• Composites Research
• /
• v.32 no.2
• /
• pp.90-95
• /
• 2019

Sloshing impact loads on liquefied natural gas (LNG) carr iers are the main issue of damage to the insulation system in LNG cargo containment system (LNG CCS). The damage to the insulation system would be fatal in maintaining a temperature-savings environment in LNG CCS. The typical method is to enhance the insulation materials that can maintain a constant cryogenic temperature. Insulation materials consist of polyurethane foam and plywood, an adhesive for bonding these two materials. This study intends to improve the absorption energy of the material when the impact load is applied by creating a glass bubble/epoxy composite resin as part of the insulation. The experimental scenarios consider the effect of temperature ($20^{\circ}C$, $-163^{\circ}C$), glass bubble weight fraction in epoxy resin through free fall experiments. Experiments have shown that if the glass bubble additive reaches 20 wt.%, the cryogenic absorption energy is a maximum performance and that 0 wt.% has a maximum ambient absorption energy. However, the agglomeration has been occurred due to deterioration of the stirring performance if weight fraction was 20 wt.% and the result of 0 wt.% have been revealed that ambient absorption energy is significantly lower.

• Proceedings of the Korean Society For Composite Materials Conference
• /
• 2002.05a
• /
• pp.93-96
• /
• 2002

Instrumented impact tests and compression-after-impact(CAI) tests have been used to evaluate the effect of temperature on the low-velocity impact characteristics of phenolic matrix composites reinforced with various woven glass fabric. Impact characteristics and damage area in laminates are evaluated by C-scan. It is shown that the extent of damage and residual compressive strength of the laminates vary with energy level and impact test temperature. The damage area increases with increasing impact energy and temperature. All these observations indicate reduced impact damage resistance and damage tolerance of the laminates at elevated temperature.

• Journal of the Korean Society for Precision Engineering
• /
• v.18 no.4
• /
• pp.135-141
• /
• 2001

An experimental study to find the effect of processing parameters for self-healing microcapules is performed. These microcapsules can be applied to accomplish the healing of delamination damage in woven E-glass/epoxy composites. This paper introduces the self-healing concept and presents a method for solving the microcapsule size and shape. Additionally, processing parameters are varied during the formation of microcapsules and these capsules are observed through optical microscope. To obtain thermogravimetric(TG) curve for the manufactured microcapsules, TGA tests are executed. From these results, the best processing conditions for the formation of capsules are found as follows: (1) temperature of solution $ 50^{\circ}C$, (2) potential of hytdrogen(pH) 3.5ppm, and (3) agitation 500~600rpm.

• Proceedings of the KIEE Conference
• /
• 1998.11c
• /
• pp.813-815
• /
• 1998

In order to analyse the degradation process of epoxy/glass fiber for outdoor condition, FRP laminate was exposed to the wavelength of ultraviolet rays and evaluated by comparing contact angle, surface resistivity, surface potential decay, and ESCA spectrum respectively. Finally, We can conclude that the degradation phenomena on the surface of epoxy composites are dominated by the induction of ester and carboxyl groups.

• Elastomers and Composites
• /
• v.32 no.1
• /
• pp.29-36
• /
• 1997

The change of elastic modulus(E'), loss modulus(E"), and loss $tangent(tan{\delta})$ were investigated on condition of double strain amplitude (DSA) at temperature of $-40{\sim}80^{\circ}C$ for carbon black filled natural rubber. E', E", and $tan{\delta}$ were increased as it closed to the glass transition temperature due to decrease of rubber network flexibility and carbon black agglomerate interaction. In the micro strain range, energy loss showed maximum value because of the chain slippage in rubber matrix, but the regeneration of carbon black agglomerate and rubber matrix affected decrease of energy loss over the mid-range strain. As a results of regression analysis, $E'\;_{max}$ correlation with ${\Delta}E'$ $(E'\;_{0.4%DSA}-E'\;_{2.0%DSA})$ showed linear relationship.

• Proceedings of the Korea Concrete Institute Conference
• /
• 2005.11a
• /
• pp.233-237
• /
• 2005

For giving self-diagnosing capability, a method based on monitoring the changes in the electrical resistance of hybrid FRP reinforced concrete has been tested. Then after examining change in the value of electrical resistance of carbon fiber in CFRP, CFGFRP, CFAFRP and e.t.c., before and after the occurrence of cracks and fracture in hybrid FRP reinforced concrete at each flexural weight-stage, the correlations of each factors were analyzed. As the results, it is clarified that when the carbon fiber tows fracture, the electrical resistance of it increase largely, and afterwards hybrid FRP composites can be resist the load due to the presence of the reinforced fiber, for example, glass fiber or aramid fiber tows.

• Proceedings of the Korean Fiber Society Conference
• /
• 1997.04a
• /
• pp.26-31
• /
• 1997

유리섬유/nylon 6 복합재료의 계면결합강도를 증가시키기 위하여 r-APS(r-Aminopropyltriethoxysilane)로 유리섬유의 표면을 처리 하였다. 이때 표면처리의 최적 조건을 찾기위해서 처리후 기기분석과 계면결합강도 측정 등을 하였다. 농도, pH, 처리시간, 온도를 변화시키면서 표면처리를 한 후 흡착량을 살펴본 결과 처리 농도에 의해서는 흡착량이 단조증가하였으며 처리시간에 따라서는 5분정도에서, 처리온도에 의해서는 30C 부근에서 최대 흡착량을 보였다. 또한 pH에 따른 흡착량은 silane의 고유 pH인 10.5부근에서 최대치를 나타냈다. FR-IR 분석에 의하면 NH2의 NH3 bending mode가 1607cm-1, 1575cm-1에서 나타났으며 SiOH의 SiO band는 960cm-1에서 나타났다. XPS를 통해서는 N ls와 Si 2p의 존재를 확인할 수 있었다. 표면처리된 유리섬유와 matrix인 nylon 6를 이용해 단섬유내장시편을 만들어 fragmentation test를 한 결과 계면결합강도는 약 5분의 처리시간과 1%(wt%)의 농도에서 최대값을 보였다.

• Elastomers and Composites
• /
• v.33 no.1
• /
• pp.10-16
• /
• 1998

In DGEBA/DDM system, the curing specimen are many curing factors which can affect on thermal and mechanical properties. This study was performed to prove the effect on curing specimen prepared by changing of the curing factors which are curing time and temperature of DGEBA/DDM system. As a result on thermal and mechanical properties, flexural strength, modulus and glass transition temperature (Tg) were increased with curing time and temperature were increased. It was found that the optimum curing condition of DGEBA/DDM system cure at $150^{\circ}C$ for 3hrs at equivalent ratio of 1/1.

• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.7 no.4
• /
• pp.610-618
• /
• 1997

$Al_2O_3$/Al composite was produced by the infiltration of molten Al Into $Al_2$O$_3$ preform at 900-$1200^{\circ}C$, The process was accelerated by spreading borosilicate glass powder onto the interface between Al powder compact and $Al_2O_3$ preform. Melt infiltration initialed after incubation period, and the growth of infiltration was observed to be linearly propotional with time. The major components of the composite are $Al_2O_3$ and Al with a trace of Si which is remained from borosilicate, the reaction accelerator. Relative density of the composite increased with the particle size of $Al_2O_3$ but decreased with infiltration temperature. As infiltration temperature increases from room to $950^{\circ}C$ higher strength and fracture toughness were obtained.

• Elastomers and Composites
• /
• v.37 no.3
• /
• pp.183-191
• /
• 2002

Rubber materials with excellent damping property are widely applied for vibration isolators. The dynamic characteristics of the rubber materials for vibration isolators were investigated. Dynamic tests for rubber materials with five different hardness were performed. In dynamic tests for test specimen, non-resonance method was used to obtain the dynamic storage modulus and loss factor. Moreover, the effect of dynamic vibration frequency, strain amplitude and temperature were investigated. As results, the storage modulus and loss factor generally increase when the hardness and frequency increase, and the glass transition temperature is $-50^{\circ}C$ by a large change in modulus and loss factor.