• Wind and Structures
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• 제9권4호
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• pp.271-296
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• 2006

The frequency of a traditional tuned liquid column damper (TLCD) depends solely on the length of liquid column, which imposes certain restrictions on its application to long span cable-stayed bridges during construction. The configuration of a cable-stayed bridge varies from different construction stages and so do its natural frequencies. It is thus difficult to apply TLCD with a fixed configuration to the bridge during construction or it is not economical to design a series of TLCD with different liquid lengths to suit for various construction stages. Semi-active tuned liquid column damper (SATLCD) with adaptive frequency tuning capacity is studied in this paper for buffeting response control of a long span cable-stayed bridge during construction. The frequency of SATLCD can be adjusted by active control of air pressures inside the air chamber at the two ends of the container. The performance of SATLCD for suppressing combined lateral and torsional vibration of a real long span cable-stayed bridge during construction stage is numerically investigated using a finite element-based approach. The finite element model of SATLCD is also developed and incorporated into the finite element model of the bridge for predicting buffeting response of the coupled SATLCD-bridge system in the time domain. The investigations show that with a fixed container configuration, the SATLCD with adaptive frequency tuning can effectively reduce buffeting response of the bridge during various construction stages.

• Steel and Composite Structures
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• 제27권6호
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• pp.727-745
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• 2018

The design criteria and the corresponding performance levels characterize the response of extended stiffened end-plate beam-to-column joints. In order to guarantee a ductile behavior, hierarchy criteria should be adopted to enforce the plastic deformations in the ductile components of the joint. However, the effectiveness of thesecriteria can be impaired if the actual resistance of the end-plate material largely differs from the design value due to the potential activation of brittle failure modes of the bolt rows (e.g., occurrence of failure mode 3 in the place of mode 1 per bolt row). Also the number and the position of bolt rows directly affect the joint response. The presence of a bolt row in the center of the connection does not improve the strength of the joint under both gravity, wind and seismic loading, but it can modify the damage pattern of ductile connections, reducing the gap opening between the end-plate and the column face. On the other hand, the presence of a central bolt row can influence the capacity of the joint to resist the catenary actions developing under a column loss scenario, thus improving the joint robustness. Aiming at investigating the influence of these features on both the cyclic behavior and the response under column loss, a wide range of finite element analyses (FEAs) were performed and the main results are described and discussed in this paper.

• Archives of Pharmacal Research
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• 제23권6호
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• pp.568-573
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• 2000

A reversed-phase high-performance liquid chromatographic method was developed to determine the optical purity of bevantolol enantiomers. (S)-(-)-Menthyl chloroformate((-)-MCF), (S)-(-)-$\alpha$-methylbenzyl isocyanate((-)-MBIC) and 2,3,4,6-tetra-O-acetyl-$\beta$-D-glucopyranosyl isothiocyanate(GITC), which can react with the secondary amine group of bevantolol were investigated as chiral derivatization reagents. Among them indirect chiral HPLC method using CITC gave the best result. The derivatization proceeded quantitatively within 20 min at room temperature. Separation of the enantiomers as diastereomers was achieved by reversed-phase HPLC within 20min using ODS column. Different ratios of (S)-(-)-bevantolol and (R)-(+)-bevantolol were prepared. Enantiomeric separation of these mixtures took place on a chiralcel OD column or, after derivatization with GITC, on a ODS column. No racemization was found during the experiment. This method allowed determination of 0.05% of either enantiomer in the presence of its stereoisomer and method validation showed adequete linearity over the required range.

• 한국세라믹학회지
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• 제49권4호
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• pp.369-374
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• 2012

Based on the structure feature of a tree, a cylindrical $Ti_2AlC$/graphite layered composite has been fabricated through heat treating a graphite column and six close-matched thin wall $Ti_2AlC$ cylinders bonded with the $Ti_2AlC$ powders at $1300^{\circ}C$ and low oxygen partial pressure. SEM examination reveals that the bond interlayers between cylinders or that between cylinder and column are not fully dense without any crack formation. During the compressive test, the strain of the $Ti_2AlC$/graphite layered composite is about twice higher than that of the monolithic $Ti_2AlC$ ceramic, and the compressive strength of the layered composite is 348 MPa. The layered composite show the noncatastrophic fracture behaviors due to the debonding and shelling off of the layers, which are different from the monolithic $Ti_2AlC$ ceramic. The mechanism of the improved deformation capacity and noncatastrophic failure modes are attributed to the presence of the central soft graphite column and cracks deflection by the bond interlayers.

• Steel and Composite Structures
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• 제30권3호
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• pp.271-280
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• 2019

In this paper, numerical and experimental assessments have been conducted in order to investigate the capability of using CFRP for the seismic capacity improvement and relocation of plastic hinge in reinforced concrete connections. Two scaled down exterior reinforced concrete beam to column connections have been used. These two connections from a strengthened moment frame have been tested under uniformly distributed load before and after optimization. The results of experimental tests have been used to verify the accuracy of numerical modeling using computational ABAQUS software. Application of FRP plate on the web of the beam in connections to improve its capacity is of interest in this paper. Several parametric studies were carried out for CFRP reinforced samples, with different lengths and thicknesses in order to relocate the plastic hinge away from the face of the column.

• Natural Product Sciences
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• 제27권4호
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• pp.264-273
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• 2021

Simultaneous quantification of multiple marker compounds in herbal medicine by high performance liquid chromatography (HPLC) analysis is still a challenge due to the complexity in various parameters to be considered and co-existing multi-components. As a case study, a reliable HPLC method for simultaneous quantification of paeoniflorin from Paeoniae Radix and decursin from Angelicae Gigantis Radix in various commercial herbal medicine was developed based on analytical quality by design (AQbD) strategy. As a first step, risk assessment was performed to select the critical method parameters (CMPs) which were decided as organic mobile phase ratio and column oven temperature. In order to evaluate the effect of the CMPs on critical method attributes (CMAs) of peak resolution and tailing, central composite design (CCD) was employed. The final chromatographic conditions were optimized as follows: column- C₁₈, 4.6 × 250 mm, 5 ㎛ particle size; mobile phase- A: acetonitrile, B: 0.1% acetic acid water; detection wavelength- 235 nm for paeoniflorin, 325 nm for decursin; column oven temperature- 25℃; flow rate- 1.0 mL/min; gradient mobile phase system as Time (min) : % A, 0:14, 25:14, 30:50, 60:50, 61:100, 65:100, 66:14, 75:14. The method was successfully validated according to the International Conference on Harmonization (ICH) guidelines and piloted for ten commercial herbal medicines.

• Steel and Composite Structures
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• 제42권2호
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• pp.161-172
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• 2022

In this paper, four specimens of CFST column joints with endplates and long bolts are tested in the scenario of progressive collapse. Flush endplate and extended endplate are both adopted in this study. The experimental results show that increasing the thickness of the endplate could improve the behavior of the joint, but delay the mobilization of catenary action. The thickness of the endplate should not be relatively thick in comparison to the diameter of the bolts, otherwise catenary action would not be mobilized or work effectively. Effective bending deformation of the endplate could help the formation and development of catenary action in the joints. The performance of flexural action in the joint would affect the formation of catenary action in the joint. Extra middle-row bolts set at the endplates and structural components set below the bottom beam flange should be used to enhance the robustness of joints. A special weld access hole between beam and endplate should be adopted to mitigate the chain damage potential of welds. It is suggested that the structural components of joints should be independent of each other to enhance the robustness of joints. Based on the component method, a formula calculating the stiffness coefficient of preloaded long bolts was proposed whose results matched well with the experimental results.

• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2002년도 추계학술대회논문집
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• pp.927-932
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• 2002

The stability ratio and vibrational amplitude of each tube inside a steam generator have different values. We estimate the characteristics of flow-induced vibration for CE type steam generator with various column and row number of the tube. To obtain the thermal-hydraulic data and stability ratio we use the ATHOS3-MODI and PIAT-FEI/TE code respectively. It turns out that the steam generator has a bounded central zone with the distributed values of the stability ratio and the vibrational amplitude, and those values across the zone boundary become decreased.

• 오토저널
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• 제14권5호
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• pp.41-53
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• 1992

The main purpose of this study is to investigate the atomizing characteristics of a two phase spray by using a liquid column type coaxial nozzle. The experiments have been carried out to analyze the atomization behavior, the droplet size distributions, and the statistical properties of droplet size distributions. Immersion sampling method and the image processing technique were adapted for the measurements of particles, and the distributions of the droplet sizes were statistically analyzed. In the experiments, the mass ratio defined as Mr= $M_{\sigma}$/ $M_{1}$ has been changed from 1.0 to 3.4 and the measurements have been performed along the axis of the spray. As a result of this experimental study, the distributions of droplet size were satisfied with the Log-Normal distributions and arithmetic mean diameter and deviation of mass ratio. Droplet volume-surface mean diameter was denoted by a exponential function of mass-ratio and the exponent was denoted by linear relation according to the central axis from the nozzle. Dispersions, skewness factors and flatness factors had comparatively constant values regardless of mass ratio and location.

• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2002년도 추계학술대회논문초록집
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• pp.390.2-390
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• 2002

The stability ratio and vibrational amplitude of each tube inside a steam generator have different values. We estimate the characteristics of flow-induced vibration for CE type steam generator with various column and row number of the tube. To obtain the thermal-hydraulic data and stability ratio we use the ATHOS3 and PIAT-FEI/TE code respectively. It turns out that the steam generator has a bounded central zone which the distributed values of the stability ratio and the vibrational amplitude, and those values across the zone boundary become decreased.