• Title/Summary/Keyword: CR 분석

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Effects of GPS heat-treatment on microstructure of as-cast Co-Cr alloy (Co-Cr 주조합금의 미세구조에 미치는 GPS 열처리 효과)

  • Ryu, Jeong Ho;Lee, Ho Jun;Cho, Hyun Su;Paeng, Jong Min;Park, Jong Bum;Lee, Jung-Il
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.27 no.5
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    • pp.263-267
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    • 2017
  • The Co-Cr as-cast alloys are widely used in the manufacturing of orthopedic implants made with investment casting techniques because of its high strength, good corrosion resistance and excellent biocompatibility properties. Carbide precipitation at grain boundaries and interdendritic regions is the major strenthening mechanism in the as-cast condition. In this study, effects of GPS (Gas Pressured Sintering) heat-treatment on the microstructure and crystallinity of the as-cast Co-Cr alloy prepared by investment casting were investigated. It was confirmed that the content of metal carbide ($Cr_{23}C_6$) was increased in the grain boundary by using optical microscopy (OM), field-emission scanning electron microscopy (FE-SEM) and energy dispersive spectroscopy (EDS).

Humidity-Sensitive Characteristics of MgO and $TiO_2$ Addition on $ZnCr_2O_4$ Ceramic Thick-Film Humidity Sensors (MgO 및 $TiO_2$가 첨가된 $ZnCr_2O_4$ 세라믹 후막 습도센서의 감습 특성)

  • Yoon, Sang-Ok;Kim, Kwan-Soo;Jo, Tae-Hyun;Shim, Sang-Heung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07b
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    • pp.898-901
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    • 2004
  • [ $ZnCr_2O_4$ ]를 모물질로 하고 MgO, $TiO_2$를 몰비로 2:1, 4:1, 6:1, 및 8:1이 되게 정량적으로 조합한 후, 조사하였다. $ZnCr_2O_4$-MgO와 $ZnCr_2O_4-TiO_2$를 X-선 분석한 결과 Spinel 결정구조를 형성하였으며, 또한 SEM과 EDX 분석결과 각각 $Li_2CrO_4$$Li_3VO_4$의 형성으로 인하여 저항 특성이 나타나는 것을 알 수 있었다. $ZnCr_2O_4-MgO$, $ZnCr_2O_4-TiO_2$에서 MgO의 양이 증가할수록 저항값은 약간 감소하는 반면, $TiO_2$의 양이 증가할수록 저항값이 급격히 증가하는 특성을 나타내었고, 감습 특성에서도 M??보다 TiO2가 더 높게 나타내었다. 습에 따른 복원 특성의 경우 $700^{\circ}C$에서 소결한 ($ZnCr_2O_4:MgO=4:1$)과 ($ZnCr_2O_4:TiO_2=6:1$) 조성의 센서가 가장 양호하였다.

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Quantitative Analysis and Comparison of DR and CR image quality (CR과 DR 영상화질의 정량적 비교분석)

  • Park, Hey-Suk;Seo, Jang-Yeon;Jeong, Jin-Hwa;Lee, Chang-Lae;Cho, Hyo-Min;Kim, Hee-Joung
    • Journal of the Korean Society of Radiology
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    • v.1 no.1
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    • pp.31-37
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    • 2007
  • The purpose of this research was to compare and analyze image quality for each Detector of CR(Computed Radiography) and DR(Digital Radiography). The results showed that CR(AGFA MD 4.0 General plate, JAPAN) was superior to DR(HOLOGIC nDirect Ray, USA) based on the quantitative values and comparison of MTF(Modulation Transfer Function), NPS(Noise Power Spectrum), Photon fluence and DQE(Detective Quantum Efficiency) which have been widely accepted for the estimation of CR and DR. Quantitative evaluations of CR and DR system were obtained and they may be very helpful for QA and QC of general X-ray systems.

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Simultaneous Spectrophotometric Determination of Cr(Ⅲ) and Cr(Ⅳ) in Chromium Plating Solution via Flow-Through Analysis (흐름계를 이용한 크롬도금 용액의 Cr(Ⅲ)와 Cr(Ⅵ)의 분광학적 동시 분석 방법)

  • Kim, Sun Kwan;Nam, Hakhyun;So, Jae Chun;Lee, Won;Cha, Geun Sig;Han, Sang Hyun
    • Journal of the Korean Chemical Society
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    • v.39 no.2
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    • pp.87-93
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    • 1995
  • The amount of Cr(Ⅲ) and Cr(Ⅵ) in a chromium plating solution could be determined simultaneously within five minutes using UV/VIS spectrophotometer coupled with a flow-through analysis(FTA) setup. The λmax's at 580 nm and 440 nm which correspond to Cr(Ⅲ) and Cr(Ⅵ), respectively, well obey the Beer-Lambert law in the range over 0.05 g/L for Cr(Ⅲ) and 0.005 g/L for Cr(Ⅵ). when the pH of the sample is less than 4.0, the absorption extinction coefficients of those peaks are not much dependent on the proton concentration. The amount of Cr(Ⅲ) and Cr(Ⅵ), and the total chromium in post treatment chromium plating solution, which normally has few g/L of Cr concentration, could be easily measured using UV/VIS spectrophotometry after the sample had been diluted with sulfuric acid of pH=1.0 in the flow-through analysis setup; this method is far more convenient and faster than the common redox titration (which requires at least 40 min/sample) method, while the accuracy of the method is highly comparable to conventional titrimetric method. Since the implementation of an PTA-UV/VIS setup in any plating industry is cost effective and easy to operate, the analytic method described in this paper may be applied directly for in situ analysis of plating solutions.

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A Comparative Study on Image Quality of Breast Image Tests using ACR Phantom (ACR 팬텀을 이용한 시스템별 유방검사 영상의 비교 연구)

  • Hong, Dong-Hee;Jung, Hong-Ryang;Lim, Cheong-Hwan
    • Journal of radiological science and technology
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    • v.29 no.4
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    • pp.241-247
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    • 2006
  • Recently, interests and utilization on Computed Radiography(CR) and Digital Radiography(DR) tends to increase owing to an introduction of Picture Archiving and Communication System(PACS) and an accuracy control of special medical equipment for a breast imaging examination. This study was intended to compare and analyze a detector's imaging quality by each system to be used for the breast imaging examination by using ACR Phantom used at the accuracy control. As an evaluation method, a significance and reliability of image's value using the ACR Phantom was analyzed by using SPSS program. The results are followed. 1. For the fiber, there was 3.9 score in Screen-Film, 4.2 score in CR($50{\mu}m$), 3.2 score in CR($100{\mu}m$), and 4.2 score in DR. There was the high score in the order of CR($50{\mu}m$), DR, Screen-Film, and CR($100{\mu}m$)(P<0.05). 2. For the calcification, there was 2.7 score in Screen-Film, 2.5 score in CR($50{\mu}m$), 2.0 score in CR($100{\mu}m$), and 2.9 score in DR. There was the high score in the order of DR, Screen-Film, CR($50{\mu}m$), and CR($100{\mu}m$).(0.025(P<0.05). 3. For Mass, there was 3.8 score in Screen-Film, 3.8 score in CR($50{\mu}m$), 3.6 score in CR($100{\mu}m$), and 4.5 score in DR. There was the high score in the order of DR, CR($50{\mu}m$), Screen-Film, and CR($100{\mu}m$) (P<0.1). 4. As the total score, there was 10.4 score in Screen-Film, 10.6 score in CR($50{\mu}m$), 8.7 score in CR($100{\mu}m$), and 11.3 score in DR. There was the high score in the order of DR, $CR(50{\mu}m$), Screen-Film, and $CR(100{\mu}m$). As shown in the above results, it can be known that DR and Screen-Film System has higher image quality than CR. But, DR has unstability caused by element, and Screen-Film has the low image quality caused by artifact as disadvantages. When Dual-Side CR($50{\mu}m$) was used among CR systems which had the problem of low image quality, it was indicated that there was no difference with Screen-Film System. Because the radiation imaging examination tends to become digitalized, each system for the breast imaging examination will need to be developed and supplemented.

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A Study on the Behaviour of High Temperature Corrosion of Fe-22Cr-5Al-X(X=Zr,Y) (Fe-22Cr-5Al-X(X=Zr,Y)합금의 고온 부식거동에 관한 연구)

  • Lee, Byeong-U;Park, Heung-Il;Kim, Jung-Seon;Lee, Gwang-Hak;Kim, Heung-Sik
    • Korean Journal of Materials Research
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    • v.7 no.10
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    • pp.898-907
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    • 1997
  • Fe-22Cr-5AI-X(X=Zr, Y)합금을 1143K, 고온 황화(P$s_{2}$=1.11x$10^{-7}$atm, P$O_{s}$ =3.11x$10^{-20atm}$) 및 황화/산화 (P$s_{2}$=8.31x$10^{-8}$atm, P$O_{s}$ =3.31x$10^{-18atm}$) 환경의 복합가스 분위기에서 1-30시간동안 노출하여 합금표면에 형성된 부식층을 관찰하여 SEM/EDS로 분석하였다. Fe-22Cr-5AI합금은 고온 부식환경에서 부식 생성물의 성장은 포물선법칙을 따르고 주요 성분은 결함이 많고 다공질인 철과 크롬의 황화물[(Fe, Cr)Sx]이므로 고온 내식성이 감소하였다. Zr을 1wt%첨가한 Fe-22Cr-5AI합금의 고온 부식거동은 Y을 1wt%첨가한 합금과 비슷한 거동을 나타내었다. 황화환경에서는 Cr의 선택 황화에 의한 크롬 황화물(CrS)이 생성되고 노출시간의 경과에 따라 (Fe, Cr)Sx나 (Cr, Fe)Sx 등의 황화물의 성장으로 고온 내식성이 감소하였다. 그러나 황화/산화환경에서는 초기에는 알루미늄산화물(A $I_{2}$ $O_{3}$)및 지르코늄산화물(Zr $O_{2}$)등이 생성되어 보호적이었으나 15시간이후 부터 (Fe, Cr)Sx나 (Cr, Fe)Sx 의 황화물의 성장으로 고온 내식성이 감소하였다.

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Analysis on Character and Ability of In -Plane Permeability of Geotextiles Used for Darainage (배수용 Geotextlle의 평면투수 성능분석)

  • 이상호
    • Geotechnical Engineering
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    • v.8 no.3
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    • pp.61-74
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    • 1992
  • In order to provide fundamental data for the design of geotextile drains, the in-plane permeability coefficients were determined by tests and permeable cllaracteristics were investigated, mainly on domestic nonwoven and composite getextile products used for drainage purpose. The results obtained are as follows, The thickness, the in-plane permeability coefficient and the transmissivity with the in- crease of compressive stress are found to be remarkably decreased when the compressive stress is lass than about 10KN/m2. The inflane permeability of filament nonwovens are found to be lower than that of composites or staple-fiher nonwovens, and the compressibility of the geotextile shown to be larger for the polyester nonwovens than for the polypropylene nonwovens. The relation of compressive stress, q and compressibility, Cr is expressed as Cr=13.37 In q+23.28 and that of compressibility on the basis of 2KN /m2, Cr' and decrease ratio of in-plane permeability coefficient is followed Pr: 1.25Cr'

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Determination of Heavy Metals for Sediment Proximated to Water in Lake(II) (호소내 퇴적물의 수질오염물질 분석(II) - 중금속 -)

  • Park, Sun-Ku;Kim, Sung-Soo;Ko, Oh-Suk
    • Analytical Science and Technology
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    • v.14 no.2
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    • pp.140-146
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    • 2001
  • The study was carried out to analyze the pollutants, Fe, Cu, Cr, Zn, Cd for 3 sediments of 5 sites collected from lake in K river basin. 5cm sediment, which is nearly proximated to water from sediment of depth 30cm, showed higher Fe, Cu, Cr, Zn, Cd data than another 5-10cm and 10cm sediment, which is separated from sediment of depth 30cm. Also, 5cm sediment nearly proximated to water showed the following data: Fe, 34.9-39.8mg/L, Cu, 34.5-44.8mg/L, Cr, 68.0-79.2mg/L, Zn, 147.4-126.0mg/L, Cd, 2.2-1.0mg/L, respectively. From this results, we know the fact that the pollution degree of sediment has an effect on the water quality in like and stream.

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Environmental Assessment of $Cr^{6+}$ Occurring in Stabilizing Processes of Soft Sea-Bottom using Cement Stabilizers (시멘트 고화제 고결공법에서 발생하는 $Cr^{6+}$의 환경영향 검토)

  • 오영민;김경태
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.14 no.4
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    • pp.319-321
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    • 2002
  • Recently, the injection of cement stabilizer is used as one of ways to improve soft sea-bottom. However, this method makes an argument with $Cr^{6+}$subject to emerge to the seawater from the cement stabilizer. To investigate the amount of$Cr^{6+}$field measurements were carried out in Ochun harbor of Chunsoo Bay. The analysis shows the amount of $Cr^{6+}$in the seawater met the demand of environmental criterion.

Abrasive wear characteristics of high Cr cast iron hardfacing (고 Cr 주철계 육성용접부의 연삭(abrasion)마모 특성에 대한 연구)

  • 이형근
    • Journal of Welding and Joining
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    • v.15 no.4
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    • pp.154-165
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    • 1997
  • Abrasive wear characteristics of high Cr white cast iron-based hardfacing were investigated using the rubber wheel abrasion wear test method according with the ASTM G65-85. Mild steel was also tested for comparison with high Cr cast iron hardfacing. Wear experiments, where the applied force, wheel revolution rate and abrasive powder feed rate were selected as test valuables, were planned and analyzed by response surface method to evaluate wear statistically and quantitatively. Weight loss of high Cr cast iron hardfacing was mostly affected by the applied force and wheel revolution rate, and little by the powder feed rate. Weight loss of mild steel was greatly affected by the wheel revolution rate and powder feed rate, and slowly and steadily increased with the applied force. Abrasive wear mechanism of high Cr cast iron and mild steel was discussed in the light of the wear test results.

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