. A significant improvement above 30% was observed in electroluminescence by the artificial defect on ZnS:Cu phosphors compared to non-treated phosphors.

• Journal of the Korean Ceramic Society
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• v.31 no.3
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• pp.337-345
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• 1994

The reaction-sintered alumina and zirconia-alumina ceramics having low firing shrinkage were prepared from the Al/Al2O3 or Al/ZrO2(Ca-PSZ) powder mixtures via the attrition milling. And in this milling process the effect of the characteristics of used powders was investigated. Attrition milling was much more effective in reducing the particle size of ceramic/metal mixed powders than ball milling. Powder mixtures of flake-type Al with coarse alumina was much more effectively comminuted by the attrition milling than the mixtures of globular-type Al with coarse alumina powders. And coarse alumina than fine alumina was much more beneficial in cutting and reducing the ductile Al particles. In the contrary to Al/Al2O3 powder mixtures, Al/ZrO2 powder mixtures was not effectively comminutd. But whether using the alumina ball media or attrition milled with Al2O3 powder rather than Al, the milling efficiency was much more increased.

• Journal of the Korean Ceramic Society
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• v.43 no.9 s.292
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• pp.519-526
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• 2006

A full-factorial design of experiments with three input factors and two levels for each factor including center points was utilized for the preparation and characterization of twelve types of $BaTiO_3$ slips for tape casting. Ceramic powders with different particle sizes, different milling methods such as high energy milling and conventional ball milling, and two types of dispersant with different polymeric species were chosen as input factors in order to investigate their effects on slip and on green tape properties. Tape casting, a small rectangular-shaped K-square preparation, characterization and quantitative data analysis using statistical software were followed. Ceramic powder was the most significant among three input factors for the output responses of slip viscosity and green tape density, showing more favorable results with large particles than with very fine ones. In addition, high energy milling for only 30 min was more efficient than 24h of conventional ball milling in terms of powder dispersion and milling. The optimum condition based on the experimental results was a slip exposed to high energy milling with large ceramic particles along with a methylethyl acetate dispersant.

• Journal of the Korean Ceramic Society
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• v.34 no.11
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• pp.1187-1197
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• 1997

Dry gel composed of primary particles more homogeneous than starting boehmite powder was prepared by dispersing and gelling the boehmite powder. The transformation temperatures of boehmite powder, dry gel seeded with 0, 1, 3, 5 wt% $\alpha$-Al2O3, and ball milled gel were 1192$^{\circ}C$, 1184$^{\circ}C$, 1141$^{\circ}C$, 1119$^{\circ}C$, 1117$^{\circ}C$, and 1106$^{\circ}C$, respectively. Sintering behavior of dry gel without seed was similar to that of boehmite powder, but the sintered density of dry gel was improved as much as 10%~15% than boehmite powder. In the case of dry gel seeded with 5 wt% $\alpha$-Al2O3, sintering behavior was much improved. The relative density of the gel seeded with 5 wt% $\alpha$-Al2O3 was 96% when sintered at 140$0^{\circ}C$ for 1h. On the other hand, ball milling of the non-seeded sol for 48h resulted in the relative density of 97% when sintered at 130$0^{\circ}C$ for 1h. The size and amount of $\alpha$-Al2O3 particles added by ball milling were 0.107 ${\mu}{\textrm}{m}$ and 0.5 wt%.

• Journal of the Korean Ceramic Society
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• v.39 no.2
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• pp.126-134
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• 2002

Fabrication of mortar containing fly ash for high strength structural material was investigated by using a Mechanochemically Processed Cement (MPC) and/or Fly Ash (MPFA), which was compared to the specimen (at the same fabrication condition of fly ash adding contents (10, 20 and 30 wt%) and curing time (7 and 28 days)) fabricated by using Ball-mill Processed Cement (BPC) and As Received Fly Ash (ARFA) in terms with compressive strength and microstructures. Mortar specimen fabricated by using MPC and ARFA showed 5-11% higher compressive strength than that in the case of using BPC and ARFA, and mortar specimen by using BPC and MPFA represented 10-20% higher compressive strength than that for the case of using BPC and ARFA. Furthermore, mortar specimen fabricated by simultaneously using MPC and MPFA exhibited about 24% higher value of compressive strength than that for the case of using BPC and ARFA, which was considered to be synergic efficiency in increasing compressive strength. Increased compressive strength as above mentioned is considered to be caused by mutually increased affinity between cement and fly ash induced during mechanochemical Processing(MP).

• Proceedings of the KSME Conference
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• 2005.11a
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• pp.31.1-31.1
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• 2005

• Korean Journal of Environmental Agriculture
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• v.35 no.1
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• pp.72-78
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• 2016

BACKGROUND: Entomopathogenic fungi have been studied to develop for biological control agents as an alternative to chemical control agents in insect pest management. This investigated to determine the optimal culture conditions in ceramic balls for maximal sporulation of entomopathogenic fungi Beauveria bassiana M130 by use rice bran extract.METHODS AND RESULTS: METHODS AND RESULTS: A culture of entomopathogenic fungi for 12day on rice bran extract(1:8, w/v) incubated in ceramic matrix at 28℃. Natural zeolite ceramic ball was high production of 4.2×108 conidial/mL. The culture condition optimized initial pH, temperature, rice bran extract concentration, adhesives substance and concentration of NaCl, respectively. The high production of spore optimal conditions were temperature 28℃, initial pH 3, rice bran extract 3 mL, starch 33 g, 5 % NaCl and sopre suspension 7 mL, respectively.CONCLUSION: This study was carried out for the mass production of entomopathogenic fungi conidia recover rate 65% in matrix of natural zeolite ceramic ball, and to develop ingredient-used formulation of Beauveria bassiana M130 conidia for biological control agents.

• The Journal of Korean Academy of Prosthodontics
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• v.40 no.6
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• pp.572-576
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• 2002

This investigation was designed to estimate the biaxial flexure strength and fracture toughness of lithium disilicate glass-ceramics of IPS Empress 2 system pressed with as-received ingots and their sprue buttons. Two groups of the lithium disilicate glass-ceramics were prepared as follows: group 1 is ingot-pressed group; group 2 is sprue button-pressed group. A ball-on-three-ball test was used to determine biaxial flexure strength (BFS) of disks in wet environment. Scanning electron microscopy(SEM) analysis was conducted to observe the microstructure of the ceramics. Unpaired t-test showed that there were no differences in the mean biaxial Hem strength (BFS) and KIC values between group 1 and 2 (p > 0.05). Two groups showed similar values in the KIC and the strength at 5% failure probability. The SEM micrographs of the IPS Empress 2 glass-ceramic showed a closely packed, multi-directionally interlocking pattern of numerous lithium disilicate crystals protruding from the glass matrix. The lithium orthophosphate crystals could not be observed on the fracture surface etched. There was no a marked difference of the microstructure between group 1 and 2. Although there were no tests including color stability, casting accuracy, etc., the results of this study implied that we could reuse the sprue button of the pressed lithium disilicate glass-ceramic of IPS Empress 2 system.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2003.05e
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• pp.57-60
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• 2003

This paper explained electric field distribution's characteristics of dielectric pellets with a shape of ball to voltage. When discharge gap of electrode and input voltage are each 20[mm], 10000[V], the electric field simulation results of dielectric pellets with a shape of ball with relative dielectric constant of several kind measured stronger electric field near electric pellets with a shape of ball of ${\phi}5$[mm] than $1{\phi}$[mm] and $3.33{\phi}$[mm] at atmosphere. And the maximum electric field of dielectric pellets with a shape of ball over ${\phi}5$[mm] increased about 5[%] to maximum electric field of electric pellets with a shape of ball ${\phi}5$[mm]. And the result of simulation, when relative dielectric constant of dielectric pellets with a shape of ball is 100, it measured about 90[%] of maximum electric field of dielectric pellets with a shape of ball with relative dielectric constant over 1000.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2004.04a
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• pp.416-423
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• 2004

This paper presents the thermal characteristic analysis of a high-speed horizontal machining center with spindle speed of 50,000rpm and feedrate of 120m/fin. The spindle system is designed based on the built-in motor, angular contact ceramic ball bearings, oil-air lubrication and oil-jacket cooling method. The X-axis and Y-axis feeding systems are composed of the linear motors and linear motion guides, and the Z-axis feeding system is composed of the servo-motor, ball screw and linear motion guides. The thermal characteristics such as the temperature distribution, temperature rise, thermal deformation and step response, are estimated based on the finite element model of machining center and the heat generation rates of heat sources related to the machine operation conditions. Especially, the thermal time constant assessed from the step response function is introduced as an index of thermal response characteristics.