• 열처리공학회지
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• 제12권1호
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• pp.21-30
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• 1999

The present study were investigated changes of precipitation behaviour of laves phase in ferrite single phase and ferrite-martensite dual phase and precipitation of laves phase under stress. Hardness changes in ferrite phase appeared two hardness peaks by precipitation of initial fine precipitator and laves phase in 3Mo-0.3Si and 3Mo-0.3Si-C specimens, respectively. Hardness changes in martensite phase of 3Mo-0.3Si-C specimen was lower in the initial stage of aging by carbide precipitation and after this, increased by re-hardening due to precipitation of laves phase. In the ferrite phase, laves phase was mainly precipitated, whereas in the martensite phase, carbide was preferentially formed during the initial stage of aging and with increasing aging time, laves phase and carbide were simultaneously precipitated by precipitation of laves phase at around carbide. In the ferrite-martensite interface, laves phase was mainly precipitated and carbide was mainly formed at boundary of lath martensite than grain boundary. Adding the stress in aging, fine precipitator of inital precipitation of laves phase precipitated in (100) of perpendicular to tensile direction and has grown to only followed<010>direction and also, volume fraction of laves phase increased. Consequently, the stress added was accelerated initial precipitation of laves phase.

• 열처리공학회지
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• 제12권3호
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• pp.206-214
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• 1999

The effect of cooling rate on carbide precipitation during quenching of austenitic manganese steel was investigated by optical microscopy, image analyzer and numerical analysis. A computer program based on the finite difference method for analyzing heat treatment processes was developed in order to evaluate cooling rates and the possibility of carbide precipitation during quenching. The area ratio of carbide precipitated in the austenite matrix was measured by the image analyzer, and used to determine the critical point of carbide precipitation. Temperature-dependent critical cooling rates at the critical points were calculated using the present simulation program, The calculated results showed a good agreement with the experimental ones.

• 동력기계공학회지
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• 제5권1호
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• pp.97-103
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• 2001

The present study was investigated changes of precipitation behaviour of laves phase in ferrite single phase and ferrite-martensite dual phase and the mechanical properties of 10%Cr ferritic alloys. In the ferrite phase, laves phase was mainly precipitated, whereas in the martensite phase, carbide was preferentially formed during the initial stage of aging and with increasing aging time. Laves phase and carbide were simultaneously precipitated by precipitation of laves phase at around carbide. Strength and toughness were lowered by the disk-type precipitator in the initial stage of aging and toughness was recovered with increasing of aging time and then, decreasing by precipitation of laves phase.

• 열처리공학회지
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• 제9권3호
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• pp.205-211
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• 1996

Structural studies have been performed on precipitation hardening discovered in $Ll_2$-ordered $Ni_3$(Al,Cr) containing 0.2 and 0.5 mol% of carbon in terms of transmission electron microscopy(TEM). By aging at temperatures around 1073 K after solution treatment at 1423 K, fine polyhedral precipitates appear firstly on the dislocations and then in the matrix. The selected area electron diffraction (SAED) studies revealed that these particles are a $M_{23}C_6$ type carbide which has the cube-cube orientation relationship with the matrix lattice. Weak-beam electron microscopy observations of deformation induced dislocations suggested that the dislocations bypass the carbide particles during deformation.

• Geomechanics and Engineering
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• 제29권1호
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• pp.79-90
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• 2022

Soybean-urease induced carbonate precipitation (EICP), as an alternative to microbially induced carbonate precipitation (MICP), was employed for soil improvement. Meanwhile, soluble calcium produced from industrial waste carbide slag powder (CSP) via the acid dissolution method was used for the EICP process. The ratio of CSP to the acetic acid solution was optimized to obtain a desirable calcium concentration with an appropriate pH. The calcium solution was then used for the sand columns test, and the engineering properties of the EICP-treated sand, including unconfined compressive strength, permeability, and calcium carbonate content, were evaluated. Results showed that the properties of the biocemented sand using the CSP derived calcium solution were comparable to those using the reagent grade CaCl₂. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) analyses revealed that spherical vaterite crystals were mainly formed when the CSP-derived calcium solution was used. In contrast, spherical calcite crystals were primarily formed as the reagent grade CaCl₂ was used. This study highlighted that it was effective and sustainable to use soluble calcium produced from CSP for the EICP process.

• 소성∙가공
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• 제17권7호
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• pp.507-510
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• 2008

Effect of V addition on the precipitation behavior and strength of Fe-36Ni based high strength Invar alloy for power transmission wire was investigated. Fe-36Ni Invar alloy plates were fabricated using conventional ingot casting followed by hot rolling. High strength can be obtained through precipitation hardening and strain hardening by cold rolling. Simulation using FactSage$^{(R)}$ revealed that equilibrium phases which can be formed are two kinds of MC-type precipitates, $Mo_{2}C$ and $M_{23}C_6$ carbide. The latter stoichiometric carbide was expected to be formed at relatively lower temperature of $800^{\circ}C$.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2008년도 춘계학술대회 논문집
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• pp.547-550
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• 2008

Precipitation characteristics of the Fe-36Ni based high strength Invar alloy for power transmission wire was investigated in this study. High strength can be obtained in this alloy through precipitation hardening and strain hardening by cold working. $FactSage{(R)}$ in this study, revealing that equilibrium phases which can be formed are two kind of MC-type precipitates and MoC carbide. The latter stoichiometric carbide was expected to be formed at relatively lower temperature $770^{\circ}C$. High strength above 1000MPa and 40% of elongation were obtained at room temperature in both cases.

• The Korean Journal of Ceramics
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• 제3권4호
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• pp.229-234
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• 1997

Silicon carbide-carbon fiber composites have been prepared by partially Infiltrating porous carbon fiber composites with liquid silicon at a reaction temperature of $1670^{\circ}C$. Reaction between molten silicon and the fiber preform yielded silicon carbide-carbon fiber composites composed of aggregates of loosely bonded SiC crystallites of about 10$\mu\textrm{m}$ in size and preserved the appearance of a fiber. In addition, the SiC/C fiber composites had carbon fibers coated with a dense layer consisted of SiC particles of sizes smaller than 1$\mu\textrm{m}$. The physical and mechanical properties of SiC/C fiber composites were discussed in terms of infiltrated pore volume fraction of carbon preform occupied by liquid silicon at the beginning of reaction. Lower bending strength of the SiC/C fiber composites which had a heterogeneous structure in nature, was attributed to the disruption of geometric configuration of the original carbon fiber preform and the formation of the fibrous aggregates of the loosely bonded coarse SiC particles produced by solution-precipitation mechanism.

• 열처리공학회지
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• 제3권4호
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• pp.10-22
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• 1990

A study has been investigated on the effect of mechanical properties (tension strength, rotary bending fatigue strength, wear resistance, hardness) according to the carbide particle size variation by the treatment of 1) quenching tempering, and 2) quenching, subzero treatment and tempering. The material used in this investigation was a typical bearing steel, high C high Cr, AISI E 52100. The result obtained in this study were as follows : (1) Finer the carbide particle size increasing the hardness and retained austenite in same quenching condition. (2) Finer the carbide particle size reduced the tension and rotary bending fatigue which were resulted from austenite grain growth and carbide precipitation on grain boundry that induced by carbide refine heat treatment. (3) Finer the carbide particel size increasing the wear resistance which were resulted by uniform distribution of carbide and increased hardness induced by microstructural uniform hardenability of matrix. (4) When the carbide particles were refinded, subzero treatment is effective only wear resistance and hardness.

• 한국원자력학회:학술대회논문집
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• 한국원자력학회 1999년도 추계학술발표회요약집
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• pp.230.2-230
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• 1999