• Title/Summary/Keyword: Carbon coated

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Evaluating Joint Motion Sensing Efficiency According to the Implementation Method of CNT-Based Fabric Sensors (CNT 기반의 직물센서 구현 방법에 따른 관절동작 센싱 효율 평가)

  • Cho, Hyun-Seung;Yang, Jin-Hee;Lee, Joo-Hyeon
    • Science of Emotion and Sensibility
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    • v.24 no.4
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    • pp.129-138
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    • 2021
  • This study aimed to determine the effects of the shape and attachment position of stretchable textile sensors coated with carbon nanotube on their performance when used to measure children's joint movements. Moreover, the child-safe requirements for fabric motion sensors are established. The child participants were advised to wear integrated clothing equipped with the sensors of various shapes (rectangular and boat-shaped) and attachment positions (at the knee and elbow joints or 4 cm below the joints). The voltage change induced by the elongation and contraction of the fabric sensors was determined for arm and leg flexion-extension motions at 60 deg/s (three measurements of 10 repeats each for 60°and 90°angles, for a total of 60 repetitions). Their dependability was determined by comparing the fabric motion sensors to the associated acceleration sensors. The experimental results indicate that the rectangular-shaped sensor affixed 4 cm below the joint is the most effective fabric motion sensor for measuring children's arm and leg motions. In this study, we designed a textile sensor capable of tracking children's joint motion and analyzed the sensor shape and attachment position on motion sensing clothing. We demonstrated that flexible fabric sensors integrated into garments may be used to detect the joint motions of the human body.

Thermal Performance Evaluation of Composite Phase Change Material Developed Through Sol-Gel Process (졸겔공법을 이용한 복합상변화물질의 열성능 평가)

  • Jin, Xinghan;Haider, Muhammad Zeeshan;Park, Min-Woo;Hu, Jong-Wan
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.43 no.5
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    • pp.555-566
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    • 2023
  • In this study, a composite phase change material (CPCM) produced using the SOL-GEL technique was developed as a thermal energy storage medium for low-temperature applications. Tetradecane and activated carbon (AC) were used as the core and supporting materials, respectively. The tetradecane phase change material (PCM) was impregnated into the porous structure of AC using the vacuum impregnation method, and a thin layer of silica gel was coated on the prepared composite using the SOL-GEL process, where tetraethyl orthosilicate (TEOS) was used as the silica source. The thermal performance of the CPCM was analysed using differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). DSC results showed that the pure tetradecane PCM had melting and freezing temperatures of 6.4℃ and 1.3℃ and corresponding enthalpies 226 J/g and 223.8 J/g, respectively. The CPCM exhibited enthalpy of 32.98 J/g and 27.7 J/g during the melting and freezing processes at 7.1℃ and 2.4℃, respectively. TGA test results revealed that the AC is thermally stable up to 500℃, which is much higher than the decomposition temperature of the pure tetradecane, which is around 120℃. Moreover, in the case of AC-PCM and CPCM thermal degradation started at 80℃ and 100℃, respectively. The chemical stability of the CPCM was studied using Fourier-transform infrared (FT-IR) spectroscopy, and the results confirmed that the developed composite is chemically stable. Finally, the surface morphology of the AC and CPCM was analysed using scanning electron microscopy (SEM), which confirmed the presence of a thin layer of silica gel on the AC surface after the SOL-GEL process.

Effects of Coating Materials on Fluidity and Temperature Loss of Molten Metals from Runner Systems in Full Moulds.

  • Cho, Nam-Don;Kim, Yong-Hyun;Choi, Jung-Kwon
    • Journal of Korea Foundry Society
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    • v.10 no.1
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    • pp.31-42
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    • 1990
  • The full mould casting process in one of the newly developed techniques which has many advantages. Unbonded sand mould has been prepared for the major mould and $CO^2$ gas mould has been used occasionally for comparison. Patterns were built up with expanded polystyrene and coated with three different materials. Silica, graphite and zircon were used for the coating layer. The effects on fluidity and temperature loss of molten metals were investigated. The molten metals were Al-5% Si alloy, Cu-30% Zn alloy and gray iron of approximately 4.0% of carbon equivalent. Experimental variables were runner section area, superheat, sprue height, coating materials, coating thickness and apparent density of EPS pattern. The effects of coating materials on fluidity and temperature loss of the molten metals during transient pouring are summarized as follows : As runner section area, superheat and sprue height increased, fluidity increased. Temperature loss decreased as runner section area and sprue height increased. However, reversed effects were observed in the case of superheat increment. The coating materials decreased the fluidity of each alloy in the order of silica, graphite and zircon. Zircon brought to the highest temperature loss among the coating materials used. The fluidity increased in the order gray iron, Cu-30% Zn and Al-5% Si alloy while temperature loss in the reverse order. Especially in case of reduced pressure process, the fluidity was increased apparently. Al-5% Si alloy showed the lowest temperature loss among the alloys. The increment of the apparent density of EPS pattern resulted in the fluidity decrease and temperature loss increase. The relation between fluidity and temperature loss of each alloy can be expressed by the following equation within the coating thickness limit of 0.5-1.5㎜. F^*={\frac{a}{T^*-b}}-c$ where, $F^*$ : fluidity in the Full mould, $T^*$ : temperature loss in the mould. a : parameter for full mould. b, c : constants.

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Humidity Sensitive Properties of Polymer Electrolytes of Quaternary Ammonium methacrylate derivatives (메타크릴레이트계 4차 암모늄 유도체 고분자 전해질의 감습특)

  • Kim, Tae-Mi;Gong, Myeong-Seon;Lee, Im-Yeol;Park, Jeong-Gi
    • Korean Journal of Materials Research
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    • v.3 no.6
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    • pp.598-605
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    • 1993
  • Methacryloxyethyl dimethyl alkyl($C_{1}\sim C_{12}$, benzyl and 2, 2-diethoxy ethyl) ammonium bromide monomers were prepared to investigate the relative humidity characteristics for polymer electrolytes with different chemical structures. They were coated on the alumna substrate printed comblike gold electrode by photopolymerization after micro-syringe injection. As the thickness of rhe humid membrane increased, the impendance decreased, whereas the impedance ~ncreased as the carbon cham of alkyl substituent in the monomer increased. The impendance of the polymeric electrolytes with $C_6\sim C_8$ substituents were varied from 19M$\Omega$ to 5K$\Omega$ for the range of 30-90% Mi. The temperature depedence coefficient in the range of 15-$35^{\circ}C$ was found to be -0.45% $RH/^{\circ}C$and the hysteresis falled within the range of $\pm$2% RH. The response time was 35 second for varying humldity from 33% to 85% RH.

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Bond Properties of CFRP Rebar in Fiber Reinforced High Strength Concrete with Surface Treatment Methods of Reinforcing Fibers (보강섬유의 표면처리에 따른 섬유보강 고강도콘크리트와 CFRP 보강근의 부착특성)

  • Park, Chan-Gi;Won, Jong-Pil;Cha, Sang-Sun
    • Journal of the Korea Concrete Institute
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    • v.21 no.3
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    • pp.275-282
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    • 2009
  • The effects of surface treatment method of reinforcing fiber on the bonding strength between carbon fiber reinforced polymer rebar (CFRP rebar) and high strength concrete have been evaluated in this study. The structural PVA fiber is coated with a proprietary hydrophobicoiling agent and crimped type polyolefin based structural synthetic fiber is deformed with a geometrical modification were used for the reinforcing fiber. The compressive tests have been performed to evaluate the strength property of high strength concrete depending on the surface treatment method of fiber. The bonding property between the high strength concrete and the CFRP rebar was evaluated by means of direct bonding test. The test results indicated that the surface treatment method of fiber effect on the bonding behavior of high strength concrete and CFRP rebar. Also, as the development and propagation of splitting cracks were controled by adding fibers into the high strength concrete, the bonding behavior, bond strength and relative bonding strength of CFRP rebar and high strength concrete were significantly improved.

An Improved Method for EM Radioautographic Techniques using Cork (EM Radioautographic Techniques에 관(關)한 연구(硏究) - Cork 방법(方法) -)

  • Kim, Myung-Kook;Hassler, R.
    • Applied Microscopy
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    • v.10 no.1_2
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    • pp.7-17
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    • 1980
  • Electron microscope radioautography introduced by Liquier-Milward (1956) is now used routinely in many laboratories. Most of the technical difficulties in specimen preparation have been overcome. This method is modified from loop method for improvement of EM radioautographic techniques. The advantages of this method are: 1. the use of single specimens on small corks and of a large wire loop, allows the experimenter to avoid the blemishes in the membrane; 2. the surfactant dioctyl sodium sulphosuccinate is added to diluted ILford L4, thus greatly prolonging the period of time over which good emulsion layers can be made; 3. corks can be handled in perspex holder which allows about 20 specimens to be developed simultaneously. The steps of the method comprise: 1. Cut ribbons of ultrathin sections of silver interference colour 2. Pick them up on formvar-coated 200 mesh grids 3. Prestaining of tissues 4. Coat the specimens with a thin layer of carbon by evaporation (30-60A) 5. Mount the specimens on corks (about 1cm apical diameter) using double-sided scotch tape 6. Emulsion coating; a. Take a 250m1 beaker, place it on the pan of a sliding weight balance and weigh it. Add 10 grams extra to the beam. Add pieces of ILford L4 emulsion to the beaker until the balance is swinging freely. Add the 20ml of distilled water that was previously measured out. b. Surfactant dioctyl sodium sulphosuccinate is added to diluted ILford L4. 7. Prepare a series of membranes of gelled emulsion with the wire loop and apply one to each cork-borne specimen. 8. Put the specimens away to expose by pushing the corks into short length of PVC tubing, each tube having a small hole in the side 9. Place the tubes in small boxes together with silica gel. 10. Exposure 11. Developer - Kodak Microdol X for 3 minutes 12. Fixer - A perspex holder can be manufactured which allows 20 specimens to be developed simultaneously. 12. Fixer - 30% sodium thiosulfate for 10 minutes 13. Examination with Siemens Elmiskop 1A electron microscope

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Controlled Formation of Surface Wrinkles and Folds on Poly (dimethylsiloxane) Substrates Using Plasma Modification Techniques

  • Nagashima, So;Hasebe, Terumitsu;Hotta, Atsushi;Suzuki, Tetsuya;Lee, Kwang-Ryeol;Moon, Myoung-Woon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.223-223
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    • 2012
  • Surface engineering plays a significant role in fabricating highly functionalized materials applicable to industrial and biomedical fields. Surface wrinkles and folds formed by ion beam or plasma treatment are buckling-induced patterns and controlled formation of those patterns has recently gained considerable attention as a way of creating well-defined surface topographies for a wide range of applications. Surface wrinkles and folds can be observed when a stiff thin layer attached to a compliant substrate undergoes compression and plasma treatment is one of the techniques that can form stiff thin layers on compliant polymeric substrates, such as poly (dimethylsiloxane) (PDMS). Here, we report two effective methods using plasma modification techniques for controlling the formation of surface wrinkles and folds on flat or patterned PDMS substrates. First, we show a method of creating wrinkled diamond-like carbon (DLC) film on grooved PDMS substrates. Grooved PDMS substrates fabricated by a molding method using a grooved master prepared by photolithography and a dry etching process were treated with argon plasma and subsequently coated with DLC film, which resulted in the formation of wrinkled DLC film aligning perpendicular to the steps of the pre-patterned ridges. The wavelength and the amplitude of the wrinkled DLC film exhibited variation in the submicron- to micron-scale range according to the duration of argon plasma pre-treatment. Second, we present a method for controlled formation of folds on flat PDMS substrates treated with oxygen plasma under large compressive strains. Flat PDMS substrates were strained uniaxially and then treated with oxygen plasma, resulting in the formation of surface wrinkles at smaller strain levels, which evolved into surface folds at larger strain levels. Our results demonstrate that we can control the formation and evolution of surface folds simply by controlling the pre-strain applied to the substrates and/or the duration of oxygen plasma treatment.

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Non-destructive Analysis on the Chemical Properties of Glass Beads (비파괴 분석을 통한 유리구슬의 화학적 특성 연구)

  • Park, Jae Hyung;Chung, Kwang Yong;Cho, Sun Heum
    • 보존과학연구
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    • s.35
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    • pp.5-23
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    • 2014
  • The possibility of non-destructive inspection glass beads for verification. Conduct a comparative analysis of the Chungcheong area with glass beads excavated Age-specific characteristics of the glass beads shall be classified by region. Trace amounts of ingredients such as CaO, $Al_2O_3$ (stabilizer), MgO, the difference is negligible. $SiO_2$ (subjects), $Na_2O$ (flux) analysis and the difference between the values was greater than in the other ingredients. Composition differences occurred rough surface to a non-uniform cross-section analysis is considered. Minimize the error value, such as the surface of carbon-coated Study, there are additional requirements. Produced at the time of the social and cultural characteristics of ancient glass and important archaeological materials, and to inform the process of cultural exchange between each region in the production of glass technology era according to the level of science and technology, arts and crafts, can be identified.

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Synthesis of Organic Radical Copolymers Based on Polystyrene and Their Performance for Batteries (폴리스티렌 기반 유기 라디칼 공중합체의 합성과 전지특성)

  • Yang, Eui-Seok;Ryu, Sang-Woog
    • Journal of the Korean Electrochemical Society
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    • v.19 no.4
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    • pp.141-147
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    • 2016
  • In this study, homo and copolymers of 2,2,6,6-tetramethyl-4-piperidyl methacrylate(TMA) and synthesized styrene derivative, 2,2,6,6-tetramethylpiperidine-4-vinylbenzyl ether(TVBE) were obtained by radical polymerization and oxidized to produce corresponding polymer radicals. The polymer radicals were mixed with carbon black, binders and coated onto Al current collector. The battery performance is then characterized by fabricating coin cells. As results, the polystyrene based organic radicals show lower oxidize efficiency and discharge capacity than methacrylate based one. However, the former shows better capacities from discharge experiments performed at $60^{\circ}C$ which suggests a possible way to overcome the high temperature fade out of performance in usual organic radical batteries. Also as expected, an excellent C-rate performance is observed in all the cells consisted of organic polymer radicals.

High Pressure X-ray Diffraction Study of LiFePO4/C-olivine-like Phase (LiFePO4/C-유사 감람석 결정구조에 대한 고압 X-선회절연구)

  • Hwang, Gil-Chan;Kim, Young-Ho
    • Journal of the Mineralogical Society of Korea
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    • v.26 no.1
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    • pp.35-44
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    • 2013
  • Synthetic carbon-coated olivine-like structured lithium iron phosphate ($Li^+Fe^{2+}(PO_4)^{3-}/C$) powder composites were compressed up to 35.0 GPa in the symmetrical diamond anvil cell at room temperature. Bulk modulus of $LiFePO_4/C$ was determined to be $130.1{\pm}10.3$ GPa. New peak appears at the d-spacing of 3.386 ${\AA}$ above 18 GPa, and another new one at 2.854 ${\AA}$ around 35 GPa. The crystallographic symmetry of the sample (i.e. orthorhombic) is apparently retained up to 35 GPa as no clear evidence for the phase transition into spinel structure has been observed. The pressure-induced volume change in the M1 site ($Li^+O_6$) is more significant than those in M2($Fe^{2+}O_6$) and $PO_4$ tetrahedral sites.