• Title/Summary/Keyword: Ca extraction

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Studies with $P^{32}$ Tracer on Laboratory Index of Available Phosphorus in Paddy Soil, Korea (II) ($P^{32}$ 추적자법(追跡子法)에 의(依)한 토양(土壤)의 유효인산정량법(有動燐畿定量法)에 관(關)한 연구(硏究) (II))

  • Lee, C.Y.;Park, Hoon
    • Applied Biological Chemistry
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    • v.13 no.1
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    • pp.73-79
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    • 1970
  • The present study has been undertaken to see if any proper measure be found for the determination of available phosphorus by chemical extraction on the basis of A-values as the standard. The results obtained are described as follows. 1. Since A-value of the samples under study showed a significant correlation with Fe-P at 1% level. The available phosphorus in the present paddy soils was considered to be affected by Fe-P. 2. Six methods for chemical extraction were not correlated with the determination of Fe-P, proving them inadequate for the quantitative measurement of available phosphorus. 3. Adequate method for extracting available phosphorus in paddy soils should rest on the measurement of the reduction intensity of Fe-P. The extractable intensity was estimated to be 270 ppm in average. 4. Bray No. 2-P showed significant correlation with Lancaster-P, Spurway-P, Truog-P, and (Ca+Al)-P at 5% level. Olsen-P and Lancaster-P indicated significant correlation with Al-P and Spurway-P with Ca-P respectively at 1% level.

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A Study on the Free Amino Acid and Minerals of Chicken Bone Extracts by Boiling time (가열시간에 따른 닭뼈용출액 중의 유리아미노산과 무기질에 관한 연구)

  • 박희옥;이혜정
    • Korean journal of food and cookery science
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    • v.11 no.3
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    • pp.244-248
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    • 1995
  • This study was carried out to investigate the free amino acid content, the free amino-nitrogen content and minerals such as Ca, P and Fe of chicken bone stock. The results were as follows. 1. In chicken bone stock, glutamic acid was the most abundant amino acid, Iysine, alanine, cysteine and glycine were followed oderly and these free amino acids seemed to be the most intensive flavor compounds. 2. The free amino acid-nitrogen content of chicken bone stock was increased after 3 hours boiling and began to decrease after 4 hours boiling. 3. After 3 hours boiling, Ca, P were 5.0 mg/100 g chicken bone and 42.5 mg/100 g chicken bone, respectively and began to decrease after 4 hours boiling. The ratio of Ca:P was about 7.8. Fe was increased after 4 hours boiling and began to decrease after 5 hours boiling. These results revealed the low effectiveness of Ca, P and Fe utilization of chicken bone stock, because of the very low extraction of minerals. But these results revealed the significant correlation of free amino acid, free amino-nitrogen contents and brothy flavor. So chicken bone stock on heating at 90-95$^{\circ}C$ for 3∼4 hours seemed to be the most intensive brothy flavor.

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Effects of Salts, pH, Acidulants and Carbohydrolase on Extraction Yield and Color Change of Garlic (염류 및 pH, Acidulants, 다당류 분해효소가 마늘 추출 수율 및 변색에 미치는 영향)

  • Cho, Jin-Sook;Kim, Dong-Hee;Kim, Woo-Jung
    • Korean Journal of Food Science and Technology
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    • v.31 no.5
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    • pp.1211-1215
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    • 1999
  • The solid yields and color changes of garlic aqueous extracts were determined to study the effects of enzymatic hydrolysis, pH treatment, and addition of organic acids and some organic or inorganic salts. Hydrolysis with commercial polysaccharases resulted in an $15{\sim}20%$ increase in the solid yields, with a greenish color change in the garlic extracts. pH treatment gave it similar effect at the pH range of $4.4{\sim}5.0$. Among the salts and acidulants used, $CaCl_2$, sodium oxalate, tartaric and phosphoric acids were effective for increase in the yield and $K_{4}P_{2}O_{7}$ was effective for both yield increase and control of greening.

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Alveolar socket preservation with demineralised bovine bone mineral and a collagen matrix

  • Maiorana, Carlo;Poli, Pier Paolo;Deflorian, Matteo;Testori, Tiziano;Mandelli, Federico;Nagursky, Heiner;Vinci, Raffaele
    • Journal of Periodontal and Implant Science
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    • v.47 no.4
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    • pp.194-210
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    • 2017
  • Purpose: The aim of the present study was to evaluate the healing of post-extraction sockets following alveolar ridge preservation clinically, radiologically, and histologically. Methods: Overall, 7 extraction sockets in 7 patients were grafted with demineralised bovine bone mineral and covered with a porcine-derived non-crosslinked collagen matrix (CM). Soft tissue healing was clinically evaluated on the basis of a specific healing index. Horizontal and vertical ridge dimensional changes were assessed clinically and radiographically at baseline and 6 months after implant placement. For histological and histomorphometric analysis, bone biopsies were harvested from the augmented sites during implant surgery 6 months after the socket preservation procedure. Results: Clinically, healing proceeded uneventfully in all the sockets. A trend towards reduced horizontal and vertical socket dimensions was observed from baseline to the final examination. The mean width and height of resorption were 1.21 mm (P=0.005) and 0.46 mm (P=0.004), respectively. Histologically, residual xenograft particles ($31.97%{\pm}3.52%$) were surrounded by either newly formed bone ($16.02%{\pm}7.06%$) or connective tissue ($50.67%{\pm}8.42%$) without fibrous encapsulation. The CM underwent a physiological substitution process in favour of well-vascularised collagen-rich connective tissue. Conclusions: Socket preservation using demineralised bovine bone mineral in combination with CM provided stable dimensional changes of the alveolar ridge associated with good reepithelialisation of the soft tissues during a 6-month healing period.

Feasibility Test for Phytoremediation of Heavy Metals-Contaminated Soils using Various Stabilizers (중금속 오염토양에 대한 안정화 및 식물상 정화공법의 동시 적용연구)

  • Jeon, Jongwon;Bae, Bumhan;Kim, Younghun
    • Journal of the Korean GEO-environmental Society
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    • v.13 no.3
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    • pp.59-70
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    • 2012
  • In this study, to select the best stabilizer for the heavy metals-contaminated soil from a smelter area during phytoremediation, a plant uptake experiment and a soil stabilization were simultaneously applied using Pteris multifida Poir. and five pre-screened stabilizers(zeolite, Mn dioxide, slag, Ca oxide, and magnetite). The extracted heavy metal was measured and compared using a 3 step sequential extraction for the soil samples. The growth rate of the plant was also evaluated. The stabilizers stabilized heavy metals in soil and reduced the extraction rate. Magnetite and calcium oxide showed better results than other stabilizers. The stabilizers enhanced the growth of the plant. All the heavy metals except for arsenic were concentrated in roots while arsenic was concentrated in leaves of the plant. It is concluded that the stabilizers can minimize the heavy metal release from the contaminated soil during phytoremediation and stimulated the growth of plant. These effects of stabilizers could compensate for some weak points of phytoremediation such as reaching of heavy metals by rainwater.

Identification of the Antibiotic-Producing Chstridium sp. KH-431 and Purification of the Antibiotics (항생물질을 생산하는 Clostridium sp. KH-431의 동정 및 항생물질의 정제)

  • 홍수형;김미정;박용복;이재근;하지홍
    • Microbiology and Biotechnology Letters
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    • v.21 no.1
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    • pp.41-46
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    • 1993
  • A strain showing antibiotic activities against various bacteria and fungi was selected from approximately 2,000 microorganisms obtained from soil samples. This strain, designated as KH-431, was identified as a Clostridium sp. by its morphological, physiological and biochemical characteristics. The highest production of the antibiotics was achieved in a fermentation medium containing sorbitol, yeast extract, d-biotin and $CaCl_2$ The antibiotics were isolated from the culture broth by solvent extraction using ethyl acetate, silica gel column chromatography and recrystallization. Two kinds of antibiotics, KG-431A and KG-431B were obtained after the purification procedure, and only KG-431B was successful to recrystallize.

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A Study on Leaching of Vanadium and Nickel from Incineration Ash of Heavy Oil Fly Ash (중유회 소각재로부터 바나듐, 니켈 침출에 관한 기초적 연구)

  • 유연태;김병규;박경호;홍성웅
    • Resources Recycling
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    • v.4 no.3
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    • pp.32-39
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    • 1995
  • Thc purpose of this study is to develop the efficient process for recovering vanadium and nickel from the incineralionash of the oil fly ash. In this paper, the physical and chemical properties of the incineration ash was examined, and theleaching characteristics of the incineration ash were investigated by water leaching and sulEuric acid leaching tcsls. The incinerationash of oil fly ash was mainly consisted of oxldes such as V,09, V,O,, NaVO,, Ni,(VO,)Z, Fe,O,, CaSO,, SiO,.Thc waler leaching showed low extraction of metallic components, while the sulfunc acid lcaching with high temperahlreand pressure increased the extraction of vanadium and nickcl considerably. For instance, the exlraction rates of the metalllccomponents on the sulfuric acid leaching were 99% for V and 45% for Ni at 90$^{\circ}$C with pH 0.5 H,SO,, and were86% for V and 75% far Ni at ZOO"C(64 psi) with pH 1.0 H-SO,. with pH 1.0 H-SO,.

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Melting of PCB scrap for the Extraction of Metallic Components (PCB스크랩으로부터 유가금속성분 회수를 위한 용융처리)

  • Kwon Eui-Hyuk;Jang Sung-Hwan;Han Jeong-Whan;Kim Byung-Su;Jeong Jin-Ki;Lee Jae-Chun
    • Korean Journal of Materials Research
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    • v.15 no.1
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    • pp.31-36
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    • 2005
  • It is well known that PCB (Printed Circuit Board) is a complex mixture of various metals mixed with various types of plastics and ceramics. In this study, high temperature pyre-metallurgical process was investigated to extract valuable metallic components from the PCB scrap. For this purpose, PCB scrap was shredded and oxidized to remove plastic materials, and then, quantitative analyses were made. After the oxidation of the PCB scrap, $30.6wt\%SiO_2,\;19.3wt\%Al_2O_3\;and\;14wt{\%}CaO$ were analyzed as major oxides, and thereafter, a typical composition of $32wt\%SiO_2-20wt\%Al_2O_3-38wt{\%}CaO-10wt\%MgO$ was chosen as a basic slag system for the separation of metallic components. Moreover a size effect of crushed PCB scrap was also investigated. During experiments a high frequency induction furnace was used to melt and separate metallic components. As a result, it was found that the size of oxidized PCB scrap was needed to be less 0.9 m to make a homogeneous liquid slag and to recycle metallic components over $95\%$.

About Chromium (VI) Extraction from Fertilizers and Soils

  • Sager Manfred
    • Economic and Environmental Geology
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    • v.38 no.6 s.175
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    • pp.657-662
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    • 2005
  • Extractions fro fertilizer and soil samples were performed to yield the operationally defined fractions 'soluble' chromate (extractable with $NH_4NO_3$), 'exchangeable' chromate (extractable with phosphate buffer pH 7.2), and these results were compared with the data obtained by extractions with ammonium sulfate, borate buffer pH 7.2, saturated borax pH 9.6, and polyphosphate (Graham's salt). In order to maintain the pH of extractant solution about constant, the concentration of extractant buffer had to be raised to at least 0.5 M. The results strongly depended on the kind of extractant, and the solid: liquid ratio. For most of the samples investigated, the extraction efficiency increased in the order borate-sulfate-nitrate-phosphate. Whereas the recovery of $K_2CrO_4\;and\;CaCrO_4$ added to the samples of basic slags prior to the extraction was about complete, the recovery of added $PbCrO_4$ was highly variable. In soil extracts, the color reaction was interfered from co-extracted humics, which react with the chromate in weak acid solution during the time period necessary for color reaction (1 hour). However, this problem can be overcome by standard addition and subtraction of the color of the extractant solution. In soil extract of about pH < 7, organic material reduced chromate during the extraction period also, and standard addition of soluble chromate is recommended to prove recovery and the stability of chromate in the samples. In admixtures of soils and basic slags, results for hexavalent chromium were lower than from the mere basic slags. This effect was more pronounced in phosphate than in nitrate extracts. As a proficiency test, samples low in organic carbon from contaminated sites in Hungary were tested. The results from $NH_4NO_3$ extracts satisfactorily matched the results of the Hungarian labs obtained from $CalCl_2$ extractants.

Quantitative Analysis about Phenolic Compounds of Dendranthema Species in Korean Native Plants (국내 자생 구절초속 중 페놀화합물 함량분석)

  • Kim, Kyeong Mi;Lee, Seon Yu;Jo, Ara;Kang, Byoung Man;Ham, Seongho;Cho, Junghee;Lee, Gukyeo
    • Korean Journal of Pharmacognosy
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    • v.48 no.1
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    • pp.70-76
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    • 2017
  • Dendranthema spp are distributed in various regions in Korea. This report is the quantitative results of phenolic compounds on the 5 resources collected from all over the country. It was known that it has phenolic compounds, as an anticoagulant activities and immunoadjuvant activity of contribute to the cardiovascular effects. This was used for quantitative analysis of chlorogenic acid(CA), 3,5-Dicaffeoylquinic acid(3,5-DCA), 4,5-Dicaffeoylquinic acid(4,5-DCA) and linarin, with UPLC-PDA and LC-IT-TOF-MS. Extraction efficiency of compounds was compared by using ultrasonic extraction and reflux extraction with different extraction conditions (methods and time). In 50% MeOH extracs (30 mins) of Dendranthema zawadskii (Herb.) Tzvelev (SDZ), Dendranthema zawadskii var. yezoense (Maek.) Y.M.Lee & H.J.Choi (NDZ), Dendranthema zawadskii (Herb.) Tzvelev var. teuisectum (Kitag.) J. H. Pak (GDZ), Dendranthema careanum (H. $L{\acute{e}}v$. & Vaniot) Vorosch. (HDC) and Dendranthema zawadskii var. tenuisectum Kitag (PDZ), chlorogenic acid contents were 1.14‰, 6.95‰, 7.27‰, 1.47‰ and 2.64‰, 3,5-dicaffeoylquinic acid contents were 3.30‰, 5.60‰, 10.81‰, 2.67‰ and 1.50‰, 4,5-dicaffeoylquinic acid contents were 0.74‰, 1.93‰, 3.36‰, 0.61‰ and 0.43‰ and linarin contents were 3.90‰, 10.15‰, 0.15‰, 0.73‰ and 0.21‰, respectively.