• Title/Summary/Keyword: Bulk samples

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Comparison of instrumental methods for color change assessment of Giomer resins

  • Luiza de Almeida Queiroz Ferreira;Rogeli Tiburcio Ribeiro da Cunha Peixoto ;Claudia Silami de Magalhaes;Tassiana Melo Sa;Monica Yamauti ;Francisca Daniele Moreira Jardilino
    • Restorative Dentistry and Endodontics
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    • v.47 no.1
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    • pp.8.1-8.9
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    • 2022
  • Objectives: The aim of this study was to compare the color change of the Giomer resin composite (Beautifil-Bulk) by using photographs obtained with a smartphone (iPhone 6S) associated with Adobe Photoshop software (digital method), with the spectrophotometric method (Vita Easyshade) after immersion in different pigment solutions. Materials and Methods: Twenty resin composite samples with a diameter of 15.0 mm and thickness of 1.0 mm were confectioned in A2 color (n = 5). Photographs and initial color readings were performed with a smartphone and spectrophotometer, respectively. Then, samples were randomly divided and subjected to cycles of immersion in distilled water (control), açai, Coke, and tomato sauce, 3 times a day, 20 minutes for 7 days. Later, new photographs and color readings were taken. Results: The analysis (2-way analysis of variance, Holm-Sidak, p < 0.05) demonstrated no statistical difference (p < 0.005) between the methods in all groups. Similar color changes were observed for all pigment solutions when using the spectrophotometric method. For the digital method, all color changes were clinically unacceptable, with distilled water and tomato sauce similar to each other and with statistical differences (p < 0.005) for Coke and açai. Conclusions: Only the tomato sauce produced a color change above the acceptability threshold using both methods of color assessment. The spectrophotometric and digital methods produce different patterns of color change. According to our results, the spectrophotometric method is more recommended in color change assessment.

Testing and evaluation of the corrosion behavior of Aluminum/Alumina bulk composites fabricated via combined stir casting and APB process

  • Abdalkareem Jasim;Ghassan Fadhil Smaisim;Abduladheem Turki Jalil;Surendar Aravindhan;Abdullah Hasan Jabbar;Shaymaa Abed Hussein;Muneam Hussein Ali;Muataz S. Alhassan;Yasser Fakri Mustafa
    • Advances in materials Research
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    • v.12 no.4
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    • pp.263-271
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    • 2023
  • In this study, AA1060/Alumina composites were fabricated by combined stir casting and accumulative press bonding (APB). The APB process was repeated up to six press bonding steps at 300Ċ. As the novelty, potential dynamic polarization in 3.5Wt% NaCl solution was used to study the corrosion properties of these composites. The corrosion behavior of these samples was compared and studied with that of the annealed aluminum alloy 1060 and versus the number of APB steps. So, as a result of enhancing influence on the number of APB process, this experimental investigation showed a significant enhancement in the main electrochemical parameters and the inert character of the Alumina particles. Together with Reducing the active zones of the material surfaces could delay the corrosion process. Also, at higher number of steps, the corrosion resistance of composites improved. The sample produced after six number of steps had a low corrosion density in comparison with high corrosion density of annealed specimens. Also, the scanning electron microscopy (SEM), was used to study the corrosion surface of samples.

Study on Auger Recombination Control using Barrier SiO2 in High-Quality Polysilicon/Tunneling oxide based Emitter Formation (고품질 polysilicon/tunneling oxide 기반의 에미터 형성 공정에서의 Auger 재결합 조절 연구)

  • Huiyeon Lee;SuBeom Hong;Donghwan Kim
    • Current Photovoltaic Research
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    • v.12 no.2
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    • pp.31-36
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    • 2024
  • Passivating contacts are a promising technology for achieving high efficiency Si solar cells by reducing direct metal/Si contact. Among them, a polysilicon (poly-Si) based passivating contact solar cells achieve high passivation quality through a tunnel oxide (SiOx) and poly-Si. In poly-Si/SiOx based solar cells, the passivation quality depends on the amount of dopant in-diffused into the bulk-Si. Therefore, our study fabricated cells by inserting silicon oxide (SiO2) as a doping barrier before doping and analyzed the barrier effect of SiO2. In the experiments, p+ poly-Si was formed using spin on dopant (SOD) method, and samples ware fabricated by controlling formation conditions such as existence of doping barrier and poly-Si thickness. Completed samples were measured using quasi steady state photoconductance (QSSPC). Based on these results, it was confirmed that possibility of achieving high Voc by inserting a doping barrier even with thin poly-Si. In conclusion, an improvement in implied Voc of up to approximately 20 mV was achieved compared to results with thicker poly-Si results.

Major Elemental Compositions of Korean and Chinese River Sediments: Potential Tracers for the Discrimination of Sediment Provenance in the Yellow Sea (한국과 중국의 강 퇴적물의 주성분 원소 함량 특성: 황해 니질 퇴적물의 기원지 연구를 위한 잠재적 추적자)

  • Lim, Dhong-Il;Shin, In-Hyun;Jung, Hoi-Soo
    • Journal of the Korean earth science society
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    • v.28 no.3
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    • pp.311-323
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    • 2007
  • The Yellow and East China seas received a vast amount of sediment $(>10^9ton/yr)$, which comes mainly from the Changjiang and Huanghe rivers of China and the Korean rivers. However, there are still no direct sedimentological-geochemical indicators, which can distinguish these two end-members (Korean and Chinese river sources) in these seas. The purpose of this study is to provide the potential geochemical-tracers enabling these river materials to be identified within the sediment load of the Yellow and East China seas. The compositions of major elements (Al, Fe, Mg, K, Ca, Na, and Ti) of Chinese and Korean river sediments were analyzed. To minimize the grain-size effect, furthermore, bulk sediments were separated into two groups, silt $(60-20{\mu}m)$ and clay $(<20{\mu}m)$ fractions, and samples of each fraction were analyzed for major and strontium isotope $(^{87}Sr/^{86}Sr)$ compositions. In this study, Fe/Al and Mg/Al ratios in bulk sediment samples, using a new Al-normalization procedure, are suggested as an excellent tool for distinguishing the source of sediments in the Yellow and East China seas. This result is clearly supported by the concentrations of these elements in silt and clay fraction samples. In silt fraction samples, Korean river sediments have much higher $^{87}Sr/^{86}Sr$ ratio $(0.7229{\sim}0.7253)$ than Chinese river sediments $(0.7169{\sim}0.7189)$, which suggests the distribution pattern of $^{87}Sr/^{86}Sr$ ratios as a new tracer to discriminate the provenance of shelf sediments in the Yellow and East China seas. On the basis of these geochemical tracers, clay fractions of southeastern Yellow Sea mud (SEYSM) patch may be a mixture of two sediments originated from Korea and China. In contrast, the geochemical compositions of silt fractions are very close to that of Korea river sediments, which indicates that the silty sediments of SEYSM are mainly originated from Korean rivers.

A Study on the Factors Affecting Asbestos Exposure Level from Asbestos Abatement in Building Demolition Sites (석면 해체·제거시 공기 중 노출수준과 영향요인)

  • Kim, Ji-Yeong;Lee, Song-Kwon;Lee, Jeong Hee;Lim, Mu Heok;Kang, Sungwook;Phee, Young Gyu
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.19 no.1
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    • pp.8-15
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    • 2009
  • This study was examined to find out asbestos exposure level the factors which affected the level at asbestos abatement sites. We visited a total of thirteen building demolition sites(3 apartments, 3 schools, 4 stores, and 3 houses) were visited to collect samples and related data from August to November, 2006. The results of this study were as follows 1. The results of an analysis of bulk samples to identify types of asbestos at the asbestos abatement sites showed that the kinds of the asbestos detected were chrysotile by 50.0%, were tremolite by 2.6%, and were the contents of chrysotile by 3 to 20%. 2. The geometric mean concentration of asbestos was 0.007 f/cc(range 0.001-0.34 f/cc) and its geometric standard deviation was 5.83. Of the samples, however, 12 exceeded the Korean Occupational Exposure Limit(0.1f/cc). 3. Of the materials, textile material had the highest concentration with geometric mean of 0.016 f/cc. When asbestos-containing materials were removed using T type tools, the geometric mean concentration of asbestos was 0.061 f/cc. The level by this method was much higher than by other removal methods. In analysis by the type of building, the geometric mean concentration of asbestos in stores was 0.042 f/cc and was higher than in other buildings. 4. The Poisson regression analysis was applied to find out the factors that affect the airborne asbestos concentration. As a result of the analysis, removal using a T type tool was the most important factor affecting the asbestos concentration(p<0.01). In conclusion, the airborne asbestos concentration(geometric mean) in asbestos abatement sites was 0.007 f/cc(0.001~0.34 f/cc), and 12(14.6%) of all samples were over the 0.1 f/cc. These results showed that asbestos abatement workers have been exposed to the high level of airborne asbestos because they have not been keeping asbestos removal rule. In accordance with increases of the number of building demolition sites, the better government regulation on asbestos abatement methods should be made and be performed well at building demolition sites.

Effect of $M_{2}CO_{3}$(M=Li, Na) Addition on the Humidity Sensitivity of $V_{2}O_{5}$-doped $TiO_2$ ($V_{2}O_{5}$를 dopant로 한 $TiO_2$의 감습에 미치는 $M_{2}CO_{3}$(M=Li, Na)의 영향)

  • 강이국;송창열;신용덕
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1995.11a
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    • pp.343-346
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    • 1995
  • In this paper, the effect of alkaline oxides on the humidity sensitivity of $V_2O_{5}$(2mol%)-doped $TiO_2$(98mol%) was investigated as functions of $Li_{2}Co_{3}$, $Na_{2}Co_{3}$. III-1. Measurement of Density. When the mole% of $Li_2$O is varied 0,1,2,5mol%, the more the mole% of additives is increased, the more difference of bulk and apparent density is largely narrowed. The difference of two densities of sample containing 2mol% $Na_2O$ was large all the moat. The sample containing 1mol% $Na_2O$ was small most. III-2. Observation of porosity. The porosity and total intrusion volume according to various amounts of $Li_2O$ was reduced and those of sample containing 2mol% $Na_2O$ as 31.13%, 0.1155mL/g was the highest and 1mol% $Na_2O$ was lowed most and 5, 10mol% $Na_2O$ was more high compare with sample without alkaline oxides. III-3. Characteristic of humidity sensitivity. 1. Impedance of samples containing $Li_2O$ was high compare with sample without alkaline oxides, so we thought it showed Poor sensitivity because it have no impedance changing rapidly as function of relative humidity. 2. When the humidity was increasing from 30RH% to 90RH%, the impedance of sample containing 2mol% $Na_2O$ at 120HZ changed exponential rapidly from 6${\times}$$10^{7}$$\Omega$) to 1.25${\times}$$10^4$$\Omega$. At under 50RH% and over 50RH%, the humidity sensitivity of samples containing 2mol% $Na_2O$ was best especially in the range of the low humidity. III-4. Characteristic of TG curves. When algal me oxide $M_{2}CO_{3}$(M=Li, Na) were added into $V_{2}O_{5}$-doped $TiO_2$, the stability of humidity sensitivity of samples containing amounts of $Li_2O$ was unstable. The samples containing 1mol% $Na_2O$ was unstable.

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Preparation of $M_xZn_{0.22}Fe_{2.78-x}O_4(M=Mn, Ni)$ Films by the Ferrite Plating and Their Magnetic Properties (페라이트 도금법에 의한 $M_xZn_{0.22}Fe_{2.78-x}O_4(M=Mn, Ni)$ 박막의 제조와 자기적 성질)

  • 하태욱;유윤식;김성철;최희락;이정식
    • Journal of the Korean Magnetics Society
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    • v.10 no.3
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    • pp.106-111
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    • 2000
  • The magnetic thin films can be prepared without vacuum process and under the low temperature (<100 $^{\circ}C$) by ferrite plating. We have performed ferrite plating of M $n_{x}$Z $n_{0.22}$F $e_{2.78-x}$ $O_4$(x=0.00~0.08) films and N $i_{x}$Z $n_{0.22}$F $e_{*}$2.78-x/ $O_4$(x=0.00~0.15) films on cover glass at the substrate temperature 90 $^{\circ}C$. The crystal structure of the samples has been identified as a single phase of polycrystal spinel structure by x-ray diffraction technique. The lattice constant in the M $n_{x}$Z $n_{0.22}$F $e_{2.78-x}$ $O_4$films increases but in the N $i_{x}$Z $n_{0.22}$F $e_{*}$2.78-x/ $O_4$films decrease with the composition parameter, x. The saturation magnetization in the M $n_{x}$Z $n_{0.22}$F $e_{2.78-x}$ $O_4$films does not greatly change, in agreement with observations on bulk samples.k samples.k samples.

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Quality Variation of Domestic Wheat Compared to Imported Wheat Depending on Harvest Year (수확 연도별 우리밀과 수입밀의 품질 변이 비교)

  • Kwak, Han Sub;Kim, Tae Jong;Joo, Eun Young;Cha, Jang Hun;Kim, Ah Jin;Kim, Mi Jeong;Kim, Sang Sook
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.46 no.1
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    • pp.146-151
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    • 2017
  • Quality characteristics (moisture, protein, ash, bulk density, falling number, damaged kernel, and foreign material) of 443 domestic wheat samples harvested between 2011 and 2013 were compared with those of 160 imported wheat samples from the United States, Australia, and Canada. Moisture content of domestic wheat (10.9~13.9%) was generally higher than that of imported wheat (8.0~12.6%). Large variation in protein content was found in domestic wheat compared to imported wheat even though variation in protein content of domestic wheat tended to decrease every year, implying quality control efforts for domestic wheat. A similar trend was observed in ash content, which was approximately 0.1% higher in domestic wheat kernels over 3 years. Imported wheat samples had a falling number of 300 or above. On the other hand, some domestic wheat samples had a falling number of 300, which meant low quality of wheat kernels. Generally, quality variations in domestic wheat kernels decreased over the years; however, it is necessary to maintain minimum requirements of moisture content and falling number for high and consistent quality domestic wheat.

Comparative analysis of the microbial communities in raw milk produced in different regions of Korea

  • Kim, In Seon;Hur, Yoo Kyung;Kim, Eun Ji;Ahn, Young-Tae;Kim, Jong Geun;Choi, Yun-Jaie;Huh, Chul Sung
    • Asian-Australasian Journal of Animal Sciences
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    • v.30 no.11
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    • pp.1643-1650
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    • 2017
  • Objective: The control of psychrotrophic bacteria causing milk spoilage and illness due to toxic compounds is an important issue in the dairy industry. In South Korea, Gangwon-do province is one of the coldest terrains in which eighty percent of the area is mountainous regions, and mainly plays an important role in the agriculture and dairy industries. The purposes of this study were to analyze the indigenous microbiota of raw milk in Gangwon-do and accurately investigate a putative microbial group causing deterioration in milk quality. Methods: We collected raw milk from the bulk tank of 18 dairy farms in the Hoengseong and Pyeongchang regions of Gangwon-do. Milk components were analyzed and the number of viable bacteria was confirmed. The V3 and V4 regions of 16S rRNA gene were amplified and sequenced on an Illumina Miseq platform. Sequences were then assigned to operational taxonomic units, followed by the selection of representative sequences using the QIIME software package. Results: The milk samples from Pyeongchang were higher in fat, protein, lactose, total solid, and solid non-fat, and bacterial cell counts were observed only for the Hoengseong samples. The phylum Proteobacteria was detected most frequently in both the Hoengseong and Pyeongchang samples, followed by the phyla Firmicutes and Actinobacteria. Notably, Corynebacterium, Pediococcus, Macrococcus, and Acinetobacter were significantly different from two regions. Conclusion: Although the predominant phylum in raw milk is same, the abundances of major genera in milk samples were different between Hoengseong and Pyeongchang. We assumed that these differences are caused by regional dissimilar farming environments such as soil, forage, and dairy farming equipment so that the quality of milk raw milk from Pyeongchang is higher than that of Hoengseong. These results could provide the crucial information for identifying the microbiota in raw milk of South Korea.

Template-Based Carbon Nanotubes Field Emitter

  • Jeong, Soo-Hwan;Lee, Ok-Joo;Hwang, Sun-Kyu;Lee, Kun-Hong
    • Journal of Information Display
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    • v.2 no.3
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    • pp.78-85
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    • 2001
  • The growth of carbon nanotubes(CNTs) in anodic aluminum oxide(AAO) template and their application to a field emitter are described. AAO templates were fabricated by anodizing bulk aluminum and sputtered thin Al film on Nb-coated Si wafers. After Co catalyst had been electrochemically deposited into the bottom of the pores in AAO template, CNTs were grown by pyrolyzing $C_2H_2$. Depending on the reaction conditions, CNTs grew up to or over the top of the pores in AAO template with different structures. The morphology and structure of CNTs were observed with a scanning electron microscope and a transmission electron microscope. The diameter of CNTs strongly depended on the size of the pores in AAO template and the growing conditions. The electron field emission measurement of the samples resulted in the turn-on field of 1.9-2.2 $V/{\mu}m$ and the field enhancement factor of 2450-5200. The observation of high field enhancement factors is explained in terms of low field screening effect.

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