• Title/Summary/Keyword: Capillary effect

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Determinaton of Chloride Ion Captured into Strong NaOH Solution from Chimney by Capillary Electrophoresis (모세관 전지영동법에 의한 굴뚝에서 포집된 NaOH 용액속의 염소이온의 측정)

  • 임인덕;성용익;김양선;임흥빈
    • Journal of Korean Society for Atmospheric Environment
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    • v.15 no.3
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    • pp.327-333
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    • 1999
  • Determination of chloride ion in concentrated NaOH solution by capillary electrophoresis has been studied. The analysis was performed by indirect UV absorption detection using chromate buffer at 254nm. The matrix effect of the sample has been observed so that the sensitivity in strong NaOH solutaion has decreased up to 10% of that in distilled water. The pH effect of the sample on the sensitivity of CE peaks has been investigated. The method for increasing the sensitivity have been investigated and the optimum pH and concentration of the buffer were 7.5 and 10mM, respectively. A cationic surfactant cetyltrimethylammonium bromide(CTAB), was added to a buffer solution in order to reverse the electroosmotic flow(EOF) in the capillary. This results in a short analysis time and better peak shapes. Using this optimum condition, the determination of chloride ion in real environmental sample has been performed, which is captured in strong NaOH absorbent prepared for absorbing gas from chimney. The standard addition method has been applied for the quantitative analysis, and it was obtained the good reproducibility.

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Flow Characteristics of Neutrally Buoyant Particles in 2-Dimensional Poiseuille Flow through Circular Capillaries

  • Kim, Young-Won;Jin, Song-Wan;Yoo, Jung-Yul
    • 한국가시화정보학회:학술대회논문집
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    • 2006.12a
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    • pp.7-10
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    • 2006
  • An experimental study has been conducted to quantitatively characterize the motion of neutrally buoyant particles in 2-dimensional Poiseuille flow through the micron-sized circular capillaries in the range of Re (Reynolds number) $\approx0.1\sim100$. $A{\mu}-PTV$ (Particle Tracking Velocimetry) system is adopted, which consists of a double-headed Nd:YAG laser, an epi-fluorescence microscope and a cooled CCD camera. Since high shear rate can be induced due to the scale effect even at low Re, it is shown that in micro scale neutrally buoyant particles in Poiseuille flow drift away from the wall and away from the center of the capillary. Consequently, particles accumulate at the equilibrium position of $0.52\sim0.64R$ with R being the radius of the capillary, which is analogous to that of tube flow in macro scale. There is a plateau in equilibrium position at small Re, while equilibrium position starts increasing at $Re\approx30$. The outermost edge of particle cluster is closer to the center of the capillary than that in previous studies due to low Re effect. The present study quantitatively presents characteristics of particle motion in circular capillaries. Furthermore, it is expected to give optimum factors for designing microfluidic systems that are to be used fur plasma separation from the blood.

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A study of Improvement of tip surface at rotator capillary using transmit effect of ultarasonic vibration energy (회전체의 초음파에너지 전달에 의한 캐피러리 조도면 개선에 관한 연구)

  • Byun Kyoung-Won;Youn Hee-Sang
    • Proceedings of the Acoustical Society of Korea Conference
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    • autumn
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    • pp.261-264
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    • 1999
  • 캐피러리(Capillary)는 반도체 납땜에 사용되는 헤더 부분으로써 현재까지는 강철핀에 다이아몬드를 부착하여 가공하였으나 가공정밀도에서 매우 불량하였다. 본 논문에서는 스핀들, 콜렉트, 척부분을 변경하여 초음파에너지를 가할 수 있도록 하였으며 특히, 주파수추종방법을 이용한 발진부 제어를 통해 부하단의 변화에도 대처할 수 있도록 하였으며 캐피러리(Capillary)의 가공을 최적화 하기 위해 혼과 진동자의 무게를 이용할 수 있도록 설계하였다. 본 방법을 사용하여 실험한 결과 캐피러리(Capillary) 조도면은 우수한 특성을 나타냈음을 확인했으며 현장에서 직접 사용할 수 있는 시스템을 제시하였다.

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An Experimental Investigation on the Variation of Heating Performance Due to the Refrigerant Flow Control in a Variable-Speed Heat Pump (가변속 열펌프의 냉매 유량제어에 의한 난방성능 변화에 관한 실험적 연구)

  • 김봉훈
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.13 no.8
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    • pp.746-756
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    • 2001
  • An experimental study was conducted to investigated the effect of refrigerant flow control on the performance of a variable-speed heat pump operating in both cooling and heating mode. For this purpose, cooling and heating capacity, EER and refrigerant mass flow rate corresponding to an electronic valve as well as a capillary tube were measured as functions of compressor speed, length of capillary tube (or valve opening of the electronic valve), refrigerant charge, and outdoor temperature. From the comparison of experimental results, it was found that the performance variation due to the electronic valve opening became significant as the operating conditions(outdoor temperature and compressor speed) deviated from the standard condition at which heating capacity and EER were rated for the indicated capillary tube.

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Analysis of Unsaturated Flow Considering Hysteresis in Porous Media under Antecedent Rainfall (선행강우가 존재하는 다공성 매질에서 이력현상을 고려한 비포화 흐름 해석)

  • Park, Chang Kun;Sonu, Jung Ho
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.14 no.5
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    • pp.1137-1143
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    • 1994
  • Through the numerical analysis of the capillary pressure-based Richards equation with and without the effect of the capillary hysteresis under the boundary condition having an antecedent rainfall. the moving tendency of the wetting front, the redistribution of the moisture content, infiltration rate, cumulative infiltration etc, were computed. The effect of the capillary hysteresis cannot be neglected in analyzing an unsaturated flow, and the more accurate results may be obtained by the consideration of the hysteresis effect. If the effect of the hysteresis cannot be considered, the analysis by the use of the main wetting curve may give more reliable result than that of the main drying curve.

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Experimental Analysis of the Effect of Phase Change at the Entrance of a Capillary Tube by Sub-cooling Control on Refrigerant-induced Noise (과냉도에 따른 모세관 입구단에서의 냉매 상태 변화가 냉장고 냉매 소음에 미치는 영향의 실험적 분석)

  • Oh, Young-Hoo;Kim, Min-Seong;Han, Hyung-Suk;Kim, Tae-Hoon;Jeong, Weui-Bong
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.22 no.12
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    • pp.1184-1190
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    • 2012
  • This study is focused on the experimental analysis of the noise induced by phase change of refrigerant at the entrance of capillary tube. The refrigerant is usually two-phase condition when it flowed into the capillary tube. At the entrance of capillary tube, the phase condition of refrigerant is formed by sub-cool control. If it has sufficient sub-cool temperature, all of the vapor refrigerants turned to liquid, which means there is only liquid. Otherwise, the gas is coexisted. Based on this theory, we experiment on each case by changing sub-cool temperature using refrigerant-supplying equipment. The noise level is measured for each case and compared.

Determination of Total Phenols in Environmental Waters by Capillary-HPLC with U.S.E.P.A. Classified Eleven Priority Pollutant Phenols after Nitrosation and Their Visible Spectrophotometric Detection

  • Chung, Yong-Soon
    • Bulletin of the Korean Chemical Society
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    • v.26 no.2
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    • pp.297-302
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    • 2005
  • The determination of total phenols was accomplished by capillary-high performance liquid chromatography (capillary-HPLC) after nitrosation of the U.S.E.P.A. classified 11 priority pollutant phenols, using the nitrosated parent phenol (POHNO) as a reference for calibration. The optimum mobile phase composition for this analysis was found by examining the effect of changing the percentage of acetonitrile (MeCN) in the mobile phase on retention factors (k values) and peak intensities. As MeCN percentage was increased, k values were reduced and peak intensities were generally increased. From the results obtained, it was found that the optimum mobile phase was 90%(v/v) MeCN solution at pH 8.0, the detection wavelength of 400 nm, and a detection limit (D.L., concentration at signal to noise ratio (S/N) of 3.0) of 4.5 ${\times}$ $10^{-7}$ M. In addition, 10 of the 11 phenols present in mineral or waste water were separated after the nitrosation by capillary-HPLC. The optimum mobile phase for separation was a 40%(v/v) MeCN solution at pH 5.0.

Geometry Effects of Capillary on the Evaporation from the Meniscus (모세관 단면 형상에 따른 계면 및 증발 특성)

  • Choi, Choong-Hyo;Jin, Songwan;Yoo, Jung-Yul
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.31 no.4
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    • pp.313-319
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    • 2007
  • The effect of capillary cross-section geometry on evaporation is investigated in terms of the meniscus shape, evaporation rate and evaporation-induced flow for circular, square and rectangular cross-sectional capillaries. The shapes of water and ethanol menisci are not much different from each other in square and rectangular capillaries even though the surface tension of water is much larger than that of ethanol. On the other hand, the shapes of water and ethanol menisci are very different from each other in circular capillary. The averaged evaporation fluxes in circular and rectangular capillaries are measured by tracking the meniscus position. At a given position, the averaged evaporation flux in rectangular capillaries is much larger than that in circular capillary with comparable hydraulic diameter. The flow near the evaporating meniscus is also measured using micro-PIV, so that the rotating vortex motion is observed near the evaporating ethanol and methanol menisci except for the case of methanol meniscus in rectangular capillary. This difference is considered to be due to the existence of corner menisci at the four comers.

Fabrication of Microstructures with Nanocomposites by Capillary Effect (모세관법을 이용한 나노 복합재료 마이크로 구조 제작)

  • Han, Soo-Ho;Hwang, Hui-Yun
    • Composites Research
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    • v.31 no.4
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    • pp.171-176
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    • 2018
  • We proposed new and easy fabrication method of micro-nano hierarchical structures for synthetic dry adhesives and conducted feasibility tests of alignment characteristics of nano-materials in the microstructures by capillary effect. Candidates of fabrication conditions were selected based on the degree of cure and viscosity of mixtures of multiwall carbon nanotubes (MWCNTs) and polydimethylsiloxane (PDMS), which were measured with respect to the fabrication conditions. Scanning electron microscopy images of cross sections of MWCNT-PDMS microstructures were analyzed. MWCNT alignment in microstructures was better when fabrication temperature and degree of cure at fabricating start were lower, but areal density of MWCNTs was little affected by fabrication conditions.

?Experimental Study on the Effects of Zanthoxyli Fructus and Fagarae mandshuricae Fructus (천초(川椒) 및 산초(山椒)의 효능(?能)에 관(關)한 실험적(實驗的) 연구(硏究))

  • O, Han-Gyun;Won, Jong-Hun;Jeong, Gyu-Man
    • The Journal of Pediatrics of Korean Medicine
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    • v.4 no.1
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    • pp.1-17
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    • 1990
  • ?In order to investigate effects of Zanthoxyli Fructus (Sample-A) and Fagarae mandshuricae Fructus (Sample-B), experimental study was performed through observation on isolated - ileum analgesic, hypothermal, anti-pyretic, anti-inflammatory, capillary permeability, blood flow rate, blood pressure and respiratory works. The results were as follows; 1. In spontaneous movement of mice isolated-ileum, both samples were noted to have strong inhibitory action after temporary contraction, and to show antagonism against acetylcholine chloride and barium chloride. 2. Both samples were showed to have antihistamin work on guinea pig isolated-ileum 3. In analgesic work by the acetic acid method, only Fagarae mandshuricae Fructus was proved to have significant analgesic effect in mice. 4. Both sample groups indicated anti-pyretic and anti-inflammatory effect. 5. Both samples were noted to have inhibitory effect against capillary permeability ?rise in mice. ?6. Both samples were noted to have dose-dependent falling effect on blood pressure in rabbits.

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